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With the addition of hexamethylenetetramine, an ambient pressure drying technique was developed for the fabrication of resorcinol-formaldehyde-based carbon aerogels.

以间苯二酚和甲醛为反应物、六次甲基四胺HMTA为催化剂、去离子水为溶剂,所合成的间苯二酚-甲醛凝胶能够在常压条件下直接进行干燥得到有机气凝胶;并经炭化,得到炭气凝胶。

Water,decyloleate,propylene glycol,stearic acid,glyceryl stearate,peg-100 stearate,iris germanica(orris extract/cells),chamomilla recutita,arctium majus,prunus dulcis,ceteareth-3, Triethanolamine,phenoxyethanol,methylparaben,imidazolidinyl urea,carbomer,c12-13 alkyl lactate,disodium edta,propylparaben,glyceryl hydroxystearate,cetyl esters,ethylparaben,pentadecalactone,cera microcristallina,trihydroxystearin,butylparaben,hydroxystearic acid,isobutylparaben,chlorhexidine digluconate,tetradecyloctadecanoic acid,tetradecyleicosanoic acid,tocopherol,lecithin,ascorbyl palmitate,glyceryl oleate,citric acid

水,油酸癸酯,丙二醇,硬脂酸,甘油硬脂酸,聚乙二醇硬脂酸酯,鸢尾花提取物/活细胞,洋甘菊萃取,牛蒡提取物,甜杏仁油,鲸蜡硬脂醇醚,三乙醇胺,苯氧乙醇,羟苯甲酯,尿素醛,卡波姆,c12-13烷醇乳酸酯,乙酸乙二胺二钠,羟苯丙酯,甘油羟基硬脂酸酯,十六烷基酯,羟苯乙酯,环十五内酯,微晶蜡,三羟基硬脂精,羟苯丁酯,羟基硬脂酸,对羟基苯甲酸异丁酯,洗必泰葡萄糖酸盐,十四烷基十八烷酸,十四烷基二十烷酸,维生素E ,卵磷脂,抗坏血酸棕榈酸酯,甘油硬脂酸,柠檬酸水:几乎所有护肤品成分第一位都是水。油酸癸酯:滋润、柔肤剂,并常添加于多种化妆品中作为溶剂

In addition, the stability of ternary Cu 〓complexes polypyridyl=1, 10-phenanthroline (Phen , pyrido [3, 2-f] [1, 7] phenanthroline , 1, 4, 8, 9-tetraazatriphenylene , dipyrido [3, 2-a: 2'3'-c] phenazine , imidazo phenanthroline and 2-phenylimidazo phenanthroline , NTP=ATP and UTP was studied by potentiometric pH titration in water at temperature 15℃, 25℃ and 35℃, and in 30% and 50% aqueous dioxane solution at 25℃.

另外,用pH电位滴定法研究了多吡啶芳香配体polypyridyl配合物Cu〓(PL=1,10-邻菲咯啉、吡啶并[3,2-f][1,7]邻菲咯啉、1,4,8,9-四氮三联苯、二吡啶并[3,2-a∶2'3'-c]吩嗪和2-苯基咪唑并邻菲咯啉或咪唑并邻菲咯啉)在不同温度(15℃、25℃和35℃)水溶液及30%和50%二氧六环-水混和溶剂(25℃)中的稳定性。

Six calix[4]recorcinarenes are synthesized by the reaction of resorcin as substrates with six aromatic aldehydes, respectively.

以间苯二酚为反应底物,分别与六种芳香醛合成了相应的杯[4]间苯二酚芳烃,并通过红外光谱和氢核磁共振谱对这些化合物进行了表征。

The main pollutants from this chemical plant is perchloroethane, pentachloroethane, hexachlorobutadiene and HCB, and such pollutants are present in the soil with high densities, some as high as 1%- 95%, of which the perchloroethane is near the purity of the corresponding product, and especially this part of the soil contains comparatively high-density persistent organic pollutant HCB, which makes it suitable to be disposed of together with other soils. Therefore it is suggest that this part of soil should be separately dug out and transported outside of the site.

化工厂的主要污染物质是六氯乙烷、五氯乙烷、六氯丁二烯和六氯苯,土壤中上述污染物的浓度非常高,有些达到1%至95%,其中六氯乙烷接近相应的产品的纯度,特别是这一部分含有较高浓度的持久性有机污染物六氯苯,不利于与其它土壤混合处理,建议将这一部分单独开挖出来并运出场外。

Four series and sixteen solid complexes of rare earth chloride with 1-naphthoic acid (L_1),benzoic acid (L_2),phenylacetic acid (L_3) and Mandelic acid (L_4) have been synthesized by method of solid state reaction at low temperature,and then these complexes were characterized by chemical analysis methods.

本文采用低温固相合成法,以稀土氯化物、1—萘甲酸(HL_1)、苯甲酸(HL_2)、苯乙酸(HL_3)、苯羟乙酸(HL_4)为原料,以六次甲基四胺为质子受体,合成并表征了四个系列十六种固态配合物。

Phenylenediamines, aminophenols, methoxyanil ines, and 1,4- hydroquinone, 1-naphthylamine were polymerized via the catalysis of horseradish peroxidase in mixed solvents of l,4-dioxane and water at amibient conditions by using hydrogen peroxide as the oxidant. Several factors influencing the polymer yield, such as the concentration of the substrate, pH value and oxidant amount were examined using a- phenylenediamine as substrate.

本文选择了苯二胺、氨基苯酚、甲氧基苯胺三个系列,以及对苯二酚、1-萘胺等单体,在二氧六环-水混合介质中以辣根过氧化物酶为催化剂,以双氧水为氧化剂进行了不同底物的室温酶促聚合,并以邻苯二胺为底物考察了溶剂用量、pH值、作为氧化剂的双氧水用量等条件对聚合物收率的影响。

The mechanism of co-fluorescence effect has been discussed. In chapter six, the new fluorescence enhancement phenomenon was observed by adding some crown ethers to samarium-thenoyltrifluoroacetone system.

在第六章中,研究发现当向钐-噻吩甲酰三氟丙酮中加入配位能力很强的大环配体冠醚时,冠醚对稀土有机配合物体系产生显著的荧光增强作用,其中冠醚二苯并18冠6后(DB18C6)可使钐-TTA二元配合物体系荧光强度增强280倍。

In the course of our study the chemistry of arenes contaning allylic acetates moiety under the catalysis of palladium, we found an efficient synthesis of benzocycles via intramolecular Friedel-Crafts reaction of halogen free 6-acetoxy-4alkenyl arens.

我们在设计钯催化的碳—氢键活化时,发现了含有烯丙基醋酸酯侧链的芳烃的三氟醋酸促进的分子内的Friedel-Crafts反应,从而为有效合成苯并六元环结构提供了一个方便的方法。

This kind of gratings can be kept in the material for a long time. A mode of molecular reorientation was used to explain the formation mechanism of these gratings and it is well consistent with our experimental results. 3. Three kinds of azobenzene polymers P , P (MMA-co-GY7) and P (MMA-co-GO13) were synthesized by radical polymerization. High-density optical storage and the three-dimension (3D) microstructures in the azobenzene polymer films were presented. Twenty gratings have been stored on the same spot in our material. It is twice as many as the best recording that has been reported. It is the first time, a rectangular microstructure and a complicated double layers nesting six-pointed star microstructure are inscribed in it by using a simple two-wave couple setup.

采用共聚反应设计合成了单偶氮苯聚合物P、双偶氮苯聚合物P(MMA-co-GY7)和P(MMA-co-GO13)三种聚合物,研究了偶氮苯聚合物薄膜中的高密度光学存储和3维微结构,成功的将20套光栅储存在样品中同一个点上,是已有报道的两倍;并首次用简单的2波混频光路在该材料中刻写出长方格子和六角星型的微结构,在制作多重不同周期不同角度的高密度光栅结构实验过程中,发现不同周期光栅的刻写顺序对整个微结构形成的最终结果具有决定性的影响,并用相衬显微镜观察了这些微结构图像。

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