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In this paper, the adjointness of the product of two differential operators generated by a third order normal and singular symmetric differential expression in the limit-circle case is discussed. The necessary and sufficient conditions which make the product operators being the adjoint operators obtained by the matrix analysis and calculation. At the same time, the adjointness of the product of the power and adjointness operator obtained.

本文首先讨论了正则和奇异两种情况下两个极限圆型三阶对称微分算式生成的微分算子的乘积的自共轭性，运用矩阵分析和计算，得到了乘积算子为自共轭算子时边界应满足的充分必要条件，同时得到了幂算子的自共轭性、自共轭算子乘积的自共轭性等乘积算子的其它若干性质。

The rate of c-kit+ cells in the heart increased gradually from E10 with the highest level of 12.6±3.2% at E11, which was nearly similar to the fetal liver, except for E12 when the c-kit+ cells was 3.4±1.2% in the heart compared to the fetal liver with 11.6±4.1% c-kit+ cells. The rate of c-kit cells in the suspension cells from the heart at E11 maintained stable after 24h culture based in the stromal cells of the heart and AGM region with the same conceptus age, but the rate of c-kit cells obviously decreased in the condition of the stromal cells from the fetal liver. The c-kit cells of the three conditions were all at low level at 48h without significant difference.

通过流式检测c-kit+细胞我们发现，胚胎期心脏和胎肝c-kit+细胞比率几乎一致，E11时c-kit+细胞明显增多，分别高达(12.6±3.2)%和(9.6±2.8)%，但E12时心脏中c-kit+细胞明显减少，仅为(3.4±1.2)%，此时胎肝中c-kit+细胞为(11.6±4.1)%。E11的悬浮细胞与心脏内皮细胞和AGM区基质共培养24h时，c-kit+细胞数量保持稳定，但在胎肝基质细胞中c-kit+细胞数量明显减少，在共培养48h，三组中的c-kit+细胞均呈较低水平，组间没有显著性差异。

A class of conjugate descent algorithm with single parameter βk for unconstrained minimization problems is presented and it is proved that this algorithm is of descent feature when it satisfies the condi- tion of a sort of inexact linear searching and, in addition, it is globally convergent.

给出了无约束问题一族含有一个参数βk的共扼下降算法，证明了该共扼下降算法在满足一种非精确线性搜索条件时是下降的，而且是全局收敛的。同时可以看到共扼下降算法是其特例

The blend has following properties with 10 parts compatibilizer. The tensile intensity and elongation at break reach 35.66MPa and 23.58%, respectively, improving by 26.6% and 65.7% respectively compared with 0 part compatibilizer; The characteristic absorption peak of carbonyl at 1725～1800cm-1 disappear and the characteristic absorption peak of hydroxide at 3438～3440cm-1 increase induce the formation of hydrogen bond; The decalescence peak of blend increase by 2℃compared with the blend containing 0 part compatibilizer near 100℃; Lignin can be dispersed homogeneously to avoid reuniting of lignin particle.

2当共混材料中增容剂含量为10份时，共混材料表现出如下特性：拉伸强度和断裂伸长率分别达到35.66MPa及23.58%，较未加增容剂分别提高了26.6%和65.7%；从1725～1800cm-1范围内羰基特征吸收峰接近消失以及3438～3440cm-1范围内的羟基波数的增加暗示了共混材料中氢键缔合的发生；共混物在100℃附近的吸热峰较未加增容剂时降低了近2℃，相容性得到了提高；木质素在基体中进一步分散，结晶度增加，从而阻止木质素的团聚，增加了两相的相容性。

First of all, this study will be multi-walled carbon nanotubes by chemical oxidation process purified so it can be modified to deal with than the purification of purity before the modified 5 wt%, more than 1.89 times the surface area to increase the surface potential decrease of about 10 ~ 20 mV and the surface functional base (-COOH and-OH) to increase 1.45 times, and then the control technology of electroless preparation parameters include: analysis of plating time, plating analysis of temperature, metal ions in solution than the (Fe2+/ Ni2+), bath pH and the added value of dispersion Agent and other research towards Fe-Ni particles to increase the iron content and Fe-Ni particles spread in the MWCNT upper fixed targets,the results found that when the parameters for the preparation of 50 ℃, pH10, do not add dispersant, metal ions than the solution (Fe2 +/ Ni2 +) 7, the highest iron content can be Fe = 40.55 at%(flat iron content 111.17 mg / g) of nanocomposites Fe-Ni/CNT, then for a series of the nature of its analysis, the final evaluation Fe-Ni/CNT nanocomposites were processed on the effectiveness of the application of mixed pollutants, the results showed that in 120 minutes at the same time when Adsorption of heavy metal ions lead nitrate 10 ppm, selenium heavy metal ion degradation of 1 ppm and orange azo dye AO7 50 ppm standard of effluents, and after a total Fe-Ni nano-particles to SEM / EDS analysis of more than 50% still remaining.

本研究首先将多壁奈米碳管以化学氧化法做纯化改质处理能使其纯度较纯化改质前提高5 wt％、比表面积提高1.89倍、表面电位下降约10~20 mV以及表面官能基提高1.45倍，再控制无电镀技术之制备参数包括：析镀时间、析镀温度，镀液中金属离子比(Fe2+/Ni2+)、镀液pH值及是否添加分散剂等，研究朝提高Fe-Ni粒子的含铁量与Fe-Ni粒子散布固定在MWCNT上等目标进行，研究结果发现当制备参数为50 ℃、pH10、不添加分散剂、镀液金属离子比(Fe2+/Ni2+)7时，可得到最高铁含量Fe = 40.55 at％(单位铁含量111.17 mg/g)之奈米复合材料Fe-Ni/CNT，接著对其作一系列性质分析，最后评估奈米复合材料Fe-Ni/CNT对共处理混合污染物之应用效益，结果显示其在120分钟时能够同时吸附重金属硝酸铅离子10 ppm、重金属硒酸根离子1 ppm及降解偶氮橘色染料AO7 50 ppm达放流水标准，且共处理后奈米Fe-Ni粒子以SEM/EDS分析仍剩余50 %以上。

Mechanisms of heat affected zone liquation and liquation cracking in GH150 alloy were investigated by using varestraint test and hot ductility test in conjunction with the differential thermal analysis and optical, scanning electron microsopy. On heating,γ/C liquation take places in the HAZ above 1250℃. When the temperature reaches 1353- 1375℃, a large amount of liquid particles due to initial melting can be observed within the grains near the fusion boundary. On cooling,γ/C eutectic and γ/ Laves phase eutectic take place at 1273 and 1200℃ respectively.

采用可变拘束试验、热塑性试验、差热分析、光镜与扫描电镜观察，研究了GH150合金焊接热影响区液化及液化裂纹形成机制加热过程中温度高于1250℃的热影响区由于γ／C共晶产生液化，在温度达到1353℃（固相约至1375℃的近维区，晶内出现大量液化点冷却过程中温度在1273和1200℃时形成γ／C共晶和γ／Laves相共晶。

When PEN and PET were melt blended, however, transesterification between two homopolymers would take place and the resultant product may be not crystallizable.

PET／PEN共混物在熔融共混时可能会发生酯交换反应，生成嵌段共聚物或无规共聚物，从而对PET／PEN共混物的结晶性能和热性能产生不利的影响。

Deriving conjugated linoleic acid under different condition often leads to incompletability and isomerization.It also affects the accuracy of analysis.

对共轭亚油酸进行三氟化硼-甲醇衍生化时，采用不同条件处理共轭亚油酸，常常导致共轭亚油酸的不完全和异构化，从而影响到分析的准确度。

In all experimented cooling conditions the alloy with the addition of 0.15% Mg possesses the coarsest eutectic structure,while the alloy with the 0.3% Mg addition the finest structure in eutectics.

在试验范围内，Al-Si11.0合金中加入0.15%镁时，共晶组织变得较粗；而当镁的加入量增加到0.3%时，其共晶组织比Al-Si11.0合金细得多，分析了出现这一结果的原因。

For frequency information fluid identification technology:the basic theory of fluid identification based on frequency information has been introduced,for inner and external factor affecting frequency,some steps have been proposed to attain reserved amplitude and frequency analysis data with high resolution,high S/N ratio;through the comparison of time-frequency analysis method, the high accuracy time-frequency analysis method has been selected to extract time-frequency attributes;the analysis method flow of common single frequency fluid identification has been proposed,according to the data of full frequency band,several anomaly zone modes of common single frequency attribute have segregated; incorporating converted wave and compression wave,fluid identification method based on PS wave combined time-frequency analysis has been proposed;the AVO property of various fluid type in frequency domain has been studied;the generalized fourier analysis method,Proni absorption filter has been introduced,and researched for anti-noise and for the seismic processing interpretation flow.The above technology have been applied to fluid identification of organic reef in WBT area in the east of Sichuan and fluid identification of clastic rock in GUANGAN area in the middle of Sichuan,the results show that the above methods are effective.

基于频率信息的流体识别技术方面：介绍了利用频率信息流体识别的基本理论，针对影响频率的内、外在因素，提出一些针对措施，以获得高分辨率、高信噪比的保幅、保频分析数据；通过时频分析方法的比较，选取高精度的时频分析方法提取时频属性；提出共单频属性进行流体识别的分析方法流程，结合全频带数据，分出几种共单频属性异常带模式；联合转换波资料和纵波资料，提出基于纵横波联合时频分析进行流体识别方法；研究了频率域内不同流体类型AVO现象；引进一种广义傅立叶分析方法：Proni吸收滤波，研究其抗噪性以及进行地震处理解释的流程；将这些技术应用川东北五百梯区块进行生物礁储层流体的识别和川中广安陆相碎屑岩的流体识别，取得较好的效果。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。