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Cystamine was used as the internal standard. Using this HPLC-FD method, the plasma total homocysteine concentration was determined in 86 patients with brain infarction, 66 patients with myocardial infarction and 80 healthy controls.

方法用TCEP将血浆中各种形式的Hcy还原成游离的总Hcy,以胱胺作内标,巯基特异性荧光衍生剂SBD-F对Hcy、胱胺等含巯基化合物进行柱前衍生,然后行高效液相色谱-荧光检测。

The results show that the effect of addition or no-addition of degasser on grain refinement of Al-5.0%Si alloy ingot is...

结果表明,除气剂的添加与否对Al-5%Si合金铸锭组织的细化没有影响,铸锭由粗大的柱状晶组织构成;采用合适的超声波处理时间,Al-5%Si合金铸锭的等轴晶获得率大幅度提高,可使整个铸锭组织变为细化的等轴晶组织;超声波振动时间过长将导致铸锭内气孔的增加;根据克劳修斯-克拉柏龙方程,某一强度的超声波引起的压力冲击波作用,导致液相转变为固相,引起了超声波的细晶作用。

CFB (Circulaiing Flued-bed Boiler), which could desulphurize by adding the lime stone in boiler, was adopted in the project of petroleum coke taking the place of oil; IGCC was adopted in coal to gas project; PC+FGD, such as limestone/plaster wet type desulfurization, liquid spray flue gas desulfurization, electron beam flue gas desulfurization and sprayed dry type desulfurization etc., was adopted in the other projects of thermoelectricity. Desulfurization inside boiler needs less running expenses but high investment and lower desulfurization efficiency.

主要为:高硫焦代油项目燃用石油焦,采用循环流化床炉内加石灰石脱硫;煤造气采用整体煤气化联合循环工艺;其余热电项目则采用煤粉炉加炉外烟气脱硫,具体的脱硫工艺选择有石灰石/石膏湿法脱硫、液柱喷射烟气脱硫、电子束法烟气脱硫以及旋转喷雾干燥法脱硫。

A method is introduced for quantitative determination of cinmethylin by gas chromatography on 5 % ov - 101 packed column and flame - ionigation detector using dipropyl phthalate as internal standard The method was simple, rapid, accurate and practical.

采用气相色谱法, 5% OV— 101填充柱和氢火焰离子化检测器,以邻苯二甲酸二丙酯为内标,对环庚草醚进行定量测定。

To establish a MPLC method for the content determination of resveratrol in Polygonum cuspidatum Sieb. Et. Zucc, Analytical column SOURCE 5RPC ST 4.6/150 was used with a mixture of acetonitrile+water (30+70,volume ratio ) as mobile phase ,with a flow rate of 1ml/min and the UV detection wavelength was 306nm, The linear range was 0.6-1.6mg/ml (r=0.9919). The average recovery of prodatin was 103.0%-90.4%(RSD=7.21%). The method is convenient and accurate. Result indicated a reverse phase chromatography media based o n polystyrene/divinyl benzene has excellent resolution for resveratrol in cuspidatum. P rovide theoretical support for process development.

色谱条件采用SOURCE 5RPC ST 4.6/150预装柱,以乙腈/水(体积比30/70)溶液为流动相,流速1ml/min、检测波长为308nm,结果表明,白藜芦醇在0.6~1.6mg/ml的浓度范围内峰面积积分值与浓度的相关系数r=0.9919;所测定的虎杖饮片中白藜芦醇平均含量为0.304%,平均回收率为103.0%~90.4%;实验表明,以聚苯乙烯为基架的反相介质对于虎杖中自藜芦醇具有良好的分辨率,适合其有效成分的检测、分离,对虎杖中白藜芦醇制备的科学研究过渡到工艺开拓有很好的借鉴。

Methods An SE-30 capillary column (30 m × 0.25 mm × 0.25 μm) and a flame ionization detector were used when n dodecane was used as the internal standard.

采用 SE 30 (30 m×0.25 mm×0.25 μm)石英毛细管色谱柱,以正十二烷为内标,进样口温度210 ℃,检测器温度300 ℃的气相色谱测定百秋李醇含量。

An electron microscopic study of resting cysts and their organelles in Paraurostyla weissei has revealed that:⑴The cyst wall is composed of four layers named from outside to inside:ectocyst,mesocyst,endocyst,and granular layer.The granular layer is delimited by the cell pellicle.Both the layer and pellicle contain a few vesicles.

为研究纤毛虫休眠状态下细胞的分化及其胞器的特征,本文以透射电镜术显示,魏氏拟尾柱虫休眠包囊中,颗粒层壁内有小泡,表膜位置也偶见小泡样结构,大部分线粒体以多个相互聚集在一起,自噬泡将线粒体等胞器包裹在内经历消化过程,细胞内膜系统十分发达。

An EPMA was performed quantitatively on the influence of Ce upon the Mn segregation in cellcrystals, columnar and Equiaxial dendrites of high-Mn steel.

与此同时,用电子探针微区分析考察了Ce对高锰钢中Mn在胞晶、柱状树枝晶及等轴晶内偏析的定量影响。

This factory's main products cre:double-spoke hand mheels,five-pointed-star-shaped knobs,arrow-shped handles,Tshaped handies,ect.,more than thity series,over two hundred special rubbr pats,nylonplasdic parts,it is also possible for this facty to produce and make all kinds of non-atsndard operating parts and special-shapediai-shpepedsealing parts according to the requireements of the customers.

弓行拉手、内波纹手轮、背波纹手轮、圆轮缘手轮、双幅条手轮、双柄手轮、小波纹手轮、镀铬手轮、手柄球、长手柄套、转动手柄、可折手柄、可调位手柄、方形拉手、椭圆拉手、星形手柄、碟形手柄、三角箭形把手、椭圆手柄套、铣床手轮、GB4141.23波纹手轮、小手轮、平面手轮、带可折手柄满幅手轮、表盘满幅手轮、把手、十字把手、压花把手、通孔把手、定位把手、T形把手、直纹把手、捏手、三棱把手、偏转旋钮、手柄套、小转动手柄、锥柱手柄、球头手柄、单柄对重手柄、双柄对重手柄、外方卡盘扳手、摇手柄、手柄座、锁紧手柄座、圆盘手柄座、4501分度盘、4502大把手、586刻度盘、工作灯、手柄杆、压配式油标、旋入式六角圆形油标、长型油标、圆形长拉手、等三十多种系列,二百多种规格,满足不同用户的需要,生产制造各种机械封件,特种橡胶件,尼龙塑料件,也可根据用户需要,生产制造各种非标操作件,异形密封件。

Three strains of bacteria were isolated from haemolymph, hepatopancreas, ascites and muscle of the diseased Eriocheir sinensis caused by aeromonas. All of the three isolates were Gram-negative rods, motile by means of single polar flagella, and were facultatively anaerobic; Glucoce was catabolized with production of acid and gas; Oxidase was positive.

利用硫酸铵盐析、Sephadex G-100凝胶层析和DEAE-Cellulose离子交换柱层析等方法,从其胞外产物中分离纯化出了2种胞外蛋白酶,用SDS-PAGE电泳测得两种蛋白酶的分子量分别为39.6kD和20kD.39.6kD蛋白酶活性在50℃~60℃范围内热稳定性最好,最适pH为9,而20kD蛋白酶的最适温度为50℃,最适pH为8。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。