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Transfers the bottom type resistance furnace structure outer covering becomes by the steel plate and the section welding, the furnace body welds the system full circle densely by the steel plate, lower part the spatial installment has the turntable support, the kingbolt, on the furnace body foot ledgerwall the installment has the velocity modulation electrical machinery and the transmission gearbox, through the umbrella type gear and the main axle connection, transfers the bottom type resistance furnace's stove village material to use fan-shaped ultra light quality high strength 0.6g/cm3 to conserveenergy the fireproof heat preservation brick, the heat insulating layer uses the aluminum silicate textile fiber felt and the inflation heat preservation powder, the resistance silk thread becomes spiral-shaped, installs according to the average temperature rule in the resistance wire trough, the basealso arranges the resistance wire in the special-purpose trough, in such stove the temperature is even, the work piece and the turntable cannot bump with the resistance wire, resistance wireThe service life is long, is not easy to damage.

转底式电阻炉结构外壳由钢板和型钢焊接而成,炉体由钢板密焊制成圆型,下部空间安装有转盘支撑,旋转主轴,炉体最下部底板上安装有调速电机和变速器,通过伞型齿轮与主轴连接,转底式电阻炉的炉村材料采用扇形超轻质高强度0.6g/cm3节能耐火保温砖,保温层采用硅酸铝纤维毡和膨胀保温粉,电阻丝线成螺旋状,按均温规律安装在电阻丝槽内,底部也布置电阻丝在专用槽内,这样炉内温度均匀,工件及转盘不会与电阻丝相碰,电阻丝使用寿命长,不易损坏。

Transfers the bottom type resistance furnace structure outer covering becomes by the steel plate and the section welding, the furnace body welds the system full circle densely by the steel plate, lower part the spatial installment has the turntable support, the kingbolt, on the furnace body foot ledger wall the installment has the velocity modulation electrical machinery and the transmission gearbox, through the umbrella type gear and the main axle connection, transfers the bottom type resistance furnace's stove village material to use fan-shaped ultra light quality high strength 0.6g/cm3 to conserve energy the fireproof heat preservation brick, the heat insulating layer uses the aluminum silicate textile fiber felt and the inflation heat preservation powder, the resistance silk thread becomes spiral-shaped, installs according to the average temperature rule in the resistance wire trough, the base also arranges the resistance wire in the special-purpose trough, in such stove the temperature is even, the work piece and the turntable cannot bump with the resistance wire, resistance wireThe service life is long, is not easy to damage.

转底式电阻炉结构外壳由钢板和型钢焊接而成,炉体由钢板密焊制成圆型,下部空间安装有转盘支撑,旋转主轴,炉体最下部底板上安装有调速电机和变速器,通过伞型齿轮与主轴连接,转底式电阻炉的炉村材料采用扇形超轻质高强度0.6g/cm3节能耐火保温砖,保温层采用硅酸铝纤维毡和膨胀保温粉,电阻丝线成螺旋状,按均温规律安装在电阻丝槽内,底部也布置电阻丝在专用槽内,这样炉内温度均匀,工件及转盘不会与电阻丝相碰,电阻丝使用寿命长,不易损坏。

With Mab 2A3, the first positive cells were detected at the limb bud stage of the embryos. Distinguishable positive haemocytes with a diameter of about 7μm appeared in embryonic-nauplius. At the following nauplius I stage, configuration of haemocytes became more integrated and clear. Their diameters were almost similar to those of haemocytes from adult shrimp. With Mab 1H11, the first positive granular haemocytes were identified at the stage of embryonic-nauplius which existed in clusters with positive punctate fluorescence of granules distributed around the periphery of granular haemocytes.

通过对包括囊胚期、原肠胚期、肢芽期、膜内无节幼体期和无节幼体Ⅰ期在内的中国对虾胚胎的间接免疫荧光检测,最早在肢芽期胚胎中检测到2A3阳性信号;在膜内无节幼体期,2A3阳性血细胞平均直径约7μm,聚集成簇;在无节幼体Ⅰ期,血细胞形态更加完整清晰,平均直径已与成体对虾血细胞相似。1H11阳性大颗粒细胞最早在膜内无节幼体期胚胎中出现,这些细胞同样成簇存在,在其细胞质外围可见点状荧光。

Pollution discharge pump, adopting special big channel impeller structure, greatly increases feculency discharging ability, and effectively make solid particle with diameter being 50% of pump outlet diameter; the type 4 can be fitted with various protective devices according to customer's requests, including stator winding temperature-rise protection, bearing temperature rise protection, oil container leakage protection, etc to enhance the exploitation reliability; adopting inner flowing recycling system to use medium cooling electric machine section to make usage more safe.

排污泵采用了独特的大通道叶轮结构,大大提高了污物通过能力,能有效的通过直径为泵口径约50%的固体颗粒;本泵型4可根据用户的要求安装各种保护装置,包括:定子绕组温升保护、轴承温升保护、油室漏油保护等以提高电泵的使用安全性;可采用内自流循环系统,利用介质冷却电机部分,使用更加安全,同时,还可以利用此结构将电泵以干式固定形式安装;采用最新材料精制而成的机械密封,其使用寿命可达8000小时以上;可采用双导轨自动耦合安装装置,使机组的安装、维修方便、快捷;可根据用户的需要配备各种形式的排污泵专用控制柜以实现自动化管理。

The dissertation mainly consists of two parts:1. The Reaction Chemistry of Alkynes under Palladium Catalysis Part 1 studies the reaction α,β-unsaturated carbonyl compounds with alkenylpalladium intermediate generated by nucleopalladation, and discovered 1 the Pd-catalyzed tandem addition reaction of halides, alkynes and α,β-unsaturated carbonyls,2 the four-component tandem addition reaction of halides, alkynes and α,β-unsaturated carbonyls, 3 the tandem intramolecular oxypalladation-conjugate additionreaction of alkynoic acids with α,β-enals. These new reactions provide notonly efficient highly stereoselective methods for the synthesis of γ,δ-unsaturated,polyunsaturated carbonyl compounds and γ-lactonic aldehydes, but also thebasic transformations for a number of C-C bond formation reactions which can be usedto design synthesis of many acyclic, cyclic or polycyclic compounds.

本论文的主要工作分为两个部分:一、钯催化下炔烃的反应化学在本小组前人工作的基础上,我们详细研究了炔烃亲核钯化产生的烯基钯中间体与α,β-不饱和羰基化合物的反应,发现两价钯催化下卤离子-炔烃-α,β-不饱和醛酮的串联加成反应、卤离子-炔烃-α,β-不饱和醛酮的西组分串联加成及炔酸分子内氧钯化-串联Michael型加成反应;由此发展了γ,δ-不饱和醛酮、多不饱和羰基化合物和带有醛酮基侧链的γ-丁内酯衍生物的高立体选择性合成方法,这一过量卤离子存在下的烯基钯对α,β-不饱和羰基化合物共轭加成反应的发现,为大量碳-碳键形成反应的实现提供了基础,使我们能够从这一基本反应出发,设计和开发多种分子内、分子间的碳碳成键反应,以好的立体、区域选择性组建开链、环状及多环类型的化合物。

Based on the results, it has found that six distinct layers can be identified from lateral to medial in the olfactory bulbs, and the adults have more cells than the subadults. Ventricles of the adults take up larger vacuity, have richer choroids plexus, and primordial pallium and primordial hippocampus of them are more developed than the subadults, in which the primordial piriform is well-developed. Ventral to the primordial hippocampus, there is a septal area which can not be divided into medial and lateral parts in both adults and subadults, nor there is lateral limiting sulcus to separate the primordial piriform and the corpus striatum, but only in the subadults, a medial limiting sulcus can be clearly identified to separate the primordial hippocampus and the septal area. Besides, the corpus striatum of Onychodactylus fischeri is paleostriatum. The cell group that located at two sides of the third ventricle is amygdale, and shape and size of neurons within the telencephalon are poorly differentiation.

结果表明:爪鲵嗅球内细胞从外到内大致可分为6层结构,亚成体的细胞数量少于成体;成体爪鲵的侧脑室所占空间较大,脉络丛更为丰富,原始大脑皮层和原始海马都比亚成体发达,后者大脑内原始梨状区较为发达;隔区位于原始海马的下方,成体和亚成体都没有外侧隔核和内侧隔核之分,也没有外侧界沟作为原始梨状区和纹状体的分界,而在亚成体的侧脑室壁有内侧界沟区分原始海马和隔区,成体则没有;此外,爪鲵的纹状体属于古纹状体,杏仁核是位于第三脑室两侧的两个细胞团,端脑内细胞形态和大小分化较为单一。

A one-step method for the synthesis of aromatic indolizine derivatives byintramolecular 1,5-dipolar cyclization reaction of 2-(2-arylethenyl)pyridinium N-ylidesin the presence of an oxidant has been studied for the first time. In the presence ofelectron-deficient olefins, however, 2-(2-phenylethenyl)pyridinium N-ylides underwent1,3-dipolar cycloadditions and then aromatized in situ by TPCD to produce indolizinederivatives, indicating 1,3-dipolar cycloaddition proceed more readily than 1 ,5-dipolarcyclization in these conditions. Pyridinium disubstituted N-ylides, readily obtainedfrom corresponding pridinium and β-chlorovinyl ketone, underwent thermalintramolecular 1,5-dipolar cyclization to give indolizine derivatives easily.Indolizinecarbaldehyde derivatives were synthesized starting from 2-pyridinecarbaldehyde in four-steps involving 1,3-dipolar cycloaddition reaction.

本文首次研究了2-(2-芳基乙烯基)吡啶N-叶立德在氧化剂存在下的分子内1,5-偶极环化反应,采用一锅法合成了中氮茚衍生物;研究了这些N-叶立德的1,5-偶极环化和1,3-偶极环加成反应的选择性,发现当有缺电子烯烃存在时,优先进行1,3-偶极环加成反应,而不再发生分子内1,5-偶极环化反应;由β-氯乙烯酮方便地得到了烯丙基N-叶立德,他们在加热时进行分子内1,5-偶极环化反应而得到中氮茚衍生物;由2-吡啶甲醛为起始原料,通过1,3-偶极环加成反应等四步反应,得到了重要的中氮茚甲醛衍生物,这些反应都具有条件温和和操作简便的特点,是合成中氮茚衍生物的新方法。

The results showed that: at metaphase I, the homoeologous chromosome pairing among different F1 hybrids ranged from 2.0 to 11.4 bi-valents formed by homoeologous chromosomes per pollen mother cell, and very few multivalents, and even very few bivalents were formed by two chromosomes within one genome rather than homoeologous chromosomes in some PMCs; at anaphase I, all biva-lents were disjoined and most univalents were divided.

结果表明在中期I阶段,这些杂种一代的近缘染色体联会变化很大,每个花粉母细胞中二价体形成的数目从平均2个到11.4个不等,甚至在某些花粉母细胞中,还发现极少的多价体和非部分同源染色体所形成的单基因组内二价体;在后期I时,所有的二价体分离,同时多数单价体也分离,分离的二价体和分离的单价体都移向两极,从而形成两组染色体;因为这时完整花粉母细胞中分离的二价体在两组染色体中总是对应出现,从而根据半二价体上染色体重组的位置可以分析在二价体的四分体时期发生在非姊妹染色体之间的多种染色体交换类型,如单交换、三线双交换、四线双交换、四线三交换和四线多交换。

Their common structure and annual changing pattern of mycorhizae are as follows: Fungi infect and form endomycorrhizal structure with plants throughout the latter's grown period, and hyphae exist in the cortical cells of roots in the following four forms: Coffee-colored or yellow big peloton consisting of twisted hyphae; Dust-colored or yellow big peloton consisting of fragmentary hyphae; Colorless scattered hyphae; Orange or yellow small peloton with blurry hyphae.

发现四种杓兰的的菌根结构及其在一个生长周期中的动态变化有以下共同特征:在其成年生活期的各个时期,都有真菌入侵形成内生菌根结构,菌丝在其根部皮层细胞内有四种存在状态:咖啡色或黄色、菌丝扭结缠绕而成的大菌丝结;灰褐色或黄色、由片断菌丝组成的大菌丝结;无色、零散的菌丝;橘红色和黄色、菌丝形态模糊的小菌丝结。

On the basis of the masteries for the aluminum oxide ore pulp drying and calcination, a mathematical model was developed for simulating the process of heat transfer and the calcination of two-phase flow in a new type furnace designed by Zhongzhou Branch Company, China Aluminium Corporation Limited. The fields of velocity, temperature and pressure of the two-phase flow and the reaction time were gained by optimizing calculation under the condition of different operational parameters and geometric parameters. The effect of vent position velocity and atomization particle diameter on the drying and calcination technology of aluminum oxide ore pulp was discussed.

在了解氧化铝矿浆干燥、烧成工艺及设备的基础上,针对中国铝业股份有限公司中州分公司开发的一种新的氧化铝矿浆干燥和烧成炉,建立了矿浆干燥、烧成炉内气固两相流的流动传热以及烧成过程的数学模型,就干燥、烧成炉运行参数及各几何参数进行优化计算,得出了炉内气固两相流动的速度场、温度场、压力场以及颗粒干燥和烧成反应时间,并分析讨论了喷口位置、喷口速度、颗粒雾化粒径等参数对氧化铝矿浆干燥、烧成工艺的影响。

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