再制备

This specific preparation methods including: parathion of the initial reaction in acid and zinc metal in the common under redox reaction, a product of the reduction of parathion - parathion, with the sodium nitrite in the cold under diazotization reaction, and bovine serum protein tyrosine on the o-hydroxy combination of the adult immune original and immune rabbit polyclonal antibody preparation.

本发明制备方法具体包括：以对硫磷为反应初始物，在酸和金属锌的共同参与下进行氧化还原反应，得对硫磷还原产物对氨基对硫磷，再与亚硝酸钠在低温下进行重氮化反应后，与牛血清蛋白酪氨酸上羟基的邻位结合，制备成人工免疫原，并免疫新西兰大白兔制备多克隆抗体。

The invention uses the method of the fusion and direct polymerization to prepare the carboxyl-terminated lactic acid prepolymer and then copolymerize with the aliphatic polycarbonate; then the reaction is done in the twin-screw extruder to screw out the extension chain and the good polylactic acid copolymer is made.

本发明采用熔融直接缩聚的方法制备出羧基封端的乳酸预聚物，接着再与脂肪族聚碳酸酯二元醇进行共聚，然后再在双螺杆挤出机中进行反应挤出扩链，制备性能良好的聚乳酸共聚物。

For the first time we synthesized nanoscale metal hydrides of lanthanum, neodymium, samarium, dysprosium, and ytterbium with high efficiency under mild condition by complexometric catalysis instead of traditional preparation at high temperature and high pressure. It is for the first time that we synthesized lanthanide organic compounds with catalysts or initiating agents at atmosphere and ambient temperature,and some of them are new compounds. Nanometric lanthanide metal powders are prepared by thermal decomposition of the compounds in vacuum. Differently from the traditional method, size of the products prepared by our method is less than 40nm, and the activity of the reaction is very high. They are pyrophoric at atmosphere. They can make some reactions without activity or low activity show extremely high activity .We investigated influent regulations of methods, conditions to scale and special surface.

我们首次成功地用络合催化等方法取代需在高温高压下进行的传统方法，在温和条件下高效率地合成出纳米尺寸镧、钕、钐、镝、镱的金属氢化物；首次在常压常温的条件下，通过催化、引发等方法合成镧系金属有机化合物，再将其真空热分解成功地制备了纳米尺寸的镧、钕、钐、镝、镱等金属粉末；与传统方法不同，这些方法得到的产品基本颗粒尺寸小于 40 nm，遇到空气燃烧，具有极高的化学反应活性，使原来活性很低甚至观察不到活性的反应大幅度提高反应速率和产率；考察了制备方法、制备条件等因素对晶粒尺寸、比表面积大小等的影响规律。

A steel plate having a tensile strength of at least about 930 MPa (135Ksi), a toughness as measured by Charpy V-notch impact test at least about 120 joules (88 ft-lb), and a microstructure comprising at least about 90 volume percent of a mixture of fine-grained lower bainite and fine-grained lath martensite, wherein at least about 2/3 of said mixture consists of fine-grained lower bainite transformed from unrecrystallized austenite having an average grain size of less than about 10 microns and comprising iron and specified weight percentages of the additives: carbon, silicon, manganese, copper, nickel, niobium, titanium, aluminum, calcium,rare earth metals, and magnesium, is prepared by heating a steel slab to a suitable temperature; reducing the slab to form plate in one or more hot rolling passes (10) in a first temperature range in which austenite recrystallizes; further reducing said plate in one or more hot rolling passes (10) in a second temperature range in which austenite does not recrystallize, quenching (12) said plate to a suitable quench stop temperature (16); and stopping said quenching and allowing said plate to air cool (18) to ambient temperature.

一种钢板，其抗拉强度至少约930MPa135ksi），在－40℃（－40°F）下，采用夏氏V型缺口冲击试验测定的韧性至少约120焦耳（88英尺－磅），并且其显微组织包含至少约90％体积的细晶粒的下贝氏体和细晶粒的板条马氏体的混合物，其中该混合物的至少约2／3由从平均粒径小于约10微米的未再结晶奥氏体转变而来的细晶粒的下贝氏体组成，而且，其中所述的钢板包含铁和特定重量百分比的添加元素：碳、硅、锰、铜、镍、铌、钛、铝、钙、稀土金属和镁，所述钢的制备过程为：将一钢板坯加热至一个适当的温度；在奥氏体可发生再结晶的第一个温度范围内，采用一个或多个热轧道次（10），将所述板坯轧制成板材；在奥氏体不发生再结晶的第二个温度范围，采用一个或多个热轧道次（10）进一步轧制所述板材；将所述板材淬火处理（12）至一个适当的淬火终止温度（16）；停止所述淬火处理并将所述板材空冷（18）至室温。

In this study, the amino propyl trimethoxy silane was used for the surface modification of silica, and the modified silica was adsorbed to surface of clay/silica (SiO2 : Clay = 4:1 and 2:1) and the clay/silica was adsorbed by the surfactant. Also, we used Dimethyldistearylammonium chloride and Dodecyltriphenylphosphonium surfactant to modify clay/silica. Then we prepared the Epoxy/clay/silica nanocomposites and Epoxy/clay/silica/DOPO composites.

中文摘要本研究利用胺基矽氧烷改质二氧化矽，并将改质二氧化矽吸附於蒙脱土上(SiO2 ： Clay = 4：1与2：1)再分别以Dimethyldistearylammonium chloride 与Dodecyltriphenylphosphonium界面活性剂改质蒙脱土/二氧化矽并与环氧树脂制备成复材，并且再另外加入含磷阻燃剂 9，10-dihydro-9-oxa-10-phosphaphenanthrene 10-oxide与环氧树脂制备成复材。

In this paper,the method to make non-drying glue by modifying polystyrene foamed plastic waste was presented.

本文介绍了废聚苯乙烯泡沫塑料的资源化再利用—改性制备不干胶的方法；对制备工艺和产品的性能进行了优化；实验结果表明此方法制备的不干胶具有良好的不干性能，粘度大，耐水性好等优点。

Thinking of presenting problems, this research mainly studied some solid base catalysts which own higher catalysis ability and longer lifetime. Then, the phase diagram and equilibrium data of oil-alcohol-biodiesel-glycerol multiphase system were measured because the biodiesel producing process lacks of thermodynamic data.Based on a double-membranes theory and the thermodynamic data, a kinetic model was proposed. In addition, a mult-step extraction process was proposed to dispose the jatropha curcas l oil with high acid value in order to decrease the acid value. Then, a new technology of biodiesel producing using solid base as a catalyst was developed. The study objects and results are as follows.

本研究针对负载型固体碱催化剂活性组分易流失、使用寿命短的缺点，制备了高效、稳定的固体碱催化剂；针对生物柴油制备体系热力学数据缺乏的问题，测定了大豆油-醇-生物柴油-甘油体系的相图和平衡特性，在此基础上基于双膜理论，建立了固体碱制备生物柴油的动力学模型；同时针对酸价较高的麻疯果油，提出了先用甲醇或乙醇多级萃取降低酸价，再用固体碱催化制备的新工艺。

The results show that the film growth conditions strongly affect the mechanical properties of the Ti-O layers on top of the TiN-covered Ti substrates.For example,the TiN/Ti-O composite films display excelle...

结果表明，在钛合金表面制备TiN薄膜后，逐渐降低N2流量至0 sccm，沉积一层Ti膜，再用逐渐通入O2制备Ti-O薄膜的工艺制备的TiN/Ti-N/Ti/Ti-O薄膜具有较好的力学性能。

The coal tar pitch powder was used with each of 22 kinds of dispersants prepared coal tar pitch water slurry,and 6 kinds of dispersants were selected to prepare coal tar pitch water slurry with the high temperature coal tar pitch powder which has a softening point of 105℃.

采用冷冻粉碎的方法将软化点为90℃的中温煤沥青制得粒度≤200目的煤沥青粉后，再与22种分散剂制备煤沥青水浆，从中筛选出6种成浆性好的分散剂再与软化点为105℃的高温煤沥青粉制备煤沥青水浆，结果表明中温煤沥青粉比高温煤沥青粉更易制得稳定性好的煤沥青水浆。

Silver in the form of silver sulphide was recovered from waste fixing solution with sodium sulphide.

用硫化钠从废定影液中以硫化银的形式回收银，高温灼烧硫化银得纯银，再制备成硝酸银。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。