再制

Ethyl 4-[(1-hydroxy-1-methyl)ethyl]-2-propyl-1H-imidazole-5-carboxylate,the key intermediate of Olmesartan ,was synthesized from butanoic acid and o-phenylenediamine via condensation under microwave-irradiation,oxidation,esterification and the Gringard reaction.

用正丁酸与邻苯二胺为原料，在微波照射下缩合成2-丙基苯并咪唑，再氧化开环制得2-丙基咪唑二羧酸，再经酯化、Gringard反应制得抗高血压药物奥美沙坦的关键中间体2-丙基-4-[(1-羟基-1-甲基)乙基]-1H-咪唑-5-羧酸乙酯，总收率32.2%。

A selective and mild PS-DIB/ionic-liquid immobilized 2, 2, 6, 6-tetramethyl-piperidin-4-ol-N-oxyl catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via the iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TeMPO catalyst, 4-(2, 2, 6, 6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from TeMPO and 1, 4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化，制得了负载型二乙酰氧碘苯作为氧化剂。2， 2， 6， 6-四甲基－N-氧自由基哌啶醇与1， 4-二溴丁烷反应生成4-溴丁氧基－2， 2， 6， 6-四甲基－哌啶－1-氧化物，再与N-甲基咪唑发生季铵化反应，生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2， 2， 6， 6-四甲基－N-氧自由基哌啶负载离子液体。

A selective and mild PS-DIB/ionic-liquid immobilized TEMPO catalytic oxidation procedure of alcohols to the corresponding aldehydes and ketones in ionic liquid BF4 at room temperature was developed. The oxidant PS-DIB was prepared via Iodation and acetylation of polystyrene resin. For the preparation of the ionic-liquid immobilized TEMPO catalyst, 4-(2,2,6,6-Tetramethyl-1-oxyl-4-piperidoxyl)butyl bromide was first synthesized from 2,2,6,6-tetramethyl-piperidin-4-ol-N-oxyl and 1,4-dibromobutane.

将聚苯乙烯树脂先碘化再乙酰基化，制得了负载型二乙酰氧碘苯(diacetoxyiodo polystyrene，PS-DIB)作为氧化剂。2，2，6，6-四甲基-N-氧自由基哌啶醇(2，2，6，6-tetramethyl-piperidin-4-ol-N-oxyl，TEMPO)与1，4-二溴丁烷反应生成4-溴丁氧基-2，2，6，6-四甲基-哌啶-1-氧化物，再与N-甲基咪唑发生季铵化反应，生成的溴化季铵盐与四氟硼酸钠进行离子交换制得氟硼酸型2，2，6，6-四甲基-N-氧自由基哌啶负载离子液体TEMPO-IL。

In the scope of our life made cards and membership cards are made of a circle or rounded corners or other irregular situation, this is when the business card printing and membership card up forming post-pressure sected, in which the effect of cutting way is to become a wooden model and then separated from the surrounding steel blade edge around it, and then be immediately arotic post-pressure sected.

在吾人生活范围里制卡和会员卡制作物经常有圆形或圆角或其他不规则情形，这是当制卡和会员卡制作完毕后压切成型的效果，此种压切方式是先装成一个木制模型然后由周围以薄型钢片刀顺其边缘围绕，再加以紧搏后压切。

XEIKON7000 is a magnetic powder business card printing and membership card making, it business card printing and membership card making into electrical impulses, as heads of the drum for replication on the magnetic latent image, a drum with a magnetic toner box, after the latent image by adsorption of ink on the wire on the ink on the charge, and then using electromagnetic will transfer to paper of ink on the image, and finally by UV and heat treated will be part of the graphics and text on a page-melting solid ink on the paper, and the magnetic drum demagnetization after cleaning and preparation for the next page of the business card printing and membership card.

XEIKON7000是磁性粉末制卡和会员卡制作，它将制卡和会员卡制作内容转换成电脉冲，经磁头复制在磁鼓上形成磁化潜影，磁鼓经过墨粉盒，磁化潜影吸附墨粉后由电极丝对墨粉充电，再利用电磁将墨粉影象转移到纸张，最后经紫外线和高温处理将页面上图文部分的墨粉熔固，而磁鼓经过清洁和退磁，准备下一页的制卡和会员卡制作。

Ulrich Thieme said we develop a Signa worktop, where output plans for integrated ring binder, adhensive and folding machine for CIP3 data, and then through a so-called PPI interface passed to relevant machinery; through membership card before such as graphic control interface to set the monlchamus area to business card printing and membership card production machine, or even through a data control automatically get operations data and pass it to the entire system.

Ulrich Thieme说：我们在Signa不不安息台上订定一个输入策画，在那边天生用于集成装订机、胶粘机和折页机的CIP3数据，然后堵住一个所谓的PPI界面传给不关的机械；堵住会员卡制息后图文把持界面不兵墨区撤销传给制卡和会员卡制息机，甚至堵住数据把持自不静获得不不安息数据再传给合座编制。

By means of the comparative analysis in the light of historical changes between China and the foreign ones, the author considers that their similar aspects are that the supply of the relative institutions both reflects the demand regulating the relative redistributive economic relations intervened by state appropriately, both reflects a kind of legal adjustments for the relative redistributive economic relations; the relative legal institutions are paid more attentions to generally in all countries; the succored objects are all distinguished into common ones and special ones generally; citizens receiving social assistance experience the changes from bounty to right generally; social assistance undergoes the development style from negative one to positive one and the changes from free burdens wholely to burdens of some duties;the functions of nongovernmental strength in social assistance are paid more attentions to generally.Their different aspects are that the patten option of distinguished institutions for the urban and rural areas is different;the special emphasis on the contents of social assistance is some different;the level of legislation for social assistance is different;the purpose and the guiding ideology of the design for the social assistance legal institutions are different.

通过对中外社会救助法律制度历史变迁视角的比较分析，认为二者的相近之处表现为社会救助法律制度的供给都体现出规制国家适度干预相关再分配经济关系的需求，都体现为对相关再分配经济关系的一种法律调整，在各国受到普遍重视，其救助对象都区分为一般对象和特殊对象，民众接受社会救助普遍经历了由恩惠到权利的变迁，社会救助普遍经历了由消极被动到积极主动模式的发展，由完全无偿向一定义务负担的转变，民间力量在社会救助中的作用普遍得到重视；差异之处表现为城乡分制模式选择不同，社会救助内容侧重点有所不同，社会救助的法治化程度不同，社会救助法律制度设计的目的存在区别，社会救助法律制度设计的指导思想不同。

By emphasizing the post-war situation and the individual existence in Japan, Kenzaburo Oe exposes the fragility of democracy and the cruelty of Japan's imperial system. He warns that the post-war distortion of values results in the nationalism thinking, and thus delivers his post-war re-enlightenment consciousness.

大江正是通过强调在战后的时代状况和生存状态之下作为一个独立个体的主体性的重要，昭示了容许天皇制存续的日本民主主义的脆弱和天皇制自身所蕴含的暴力因素，并提示了战后价值体系的扭曲是国家主义风潮再起的精神土壤，以此警示日本民众，表达自己的战后再启蒙意识。

The coal tar pitch powder was used with each of 22 kinds of dispersants prepared coal tar pitch water slurry,and 6 kinds of dispersants were selected to prepare coal tar pitch water slurry with the high temperature coal tar pitch powder which has a softening point of 105℃.

采用冷冻粉碎的方法将软化点为90℃的中温煤沥青制得粒度≤200目的煤沥青粉后，再与22种分散剂制备煤沥青水浆，从中筛选出6种成浆性好的分散剂再与软化点为105℃的高温煤沥青粉制备煤沥青水浆，结果表明中温煤沥青粉比高温煤沥青粉更易制得稳定性好的煤沥青水浆。

Carving gravure of business card printing and membership card making production and offset business card printing and membership card making, and so on are very different, first of all the manuscripts submitted to approx 10 times, the perimeter line by hand is decisived on top of a piece of zinc tablet with a smaller machine to get an outside line back into the original large carved in a piece about an inch of eight brass, and copper strip it is some anticorrosive toppedwith films, because of copper strip is triggered from the perimeter line, so the rough body by hand for the film, when removed, and then use the medicine to the erosion of deep water, and proto-end knife with a magnifying glass and, thetolerant to the edge, sharp corners repaired, such as location on a layer of chrome, it's a printing plate.

雕刻凹版的制卡和会员卡制作制作与柯式制卡和会员卡制作等有很大的分别，首先把来稿放大约十倍，把外围线用手工刻划在一块锌片之上，再用一部缩细机械把外线缩回原大刻在一块约八份一寸的铜片上，而这件铜片上是涂有一些防腐蚀薄膜的，因为铜片只是勾上字的外围线，所以要用手工将粗身地上的薄膜刮去，然后用药水将印纹蚀深，最后仍要用放大镜及雕刻刀，耐性地将线边、尖角等位置修好，再镀上一层铬，这印版便大功告成。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。