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再密封

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For those slurry pump with expeller seal combined with packing or packing seal, the shaft together with impeller should be able to be rotated along pump rotation direction by hand. Otherwise the impeller clearance should be adjusted (For those slurry pump with mechanical seal, adjust the impeller gap first, then mechanical seal).

对于填料加付叶轮组合式密封或填料密封式渣浆泵,用手按泵转动方向转动轴,轴应能带动叶轮转动,不应有摩擦,否则应调整叶轮间隙(对于机械密封式渣浆泵,应先调整叶轮间隙,再调整机械密封)。

For those slurry pump with expeller seal combined with packing or packing seal, the shaft together with impeller should be able to be rotated along pump rotation direction by hand. Otherwise the impeller clearance should be adjusted (For those slurry pump with mechanical seal, adjust the impellergap first, then mechanical seal).

对于填料加付叶轮组合式密封或填料密封式渣浆泵,用手按泵转动方向转动轴,轴应能带动叶轮转动,不应有摩擦,否则应调整叶轮间隙(对于机械密封式渣浆泵,应先调整叶轮间隙,再调整机械密封)。

Connect joint of mechanical seal with shaft seal water pipeline (For newly installed shaft seal water pipelines, please clean up or rinse out sundries such as welding dregs, sand which are remnant in pipelines in advance). Start shaft seal pump, unclose shaft seal pipeline valve and turn pump shaft by manpower, if leakage, that indicates dunghill exist on shaft seal end-cover, here gland bolts should be loosened to wash mechanical seal with clean water and then impact gland.

将机械密封的接口连通轴封水管路(新安装的轴封水管路应事先将残存在管路内的焊渣,泥沙等杂物清理或清洗干净),启动轴封泵,打开轴封水管路阀门,人工转动泵轴,如有滴漏现像说明轴封端面有脏物存在,应将压盖螺栓松开用清水冲洗机械密封后,再将压盖压紧。

Connect joint of mechanical seal with shaft seal water pipeline (For newly installed shaft seal water pipelines, please clean up or rinse out sundries such as welding dregs, sand which are remnantin pipelines in advance). Start shaft seal pump, unclose shaft seal pipeline valve and turn pump shaft by manpower, if leakage, that indicates dunghill exist on shaft seal end-cover, here gland bolts should be loosened to wash mechanical seal with clean water and then impact gland.

将机械密封的接口连通轴封水管路(新安装的轴封水管路应事先将残存在管路内的焊渣、泥沙等杂物清理或清洗干净),启动轴封泵、打开轴封水管路阀门,人工转动泵轴,如有滴漏现像说明轴封端面有脏物存在,应将压盖螺栓松开用清水冲洗机械密封后,再将压盖压紧。

Preparation of the cathode includes:shaping under the press of 40Mpa, sintering at 550℃for 1 hour and at 900℃for 8 hours and threading with molybdenum bar; Considering the literatures we choose CaCl2 as salt for preparation titanium. Pretreatment of salt is for 1 hour at 100℃and for 2 hours at 300℃. Partial pressure of oxygen which need lower than 5.11×10-7Pa to reduct titanium oxides and hygroscopic property of salt need a sealed equipment to electrolyse. And finally successfully designed a satisfied one and the results show that the equipment can be satisfied the requirment of the experiment. Flow of the inert gas is 1.5L/min, the voltage is 2.8 V, temperature is 850℃and time is 2 hours during pre-electrolysis. Flow of the inert gas is 0.2L/min, the voltage is 3.1 V, temperature is 900℃and time changes with the mass of TiO2 during electrolysis, namely the greater need the longer time; To eliminate influence of salt and other impurities, the products need to wash with distilled water and dilute chlorhydric acid , then wash with dilute hydrochloric acid under supersonic wave assistant. Finally, electrometical properties of the electrolysis of TiO2 is researched by cyclic voltammetry and chronoamperometry, and results show that there are two main reodox steps, namely from TiO2 to TiO and from TiO to Ti.

阴极制备主要包括40MPa压力下模压成型、两段式烧结(1小时内升至550℃保温1小时,再1小时升温至900℃保温8小时)及烧结后TiO2块打孔用钼棒串接三个主要环节;实验中选用CaCl2作为电解熔盐,并对其进行预处理(100℃,保温1小时; 300℃,保温2小时);经热力学计算,还原钛氧化物的氧分压至少要低于5.11×10-7Pa,结合电解过程中所用熔盐CaCl2有极强的吸水性的特点,电解装置应有较高的密封性,自行设计了一套密封性可靠的电解装置,便于实验过程中熔盐预处理和氧分压的控制;通过干燥处理预电解过程中Ar流量大约为1.5L/min、电压为2.8 V、温度为850℃、时间为2小时,电解过程中Ar流量大约为0.2L/min、电压为3.1V、温度为900℃,实验结果表明电解时间与TiO2质量密切相关,质量越大需要电解的时间越长;通过自来水冲洗—稀盐酸浸泡、洗涤—在超声波辅助作用下稀盐酸洗涤,可减少熔盐及其它杂质对电解产物检测结果的影响;最后,通过循环伏安法、计时电流法对电解机理的研究,确定电解还原TiO2制备金属钛主要经历了TiO2-TiO-Ti的过程。

The synthesis method of the invention is as follows: first, 5-amino-2-(p-aminophenyl)- benzoxazole and aliphatic diacid are respectively recrystallized; NMP is distilled; solubilizer is dried; second, in an atmosphere of nitrogen, after Py and NMP are mixed evenly and added to a sealed reactor, the solubilizer is added into the reactor, followed by the 5-amino-2-(p-aminophenyl)- benzoxazole, then the mixture in the reactor is stirred; second, in an atmosphere of nitrogen, the mixture in the second step is stirred and heated to 50-150 DEG C, then the aliphatic diacid is added, followed by TPP for condensation; fourth, after methanol is poured into the reactor, the sediment is separated out from the mixture, filtered, washed and dried, so the semi-aromatic polyamide containing oxazole ring is obtained.

本发明的合成方法如下:一、分别重结晶5-氨基-2-苯并唑与脂肪族二酸;蒸馏NMP;干燥增溶剂;二、在氮气气氛下,Py与NMP混匀后加入密封的反应器中,再加入增溶剂,然后加入5-氨基-2-苯并唑,搅拌;三、在氮气气氛下,将步骤二的混合液搅拌并升温至50℃~150℃后加入脂肪族二酸,再加入TPP后缩聚;四、再倾入甲醇析出沉淀,过滤,清洗沉淀,再干燥;即得到含唑环半芳香聚酰胺。

When cooking to To dozens of raw materials have been put Sheng Tan Shaoxing wine, I altar of paper and then seal the lid Gaijin, Wanghuo first boiling and then simmer slowly slow fire.

烹制时要把几十种原料放进盛过酒的绍兴酒坛中,坛口用纸密封再用盖子盖紧,先用旺火烧沸,再用文火慢煨。

Mechanical seal assembly: In the dynamic and static loop mirror coating on the 20th floor cleaner lubricants; add lubricant bearing guided, first gently positioning ring static load bearing guide; longer shaft add the oil, the mechanical seal part of the dynamic ring gently into the shaft, the hand-push retractable seal ring should be able to freely (Note that dynamic and static part of the anti-ring to the assembly site to be in place).

机械密封装配:在动、静环镜面上涂一层洁净的20号润滑油;导轴承座抹上润滑油,先把静环轻轻定位装入导轴承座;再在泵轴上抹上润滑油,把机械密封的动环部分轻轻装渗透泵轴上,用手轻推密封环应能伸缩自如(注意动、静环部分的防转部位需装配到位)。

Mechanical seal assembly: In the dynamic and static loop mirror coating on the 20th floor cleaner lubricants; add lubricant bearing guided, first gently positioning ring static load bearing guide; longer shaft add the oil, the mechanical seal part of the dynamic ring gently into the shaft, the hand-push retractable seal ring should be able to freely (Note that dynamic and static part of the anti-ring to the assembly site to be in place).

机械密封装配:在动、静环镜面上涂一层洁净的20号润滑油;导轴承座抹上润滑油,先把静环轻轻定位装入导轴承座;再在泵轴上抹上润滑油,把机械密封的动环部分轻轻装入泵轴上,用手轻推密封环应能伸缩自如(注意动、静环部分的防转部位需装配到位)。

Mechanical seal assembly: In the dynamic and static loop mirror coating on the 20th floor cleaner lubricants; add lubricant bearing guided, first gently positioning ring static load bearing guide; longer shaft add the oil, the mechanical seal part of the dynamic ring gently into the shaft, the hand-push retractable seal ring should be able to freely (Note that dynamic and static part of the anti-ring to the assembly site to be in place).

机械密封装配:在动、静环镜面上涂一层洁净的20号润滑油;导轴承座抹上润滑油,先把静环轻轻定位装入导轴承座;再在泵轴上抹上润滑油,把机械密封的动环部分轻轻装入泵轴上,用手轻推密封环应能伸缩自如(注重动、静环部分的防转部位需装配到位)。

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