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Nucleophilic opening of the terminalepoxide 57 by a lithium acetylide from 27 in the presence of BF3·EtO furnishedcompound 58, which had the skeleton of target molecule, subsequent conversionsinvolved the introduction of γlactone gave Annonacin.

然后以三氟化硼参与的炔负离子开环氧反应建立分子骨架,得到化合物58。随后经氢化,引入α,β不饱和丁内酯环、去保护等几步反应,就得到Annonacin。

Objective:To explore the effects of aldosterone antagonism spironolactone on cardiac fibrosis in patients with essential hypertension.

目的 :观察醛固酮拮抗剂———螺内酯对原发性高血压患者心肌纤维化的影响。

Water,glycerin,rosa centifolia flower water,butylene glycol,centaurea cyanus flower water,peg-40 hydrogenated castor oil,propylene glycol,ppg-26-buteth-26,phenoxyethanol,methylparaben,sorbic acid,benzophenone-4,pentadecalactone,citrus aurantium dulcisoil,panthenol,menthyl lactate,sodium hydroxide,glycyrrhiza glabraroot extract,aesculus hippocastanumseed extract,citrus aurantium amaraoil,allantoin,limonnene,linalool,blue 1(ci 42090),yellow 5ci 19140

水,甘油,千叶蔷薇花水,丁烯二醇,矢车菊花水,PEG-40氢化蓖麻油,丙二醇,PPG-26-丁醇聚醚-26,苯氧乙醇,对羟基苯甲酸甲酯,山梨酸,二苯甲酮-4,环十五内酯,甜橙油,泛醇,乳酸孟酯,氢氧化钠,甘草根萃取,七叶树籽萃取,苦橙油,尿囊素,柠檬精油,芳樟醇,蓝,黄水:几乎所有护肤品成分第一位都是水。

Methods The kindling model of epilepsy induced by corciaria lactone in rats was used.

方法采用马桑内酯慢性致痫大鼠模型,通过免疫组化方法观察Merlin在点燃组、未点燃组及对照组中颞叶皮层及海马CA1区的表达。

4R,5S,6R-5,6-Bis-allyl-6-aldehyde-γ-hexanelactone I-145 was prepared from D-arabinose by six steps. Compound I-145 underwent Mukaiyama-type intramolecular aldolization to produce bicyclooctane I-147 stereospecifically.

我们以D-阿拉伯糖为起始原料,经六步反应,得到(4R,5S,6R)-5, 6-二烯丙氧基-6-醛基-γ-己酸内酯I-145,然后I-145发生分子内的Mukaiyama式aldol缩合反应,完全立体专一性地得到环化中间体I-147。

It was found that the reactions of C_(60) with anthranilic acids and isoamyl nitrite in the presence of triethylamine unexpectedly afforded C_(60)-fusedδ-lactones,which would be difficult to be prepared by other known methods.

通过在三乙胺作用下,富勒烯与邻氨基苯甲酸类化合物和亚硝酸异戊酯的环化反应,首次合成了一系列富勒烯并六元环内酯。

Series of FAnC(n=1~4) were synthesized by acylation reaction of FAn (scheme 1) with cinnamyl choride.

通过肉桂酰氯与ε-己内酯改性丙烯酸酯间的酰基化反应,合成了一系列光敏性大单体。

The synthesis, characterization and polymerization of a new cyclic 6-(N-isopropyl acylamine ethylidene)-ε-caprolactone were reported.

研究了官能团化新型己内酯单体的合成及其与丙交酯无规共聚物的降解性能。

A series of ABEPS were synthesized from long chain fatty acids, benzene, polyglycol and 1, 3-propane sultone by the procedure of Friedel-Crafts acylation, Huang-Minlon reduction, Williamson and sulfonation reaction, and these compounds had never been reported in the past time.

以长链羧酸、苯、多缩乙二醇和丙烷磺内酯为初始原料,依次经Friedel-Crafts酰基化反应、Huang-Minlon还原、Blank反应、Williamson成醚以及磺化反应等过程,合成了系列未见报道的ABEPS。

In this report, half-esterification between these pendent hydroxyl groups of hydroxyl-PU and maleic anhydride could lead to new pendent groups, carboxylic groups. These highly polar carboxylic groups in the side chain of PU could play the role of internal emulsifier. They had self-dissociation ability in the water or were neutralized first by appropriate amount of base. Then, PU bearing carboxylic group could dispersed steadily in the water, named aqueous-based polyurethane dispersion.

在本论文中,利用原来亲油性Hydroxyl PU主链段上悬挂的羟基经由与琥珀酸酐的半酯化(Half-esterification Reaction)反应后,使PU在侧链上悬挂具有强极性的羧酸基,其可作为聚胺酯分子中的内乳化剂,羧酸基能在水相中自身解离产生离子或加入适量碱使之中合,使聚氨酯高分子能够稳定分散於水中,即所谓水性PU分散液(Aqueous-based Polyurethane Dispersion)。

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