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The results showed that temperature rise would inhibit their esterification capacity, ethyl caproate-producing capability of raw zymin of 1# high-temperature monascus improved with the prolong of the esterification time when ethanol concentration was 4 %vol and caproic acid content was 4 mL, and when ethanol concentration and caproic acid content was within proper range, caproic acid content had more effects on the formation of ethyl caproate by raw zymin than ethanol concentration.

结果表明,温度相对升高对其酯化力的形成有一定的抑制作用;高温型红曲1#酯化菌株粗酶制剂的酯化力在乙醇浓度为4 %vol、己酸含量为4 mL时,产生己酸乙酯的能力随酯化时间的延长而增强;在适宜的乙醇浓度和己酸含量范围内,己酸含量对酯化酶粗酶制剂己酸乙酯生成影响比乙醇含量的影响大。

The article in recent years the research progress of disease of oral cavity of TP prevention and cure makes one overview. The compositive TP of the basic research 1.1 TP of 1 TP is the floorboard that phenolic apperception of a kind of many hydroxyl closes matter, 25% what hold tea dry weight about, its are main component includes to express gallnut of gallnut catechu element gallnut of element of catechu of gallnut of acerbity ester, watch, watch catechu element is acerbity element of catechu of ester, watch, express gallnut of gallnut catechu element among them acerbity ester content is highest, occupy the 80%[1] of catechu element about, fighting oxidation with its unique element structure, fight the position with fight the respect such as tumor to have choppy, significant. The 1.2 TP absorption in oral cavity and metabolization Lee [2] is measured normally inside a hour after healthy person is chewing green tea Xie Huo contains juice of gargle green tea, content of the TP in saliva is very high, after observing green tea passes salivary enzymatic hydrolyze, TP is slow release and in oral cavity;Yang of local play action [the salivary level after 3] checked 6 volunteers to drink tea, chroma of the TP in making clear the saliva after drinking tea as a result is serous TP pH indicator 2 times, and the salivary TP concentration that contains gargle tea solution a few minutes to be able to produce higher level, and TP can be absorbed through oral cavity mucous membrane.

本文就近年来TP防治口腔疾病的探究进展作一综述。1 TP的基础探究1.1 TP的组成TP是一类多羟基酚类化合物的总称,约占茶叶干重的25%,其主要成份包括表没食子儿茶素没食子酸酯、表没食子儿茶素、表儿茶素没食子酸酯、表儿茶素等,其中表没食子儿茶素没食子酸酯含量最高,约占儿茶素的80%[1],并以其独特的分子结构在抗氧化、抗突变、抗肿瘤等方面占有重要的地位。1.2 TP在口腔中的吸收和代谢Lee等[2]测得正常健康人在咀嚼绿茶叶或含漱绿茶液后的一个小时内,唾液中TP含量很高,并观察到绿茶通过唾液酶水解后,TP缓慢释放并在口腔局部发挥功能;Yang等[3]检查了6位志愿者饮茶后的唾液水平,结果表明饮茶后唾液中TP浓度是血浆TP浓度的2倍,而含漱茶溶液几分钟即可产生更高水平的唾液TP浓度,且TP可通过口腔黏膜吸收。

The cis novel bisoxazoline ligands L1-L4 have been synthesized through the treatment of new cis dihydroxy diamide with p-toluenesulfonyl chloride in the presence of catalytic quantity of 4--pyridine, and the cis dihydroxy diamide could be achieved from the condensation of the amino alcohols and cis cyclopropane dicarbonyl chloride prepared via oxidation and halogenation from cis-2,2-dimethyl-3-formylcyclopropanecarboxylate with DCC.

我们以蒈醛酸内酯为起始原料,经过氧化反应、酰氯化反应得到顺式环丙烷二酰氯,然后在二环己基碳二亚胺的催化下与相应的氨基醇反应合成了顺式二羟基酰胺,再用对甲苯磺酰氯将羟基活化,最后在二甲氨基吡啶的催化下关环合成顺式双噁唑啉配体L1~L4。

The reaction of polyfluoroalkyl iodides with 4-pentenoic acids in the presence of sodium dithionite at room temperature in aqueous acetonitrile solution [CH〓CN: H〓O=3: 1 ] to gave the corresponding adducts, the latter could form γ-lactones 31~51 in the same medium in 62~92% yield.

室温下,在乙腈/水[3:1]的介质中,多氟烷基碘化物在连二亚硫酸钠的存在下与4-戊烯酸及其在2或3位上具有取代基团的衍生物进行反应,反应2~5h,起先生成两者的加成物,该加成物无需分离,在同一介质中,可进一步反应得到相应的多氟烷基取代的γ-丁内酯31~51,产率62%~92%。

P28 紫色 Formation of a peptide bond 肽键形成–4侧链具有的反应–形成二硫键-其它反应 Tyr,His,Arg Review Isoelectric Point Titration滴定 of an amino acid 滴定 Gly幻灯片 18 His Lys Glu Reaction of amino acids Section 4 Protein isolation and purification 蛋白质分离及提纯 Working With Proteins Experimental techniques for protein analysis and characterization Purification steps A cell contains many types of proteins In the lab we want to isolate a single protein for experiments Purification steps We first grow cells or isolate tissues that contain the protein of interest We break open the cells to produce a crude extract Use centrifugation离心 to separate soluble from insoluble material We fractionate 分离 the protein mixture based on properties of such as size, charge affinity or solubility.

丹磺酰氯与氨基酸反应生成荧光性质强和稳定的磺胺衍生物,用于多肽链NH 用于多肽链 3末端氨基酸的标记烃基化反应(1) 2,4-二硝基氟苯2,4-dinitrofluorobenzene,二硝基氟苯(二硝基氟苯 DNFB也叫做试剂。DNFB在弱碱性溶液也叫做Sanger试剂试剂中与氨基酸发生取代反应,生成黄色化合物二硝基二硝基苯基氨基酸(dinitro phenyl amino acid, DNP氨基酸氨基酸)苯基氨基酸氨基酸(2)苯异硫氰酸酯(phenylisothiocyanate, PITC)在弱碱性条件下,与氨基酸反应在弱碱性条件下,生成苯乙内酰硫脲 PTH衍生物,(phenylthiohydantoin, PTH)衍生物,即PTH-氨基酸,此反应又称之Edman反应,该反应是蛋白质或多肽氨基酸序列测定常用的反应。

Based on minor structural difference in the C-2 side chain, these autoregulators chemically identified to date can be classified into three types: the A-factor type, the virginiae butanolide type and the IM-2 type.

γ-丁酸内酯自动调控因子是一种由链霉菌产生的被称为微生物&激素&的小分子化合物,它控制着链霉菌次级代谢物的产生或形态分化。

ABSTRACT γ-Butyrolactone autoregulator produced in Streptomyces is a low-molecular-weight compound controlling secondary metabolism and morphological differentiation in Streptomyces.

γ-丁酸内酯自动调控因子是一种由链霉菌产生的被称为微生物&激素&的小分子化合物,它控制着链霉菌次级代谢物的产生或形态分化。

Those biodegradable materials finally form into CO2 and H2O via culture of tricarboxylic acid cycle, which can be excreted from lung, kidney, and skin. Hydroxyacetic acid is a metabolic product of amino acids. Therefore, velocity of bioldegradable materials can be controlled in vivo. The recent contraception focuses on discover a sustained release system of biodegradable materials.

生物可降解材料包括聚乳酸、聚ε-己内酯、乳酸-羟基乙酸共聚物等,这些材料有很好的生物相容性,植入体内后可经生物降解成乳酸单体,经三羧酸循环后最终成为CO2和H2O,经肺、肾、皮肤排泄,羟基乙酸也是机体氨基酸代谢产物,而且生物可将解材料在体内降解速度是可控的,用生物降解聚合物作为药物载体的缓释避孕系统是目前材料学以及避孕节育研究的一大重点。

Fat tissue is hydrolyzed and released fatty acid as well triolein by lipase; on the other hand, high fat diet can't be directly absorbed across the intestinal mucosa.it must be firstly decomposed into one 2-monoglyceride and two free fatty acids by pancreatic lipase ,which is delivered into the lumen of the gut as a constituent of pancreatic juice.

脂肪酶能够使体内的多余脂肪组织分解成三酸甘油酯,另一方面,人体摄入高脂肪食物,并不能直接被小肠粘膜吸收,而是先被小肠内的胰脂肪酶分解成2-单酸甘油酯和两个游离脂肪酸,然后和胰液一起被运输到肠道的内腔被吸收。

The results showed that the thermal stability and the dielectric properties of the cured film are greatly improved with the increasing cyrante resin mass percentage composition within the range of research.

结果表明,在研究范围内,随着氰酸酯含量的增加,固化膜的热稳定性和介电性得到了较大的改善。

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