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再沉淀

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A process for treating the sludge generated by alumina sewage treating system incldues such steps as pumping the alumina sewage in sand depositing pool then in depositing pool, mixing the bottom sludge, the sewage from sand-water separator, and the regenerated water from filter to obtain backflush water, heating in desilicating heater, washing the secondary red mud to recover Na2O and Al2O3, anjd returning the washing liquid containing Na2O and Al2O3 back to the flow of production of alumina.

本发明公开了一种氧化铝废水处理系统的污泥处置新工艺,它将氧化铝废水先进入沉砂池中进行沉砂处理后才进入沉淀池中,将虹吸泥机从沉淀池中吸出的底流污泥和砂水分离器分离出的污水以及将部分经过滤器过滤后所得的再生水作为反冲洗水一起通过污泥泵送到脱硅加热器中加热得污泥热水,然后将污泥热水用于二赤泥洗涤沉降,以回收赤泥附着的Na2O和Al2O3,将洗涤赤泥后含有Na2O和Al2O3的洗液送到氧化铝生产流程中重新使用。

The results indicate that the precipitation rate of phosphoric acid is larger than 99% under the conditions of 2530 ℃, the mole ratio of trimeric cyanamide to phosphoric acid 21, two-step precipitation by trimeric cyanamide divided into two portions and separately stirring 60 min.

研究结果表明:在25~30 ℃、三聚氰胺与磷酸摩尔比为21、三聚氰胺分成两份进行两步沉淀、各搅拌60 min为三聚氰胺沉淀磷酸的最佳条件,在此条件下磷酸沉淀率大于99%;在磷酸三聚氰胺沉淀中夹带的氯化钙在固液质量比15、温度40 ℃和搅拌60 min下用水反复洗涤3次后可被完全去除;再将净化后的磷酸三聚氰胺与氨水反应,制得了符合GB 10205—2001标准的磷酸一铵和磷酸二铵产品。

The precipitate in liquor is a common problem in distilleries which have to tackle with and the frequent causations are as follows: floccule induced by three kinds of higher fatty acid ethyl ester and microthermal storage and filtration could prevent it; white flakes of precipitate induced by containers for liquor storage such as aluminous pots which produced alumina and mare nectaris which dissolved into coating and then caused precipitate; precipitate induced by undergrade additives and CP grade or AR grade additives could prevent it; precipitate induced by water quality and strict management of water quality could prevent it; precipitate induced by packing materials and the solution was acid water washing for new bottles and liquor filling after the inner of the bottles was completely dry.

白酒产生混浊沉淀是一普遍问题,常见的有絮状沉淀,主要由3种高级脂肪酸乙酯引起,可于低温贮存过滤;白色片状沉淀,由贮酒容器引起,铝罐贮酒,会产生氧化铝溶入沉淀,最好不用铝罐贮酒;酒海贮酒会溶入涂料,造成沉淀,酒海贮酒不宜过久;由劣质添加剂引起,最好使用CP级或AR级添加剂;水质引起,对水处理应严加管理;包装材料引起,新瓶应用酸性水洗,且须控干水后再灌酒。

The sediment of sulfide can be separated from the solution by filtration and syphon. After the sediment is dissolved by diluted nitric acid, Ni 2+ and Co 2+ in solution can be determined by the flame atomic absorption spectrometry method.

将沉淀过滤,或者加入明矾以加速硫化物的沉降、凝结,再用虹吸法吸去上层清液的方法将沉淀分离,用热稀硝酸将沉淀溶解后直接用火焰原子吸收法测定镍、钴的含量。

Gather a sour buffer liquid of the sugar adoption lemon to carry on taking out to lift to the sweet dew in the beer leaven, separate many sugar from ferment a liquid, is precipitate with cold methyl alcohol, get a white thick lift a thing, use the 铵 salt and boric acid of the quarter again with many sugar the formation match with a thing, adding ether to precipitate, getting white and refined sample, average each 50 gs the wet leaven cell can get such refined sweet dew to gather the sugar 0.6 gs, computing with the this kind method withdraw of produce a rate for 1.2%.

对啤酒酵母内的甘露聚糖采用柠檬酸缓冲液进行抽提,从发酵液中分离多糖,以冷甲醇沉淀,得白色粗提物,再用季铵盐和硼酸与多糖形成配合物,加乙醇沉淀,得到白色精制样品,平均每50g湿酵母细胞可得到这样的精制甘露聚糖0.6g,计算出以此种方法提取的产率为1.2%。

The nitrite in food was converted to manganese bioxide precipitate by potassium permanganate under acid condition. The precipitate was dissolved in sulphuric acid and the absorptivity of manganese was determined by atomic absorption spectroscopy, so that the content of nitrite was obtained indirectly.

在酸性条件下,用高锰酸钾将食品中的亚硝酸盐先转化成二氧化锰沉淀,再用硫酸溶解沉淀,以原子吸收光谱法测定锰的吸光度,从而间接得到亚硝酸盐的含量,回收率在97.6%~105.2%之间。

The result shows that dregginess can be checked by blowdown photoelectricity sensor after high density organic waste water enter pool,and dregginess is excluded out of pool by dredg...

结果表明,高浓度有机废水流进沉淀池中,排污光电传感器+排污泵可把检测到的沉淀物排出沉淀池,而池中上清液被浑水光电传感器,清水泵和上浮球把检测到的上清液水排入过滤装置内进行过滤,随后加入絮凝剂进行沉淀分离,再经消毒以达到二次水利用的目的成为现实。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下:一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸;蒸馏NMP;干燥增溶剂;二、在氮气气氛下,Py与NMP混匀后加入密封的反应器中,再加入增溶剂,然后加入5-氨基-2-苯并唑,搅拌;三、在氮气气氛下,将步骤二的混合液搅拌并升温至50℃~150℃后加入脂肪族二酸,再加入TPP后缩聚;四、再倾入甲醇析出沉淀,过滤,清洗沉淀,再干燥;即得到含唑环半芳香聚酰胺。

According to the result showed at 280nm and at 490nm,in the comparison of whether protein absorption top and sugar quantity top overlapped,glycoproteins would be detected preparatorily,and as a result,tubes in two distinct areas had glycoproteins by this method. Proteins were precipitated with trichloroaceticacid and with cold acetone,and glycoprotein was determined from SDS-gel.

再从各收集管的收集液中,用三氯乙酸沉淀蛋白法、冷丙酮沉淀蛋白法相结合浓缩、制备蛋白样品,进行SDS—PAGE,对SDS胶进行PAS糖链染色鉴定糖蛋白,并从茶树叶分级蛋白中准确地鉴定出两个区域的收集管中含有多种糖蛋白。

Dorsalis by salting out, ion exchange chromatography, and gel filtration chromatography. By salting out the egg homogenate, SDS-PAGE analysis revealed that the Vns were mainly precipitated in a 50~70% ammonium sulfate solution. The salted-out proteins were further purified by ion exchange chromatography, and the result showed that Vns were mainly eluted with a 0.3~0.5 M sodium chloride gradient. Finally, the elutes of ion exchange chromatography were refined by running them through gel filtration chromatography to obtain purified Vns. SDS-PAGE separated the 48- and 51-kDa purified Vns, and used them as antigens to raise polyclonal antibodies.

利用硫酸铵盐析法初步分离果实蝇卵中的蛋白质,以SDS-PAGE蛋白质电泳分析得知,卵黄蛋白主要在硫酸铵溶液浓度为50~70%时被沉淀出;盐析沉淀所得之卵黄蛋白,再以离子交换层析法进一步纯化显示,卵黄蛋白主要会在0.3~0.5 M氯化钠的浓度范围间被析出来;再将析出液浓缩后,经凝胶过滤层析法做最后的纯化,即获得纯化之卵黄蛋白。

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