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After centrifugation, the extracts were separated on HILIC column by using acetonitrile-water as mobile phase. The analytes were identified and quantitated by LC-tandem MS under the positive/negative electrospray ionization and multiple reaction monitormode. The calibration curves showed good linearity in the range of 25-5000 μg/kg for melamine and cyanuric acid, and 50-10000 μg/kg for ammeline and ammelide. The limits of detection and limits of quantification were in the range of 5-20 μg/kg and 50-100 μg/kg, respectively.

牛奶样品直接用乙腈超声波提取;奶粉样品先用水溶解后再加乙腈超声波提取,高速离心后以乙腈-水为流动相,采用亲水作用色谱柱分离这4种化合物,在电喷雾正、负电离切换多反应监测模式下进行定性与定量分析,三聚氰酸一酰胺与三聚氰酸二酰胺含量在50~10000μg/kg之间、三聚氰胺与三聚氰酸在25~5000μg/kg之间,均获得良好的线性。

The suitable method to dissolve Antheraea pernyi silk fibroin fibers and the character of regenerated silk fibroin solution were investigated in this paper.

研究了柞蚕丝素纤维的溶解途径和再生丝素溶液的性质,指出硝酸钙和硫氰酸锂的浓溶液是柞蚕丝素纤维的良溶剂,再生柞蚕丝素的分子量为20kDa~102.4kDa,硝酸钙对丝素大分子的破坏程度比硫氰酸锂大。

The nitrite in food was converted to manganese bioxide precipitate by potassium permanganate under acid condition. The precipitate was dissolved in sulphuric acid and the absorptivity of manganese was determined by atomic absorption spectroscopy, so that the content of nitrite was obtained indirectly.

在酸性条件下,用高锰酸钾将食品中的亚硝酸盐先转化成二氧化锰沉淀,再用硫酸溶解沉淀,以原子吸收光谱法测定锰的吸光度,从而间接得到亚硝酸盐的含量,回收率在97.6%~105.2%之间。

The specific course of the production process is:firstly,make waste electrolyte into saturated solution,then heat it and dissolve it,remove the sodium and mix it with bischofite solution perfectly.

工艺的具体过程是:将废电解质制成饱和溶液,加热溶解、除钠,再与水氯镁石溶液充分混合,经沉降槽自然冷却降温,结晶析出合成光卤石。

Animals after chemolysis failure to homogenate respectively,centrifugate and take the pure liquid,mcasure collagenase activity with Blanckaert method,the data handled with statistics did not show obvious difference.

组织化学检测:将实验动物组、对照组、手术组和化学溶解术失败再手术组标本的纤维环内层、中层和外层分别匀浆、离心,取上清液,按Blanckaert法测定胶原酶,所得据经统计学处理差异无显著性。

A method has been deviced to improve the form of the ceric iodateprecipitate by slow precipitation in homogeneous solution.

利用碘酸亚铈能溶解于稀酸溶液而碘酸铈则不溶的区别,先用过氧化氢把全部铈离子还原,再加入碘酸铵,然后进行氧化,使碘酸铈在均匀溶液中沉淀出来。3。

When all the sodium has dissolved, a mixture of 164 parts of ethyl phenylacetateand 118 parts of diethyl carbonate is added during 5 minutes and the mixture is maintained at the boil for a further hour.

当所有的纳都溶解后,然后在五分钟内添加164份乙基乙酸苯酯和118份二乙基碳酸酯的混合物,混合物再另外维持一个小时的沸腾状态。

The NSE immunohistochemical reaction could be shown in the cell bodies and axons of motorneurons after 4 h of reperfusion, and the distribution of NSE in the cell bodies was divergent, rare and disintegrative, the axons were swollen and vanish.

再灌流4小时,脊髓前角运动神经元胞体和轴突内NSE反应阳性,胞体内NSE散乱、稀疏和溶解,轴突肿胀、扩大、消失。

In this paper, initiator is dissolved in 1-bromopropane which is solvent. Then the propene and hydrogen bromide that can be dissolved in 1-bromopropane are inlet in l-bromopropane when initiator is decomposing. The reaction occurs in fluid phase and high-purity 1-bromopropane is synthesized by one step method. In this paper, the material HBr is synthesized with NaBr and sulfuric acid at the presence of hydrobromic acid.

本论文以1-溴丙烷为溶剂,将引发剂溶于其中,加热到引发剂开始分解时再通入丙烯和HBr,使二者溶解于1-溴丙烷中,在液相中进行反应,实现丙烯&一步法&合成高纯1-溴丙烷利用NaBr与硫酸在氢溴酸存在下反应制备HBr气体,以作为合成1-溴丙烷的原料。

The present invention uses isocyanuric acid as main raw material, and adopts the following main steps: adding alkali to make solvation, chlorization, bromation, secondary chlorization, filtering and drying to prepare bromochloro-isocyanuric acid.

本发明公开了一种溴氯异氰尿酸消毒灭菌剂的制备方法。该方法以异氰尿酸为主要原料,通过加碱溶解、氯化、溴化、再氯化、过滤、干燥主要步骤制备溴氯异氰尿酸。

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