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六亚甲基四胺

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Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用"一勺烩"方法,以4-羟基苯甲腈为起始原料,首先与硫氢化钠和无水氯化镁在N,N-二甲基甲酰胺中反应,所得中间体不经分离,直接加入2-氯乙酰乙酸乙酯进行环合反应,得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(2);然后通过六亚甲基四胺/三氟乙酸进行Duff反应,得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(3);再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

Nanosized titania particles consisting of anatase, rutile and brookite phases were synthesized under solvothermal conditions with different alcohols as solvents, hexamethylene tetramine as precipitant as well as precursor of titanium trichloride.

采用不同的醇溶剂,以六亚甲基四胺为沉淀剂,以TiCl3为前驱体,通过溶剂热的方法控制合成出纳米级的锐钛矿型、金红石型和板钛矿型的二氧化钛。

Determination of hexamethylenetetramine content.

六亚甲基四胺含量的测定。

CeO2 nanoparticles were prepared using cerium nitrate and hexamethylenetetramine as starting materials, and the prepared powders were collocated into polishing slurry for chemical mechanical polishing of GaAs wafer.

以硝酸铈和六亚甲基四胺为原料制备出不同粒径的纳米CeO2粉体颗粒,将纳米CeO2粉体配制成抛光液并用于砷化镓晶片的化学机械抛光。

Fumed-silica surfaces were modified with resorcinol and hexamethylenetetramine complex, and NR/M-silica nanocomposites were prepared in mixing and curing process. Structure and properties of NR/M-silica nanocomposites were investigated by mechanical testing ,cross-linking density determination, transmission electron microscopy, differential scanning calorimetry, fourier transform infrared spectroscopy and X-ray photoelectron spectroscopy. The results showed that M-silica have obvious reinforcement effect on NR vulcanizate.

用间苯二酚与六亚甲基四胺络合物对气相法白炭黑进行表面改性,通过混炼和硫化制备了天然橡胶/改性气相法白炭黑(NR/M-silica)纳米复合材料,并通过力学性能测试、交联密度测定、透射电镜、差示扫描量热法、红外光谱和X射线光电子能谱等手段研究了纳米复合材料的结构和性能。

By using water bath method that an aqueous solution of zinc nitrate(Zn(NO3)2·6H2O)reacted with an aqueous solution of equimolar methenamine(C6H12N4),ZnO nanomaterials with controllable morphologies are successfully prepared. The influences of solution concentration and substrates on morphology of ZnO nanomaterials are discussed.

用硝酸锌(Zn(NO3)2·6H2O)与六亚甲基四胺(C6H12N4)以等浓度配制成反应溶液,通过水浴法制备出了形貌可控的棒状ZnO纳米结构,讨论了不同反应浓度及衬底对ZnO表面形貌的影响。

Pneumocystis carinii cysts were observed in the lung print smear after staining with gormori methenamine silver,and pathological changes in the lung section were observed after staining with hematoxylin-eosin.

3肺组织印片六亚甲基四胺银染色观察卡氏肺孢子虫(Pneumocystis carinii,Pc)包囊,肺组织切片苏木素-伊红(hematoxylin-eosin,HE)染色观察其病理变化。

When 45% methanol solution containing 0.5 mmol/L hexamethylene tetraamine was used as the pump carrier, the pump flow rate and output pressure achieved 0.58 mL/min and 0.79 MPa at 4950 V, respectively. By using the pump carrier as the mobile phase, benzene and naphthanlene were separated on baseline by the EFA system.

在4950 V的外加电压下,以含0.5 mmol/L六亚甲基四胺的45%甲醇溶液为泵载流,电渗泵的流量和输出压强分别为0.58 mL/min和0.79 MPa,以泵载流为流动相,该系统对苯和萘进行了反相色谱分离。

Methods 4-Hydroxy- benzonitrile was treated with sodium hydrogen sulfide and anhydrous magnesium chloride in dimethyl formamide to give thioamide, which was then directly cyclized with ethyl 2-chloroacetoacetate without separation to give ethyl 2-(4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(2) in one-pot; then 2 was formylated with Duff reaction adopting hexamethylenetetramine in trifluoroacetic acid to give ethyl 2-(3-formyl-4-hydroxyphenyl)-4-methylthiazole-5-carboxylate(3); finally, the target compound was obtained by the treatment of 3 with hydroxylamine hydrochloride and sodium formate in formic acid.

采用&一勺烩&方法,以4-羟基苯甲腈为起始原料,首先与硫氢化钠和无水氯化镁在N,N-二甲基甲酰胺中反应,所得中间体不经分离,直接加入2-氯乙酰乙酸乙酯进行环合反应,得到2-(4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(2);然后通过六亚甲基四胺/三氟乙酸进行Duff反应,得到2-(3-甲酰基-4-羟基)苯基-4-甲基-5-噻唑甲酸乙酯(3);再经盐酸羟胺/甲酸/甲酸钠体系脱水得到目标化合物。

First use soap-free emulsion preparation for polystyrene spheres, and the kernel, Reuse are silicon acetic tetraethyl ortho-silicate in ammonia catalytic hydrolysis, formed under the condition of silica, charged by six water or their cerium, six of methylene amine solution HMT (4) into the negatively charged, uniform cerium oxide coated surfaces to PS microspheres, core-shell structure of PS - CeO2 and PS - SiO2 composite microspheres.

首先用无皂乳液制备了聚苯乙烯微球,并以此为内核;再利用正硅乙酸乙酯在氨水催化条件下水解,形成带负电性的二氧化硅,或者利用六水亚硝酸铈、六亚甲基四胺水溶液分解出带负电性的氧化铈,均匀的包覆到PS微球表面,形成核-壳结构的PS-CeO2和PS-SiO2复合微球。

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