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But the concentration of Li2CO3 remains nearly consistent and a new component, CH3OLi, is found in SEI. It can be concluded from these results that anisole reacts with the reduction product of EC and DEC, RCO3Li, in the first process of Li+ intercalating into the carbon electrode. The obtained CH3OLi is helpful in building up a more effective and stable SEI of the carbon electrode, reducing the cointercalation of solvent molecular. All these contribute to the improvement of the cycle performance of lithium-ion battery.

根据以上分析结果,提出了苯甲醚对锂离子电池循环性能的影响机理:在Li+嵌入石墨电极的初次过程中,苯甲醚和EC、DEC的还原分解产物RCO3Li发生基团交换反应,生成CH3OLi,该产物能有效提高石墨电极表面SEI的稳定性,减少锂离子嵌入石墨过程中引起的溶剂分子共嵌入,从而改善电池的循环性能。

Purposes:With ethanol, ethyl ether, chloroform, benzene, ether and other immiscible oil, and with some solvents can be formed azeotrope.

用途:与乙醇、乙醚、氯仿、苯、石油醚等混溶,并与可其中一些溶剂形成共沸物。

In the reaction of substituted arylamine and sulfuric acid, and utilizes the feature of that said inert organic solvent is easy to form azeotrope with water to continuously deliver the water produced in the couse of reaction from the reactor.

本发明在取代芳胺与硫酸的反应中加入了一种惰性的有机溶剂,如:氯苯,二氯苯,三氯苯,硝基苯等,利用其易与水形成共沸物的特点,将反应生成的水不断地导出反应器。

Batch extractive distillation is used to separate azeotrope or the mixture of which the relative volatility is close to 1.0. For it has both advantages of batch distillation and extractive distillation, batch extractive distillation is becoming increasingly important to the production of small scale and high value products like fine chemicals and pharmaceuticals.

间歇萃取精馏是分离共沸物或近沸物的一种方法,由于它结合了间歇和萃取的优点,特别适用于化工、制药、溶剂回收、天然产物提取等产量小,品种多的行业,因此间歇萃取精馏近年来已成为非常活跃的研究和开发领域。

In this paper,chain transfer constant of graft copolymerization of SBS and MMA was determined.

测定了MMA与SBS接枝共聚合的链转移常数,讨论了引发剂浓度、温度及溶剂对链转移常数的影响。

Its bonding characterization and stability are discussed. The results show that these complexes are covalence complexes and that both the in-plane σ-bond and the in-plane π-bond in these complexes play an important role. The ESR spectra of VO -Ser system, VO -Ser-Phen system and VO -Ser-Bipy system in binary solvent glycol/water (V/V=1: 1) solution at various acidities (pH=1~14) have been observed at low temperature. It is found that in different pH ranges different structural complexes are formed.

测定了五种氨基酸席夫碱铜配合物的室温多晶粉末ESR谱、在不同溶剂中的室温及低温溶液ESR谱,确定配合物的配位环境;对室温溶液谱中观察到的二级效应和驰豫效应给予了理论解释、计算了驰豫参数;根据低温ESR波谱,计算了配合物的成键特性及稳定性,发现此类配合物为共价型配合物,平面内σ配键和平面内π配键均起重要作用。

The solvent selection for extractive distillation and separation of azeotropic mixtures by batch extractive distillation were studied via theoretical analysis and the experiment.

本文通过理论分析和实验相结合的方法,主要研究了共沸物萃取精馏溶剂的选择以及共沸混合物的间歇萃取精馏工艺。

The copolycondensation type polyamic acid was synthesized by using 3,3', 4,4'-Benzophenonetetracarboxylic dianhydride as the dianhydride monomer, 4,4'-Diamino diphenylmethane and 4,4'-Oxydianiline as the diamine monomer under microwave irradiation in Dimethylformamide.

在微波辐射条件下,采用3,3',4,4'-二苯酮四羧酸二酐、4,4'-二氨基二苯甲烷和4,4'-二氨基二苯醚为单体,N,N'-二甲基甲酰胺为溶剂,低温合成一种共缩聚聚酰亚胺的前驱体聚酰胺酸,化学亚胺化脱水环化生成BTDA型共缩聚聚酰亚胺。

The copolycondesation type polyamic acid was synthesized by using pyromellitic dianhydride and 3,3',4,4'-benzophenonetetracarboxylic dianhydride as the dianhydride monomers, 4,4'-diamino diphenylmethane and 4,4'-oxydianiline as the diamine monomers under microwave irradiation in dimethylformamide.

在N,N'-二甲基甲酰胺溶剂中,以均苯四甲酸酐和3,3',4,4'-二苯酮羧酸二酐为二酐单体,4,4'-二氨基二苯醚和4,4'-二氨基二苯甲烷为二胺单体,采用微波辐射低温溶液共缩聚,合成了聚酰胺酸预聚体,然后亚胺化脱水、环化,生成共缩聚聚酰亚胺。

It is prepared from titanium tetrachloride carried on an alcohol carrier that Mg and Li chlorides with molar ratio of 1:(2-20) are dissolved in alcohol, and by: co-dissolving Mg chloride and Li chloride in a low carbon alcohol and stirring at high speed in an inert medium to form micro-particles; reacting the said alcohol with titanium tetrachloride twice, adding organic acid polyester at first time, washing out uncarried titanium tetrachloride, and drying to obtain powdery pruduct.

它是由四氯化钛负载于将氯化镁和氯化锂共溶于醇形成的醇合物载体上组成,其中氯化锂与氯化镁的摩尔比为1∶2~1∶20。这种主催化剂组分的制备有两个步骤:(1)无水氯化镁和氯化锂共溶于低碳醇中形成醇合物,并在惰性介质中高速搅拌形成醇合物微粒;(2)醇合物与四氯化钛进行两次反应,其中第一次反应时加入有机酸多元酯。反应结束后用惰性溶剂洗去未负载的四氯化钛,干燥后得到呈粉末状的主催化剂组分。

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It has been put forward that there exists single Ball point and double Ball points on the symmetrical connecting-rod curves of equilateral mechanisms.

从鲍尔点的形成原理出发,分析对称连杆曲线上鲍尔点的产生条件,提出等边机构的对称连杆曲线上有单鲍尔点和双鲍尔点。

The factory affiliated to the Group primarily manufactures multiple-purpose pincers, baking kits, knives, scissors, kitchenware, gardening tools and beauty care kits as well as other hardware tools, the annual production value of which reaches US$ 30 million dollars.

集团所属工厂主要生产多用钳、烤具、刀具、剪刀、厨具、花园工具、美容套等五金产品,年生产总值3000万美元,产品价廉物美、选料上乘、质量保证,深受国内外客户的青睐

The eˉtiology of hemospermia is complicate,but almost of hemospermia are benign.

血精的原因很,以良性病变为主。