再制备

The lauan wood is used as a template to prepare Al/C and Al/ composites. Porous carbon is first pyrolyzed from the wood template. The final composites having wood structure are obtained by injecting aluminum alloy and silicone resin into the porous carbon. The microstructures, thermal expansions, and thermal conductivity of these products are analyzed by the scanning microscope, dilatometer, and conductometer. The model of thermal conduction is established.

该文以柳桉木材为模板，先将其转变为多孔碳，再通过铝合金和硅树脂的浸渍，制备了具有木材结构的Al/C、Al/两种铝基复合材料，并通过扫扫电镜、热膨胀仪和导热仅对复合材料的微观结构、热膨胀性能及导热性能进行了研究，建立了导热模型。

The copperas, a raw material, was oxidized by the oxidant under certain temperature, and then the sulfuric acid and the catalyst were added to the mixture. After the hydrolisis polymerization curing, the polymeric ferric sulfate was prepared.

采用钛白生产中的副产品绿矾(FeSO47H2O)为原料，在一定的温度下经氧化剂氧化，再加入硫酸和一定量的催化剂经水解聚合、静置熟化制备固体聚合硫酸铁。

First, the precursor polymer with azobenzene groups on main-chain was obtained by condensation polymerization between 4,4'-dihydroxyazobenzene and N,N-(2-bromoethyl)aniline through Williamson reaction. Then the azo polymer containing azobenzene groups both on main-chain and side-chain was prepared through an azo-coupling reaction between the precursor polymer and the diazonium salt of 4-nitroaniline.

设计并合成了一种新型的主侧链均含偶氮生色团的聚合物，首先通过4，4'-二羟基偶氮苯与N，N-二溴乙基苯胺之间的Williamson反应缩聚得到主链含偶氮苯基团的先驱聚合物，再通过重氮偶合反应得到目标产物，并利用核磁共振、红外光谱、紫外可见光谱、热分析等手段确认了所制备聚合物的结构。

Garlic essence is used for raw material which conducts chemical reaction with iodine or iodine chloride to generate iodated modified garlic essence. Said modified garlic essence is then passed through emulsifying and glucose absorption to make into odourless powder with good dispersiveness in water.

碘化改性大蒜素的制备方法是采用大蒜素为原料和碘或氯化碘发生化学反应，生成碘化改性大蒜素，再经乳化、葡萄糖吸附制成无臭的水中分散性良好的粉剂。

The former is to prepare polymolybdates coordinated' directly by organic ligands using Na2MoO4 and MoO3 precursors; The latter plays emphasis on exploiting a simple and effective routine to synthesize Keggin polytungstates in which the transition metal or Si acts as the heteratom by reaction precursor Na2WO4.We have synthesized a 4,4'-bipyridine bridging dumbbell-like polymolybdates a metatungs...

前者主要是制备有机配体键合的多金属钼酸盐；后者重点是探索出一个简易、有效的合成过渡金属或主族元素硅作杂原子的Keggin多金属钨酸盐的方法，然后通过变换过渡金属或有机配体的种类探讨对产物结构的影响，再对所得化合物的结构和组成通过物理测试手段进行表征，同时研究其在光、电、磁等方面的性质。

This article provided a new route to produce 4-dimethoxy phenethylamine. In basic condition, the product could be obtained through etherization, bromation, Grignard reaction, hydroxyethylation, esterification and Gabriel reaction with phenol as raw material, the overall yield is 45.0%.

提出了合成4-甲氧基苯乙胺的新方法，即在碱性条件下，苯酚首先与硫酸二甲酯反应，再选用高选择性的溴化剂溴化后，经格氏反应、羟乙基化反应和酯化反应，最后经Gabriel反应可以制备目标产物，反应总收率为45.0%。

After esterification, the ethyl-2-chloro-3-phenylpropionate reacts with diethyl malonate under the catalysis of sodium ethylate, and we obtain the corresponding triethyl ester. The-benzylsuccinic acid is formed by the triethyl ester reacting with concentrate hydrochloric acid and taking place hydrolyzation and decarboxylation reaction at the same time. In order to avoid the formation of cinnamic acid, the sodium ethylate and diethyl malonate must be react sufficiently. The course has simple operation, inexpensive materials and better yield.

具体制备工艺为：首先以L-苯丙氨酸为原料采用重氮化方法得到-2-氯-3-苯基丙酸，再经酯化得到-2-氯-3-苯基丙酸乙酯后在乙醇钠催化作用下和丙二酸二乙酯缩合，发生SN2反应，得到相应的三乙酯，然后经水解和脱羧，得到-苄基丁二酸；在实验中乙醇钠要和丙二酸二乙酯充分反应，避免生成肉桂酸乙酯；该过程操作简单，原料便宜，产率较高，总收率可达到26.8%。

Therefore, this article has put forward the concept that using hot-dip galvanizing dregs to prepare zinc powders directly;Formulate reasonable experiment craft route which according to the physicochemical characteristics of zinc that near the melting point the vapor pressure of hot-dip galvanizing will change exponential.

中文摘要：根据目前热浸镀锌行业的不断发展、锌资源日益减少和热浸镀锌渣产量逐渐增多的现状，热浸镀锌渣再生回收的问题成为行业界关注的焦点，传统上锌渣回收的方法主要是先将锌渣处理成锌锭后再用锌锭制备金属锌粉。

The addition of the matting agent mainly have two methods: the first is directly added to paint system in powder form; the second, flatting paste is prefabricated, then add them into paint system.

消光剂的添加方法主要有2种：一种是以粉状形式直接添加到涂料体系中；另一种是预先制备消光浆，再以消光浆的形式添加到涂料体系中。

Methods Forebrain ischemia model of gerbil was produced by occlusion of bilateral carotid arteries for 5 minutes.

采用双侧颈总动脉阻断法制备沙土鼠（64只）前脑缺血再灌注损伤模型，缺血5分钟。

It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发，分析对称连杆曲线上鲍尔点的产生条件，提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品，年生产总值3000万美元，产品价廉物美、选料上乘、质量保证，深受国内外客户的青睐