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Then the surface of the star polymer was intramolecularly crosslinked using octa(3-azidopropyl)polyhedral oligomeric silsesquioxane, POSS-(N_3)_8,as the inorganic multifunctional crosslinker at high dilution concentration via click chemistry,forming a novel POSS/polymer hybrid nanostructure.Thermogravimetric analysis shows that after surface crosslinking, the thermostability of the core crosslinked PS can be remarkably improved.In the second work,we synthesized of a novel polymer with quatrefoil-shaped topology.

接着,我们合成了一种结构规整的含八个叠氮功能团的无机分子—多面低聚倍半硅氧烷,以其为交联剂,我们通过Click反应在即稀浓度下实现了前驱体星型聚合物的分子内表面交联,得到了外层为无机分子交联,内层为有机高分子的星状高分子,这种新型的星状聚合物表现出了优良的热稳定性能。

Unfortunately, although the real estate industry is seen as a large number of gathered wealth industry, but in the State Administration of Taxation recently released "2003 China top tax hundred", the did not have a real estate Enterprise finalists, even the real estate industry in Shenzhen Overseas Chinese Town real estate tax scholar Limited, tax amount is only 199 million yuan, with the National in the last one hundred (873,230,000 yuan) there are still several times the gap.

不幸的是,虽然房地产行业被认为是大量的聚集财富的行业,但在国家税务总局最近公布的& 2003年中国最高税率100 &的项目,没有一家房地产企业入围,即使房地产业华侨城房地产税学者有限公司,纳税额只有199万元,与全国在过去的100 (八万七千三百二十三点〇〇万元)还有几倍的差距。

Japan's whaling ships returned to port in April from the Antarctic with 863 whales, nearly double the number of whales killed last year.

今年四月,日本捕鲸船从南极地区回到港口时,运载有八百六十三条鲸鱼,此数量几乎是去年被杀鲸鱼数目的两倍。

Employing high-dilute method and 5-fold excess amine prepared two new "two-armed" acyclic diamine intermediates I_a and I_b, which are also intermediates of synthesizing microcyclic compounds, and eight aromatic Schiff bases, II_, were synthesized from reaction of I_a or I_b condensing with different aromatic aldehydes. Their composition and structure were characterized by Elemental analysis, IR, UV-Vis, LIF,~1HNMR and MS. The hydrogen bond interactions and MS fragmental patterns were also discussed.3. Several novel transition metal complexes using II_a as ligand were synthesized and identified by Elemental analysis, IR, UV-Vis,~1HNMR and molar conductivity.

1,采用高度稀释及胺过量五倍的方法合成了两个具有吡啶双酰胺臂的非环二胺Ⅰ_a和Ⅰ_b,并以它们为中间体进一步合成了八个芳香席夫碱Ⅱ_a-Ⅱ_h,通过元素分析及各种波谱测试鉴定了它们的组成与结构,对化合物的UV-Vis、LIF、IR、~1HNMR及MS进行了较为详细的讨论,还探讨了席夫碱的氢键相互作用及质谱裂解方式; 2,以席夫碱Ⅱ_a为配体合成了几个新型的过渡金属配合物,并通过元素分析、UV-Vis、IR、~1HNMR、摩尔电导及DTA—TG对其进行了表征,讨论了化合物的配位情况及配体在配位中的脱质子行为。

Carving gravure of business card printing and membership card making production and offset business card printing and membership card making, and so on are very different, first of all the manuscripts submitted to approx 10 times, the perimeter line by hand is decisived on top of a piece of zinc tablet with a smaller machine to get an outside line back into the original large carved in a piece about an inch of eight brass, and copper strip it is some anticorrosive toppedwith films, because of copper strip is triggered from the perimeter line, so the rough body by hand for the film, when removed, and then use the medicine to the erosion of deep water, and proto-end knife with a magnifying glass and, thetolerant to the edge, sharp corners repaired, such as location on a layer of chrome, it's a printing plate.

雕刻凹版的制卡和会员卡制作制作与柯式制卡和会员卡制作等有很大的分别,首先把来稿放大约十倍,把外围线用手工刻划在一块锌片之上,再用一部缩细机械把外线缩回原大刻在一块约八份一寸的铜片上,而这件铜片上是涂有一些防腐蚀薄膜的,因为铜片只是勾上字的外围线,所以要用手工将粗身地上的薄膜刮去,然后用药水将印纹蚀深,最后仍要用放大镜及雕刻刀,耐性地将线边、尖角等位置修好,再镀上一层铬,这印版便大功告成。

Recent three months, the listing may be approved by the peatlands Yangchanfang number is nearly double the previous eight months, the industry is expected to reach 25% of the incremental pace.

最近三个月来,被审批通过可上市的央产房数量是前八个月放量的近一倍,业内预计其月递增速度将达到25%。

The orange bailey bridge of No.86 expressway becomes a wonderful nature scene on the south grassland of Ten Drum Culture Village. The soaring old chimney and the spanning orange bridge afar interact to symbolize the spirit of Ten Drum-「十」. In the embrace of the large grassland with the old chimney and orange bridge in the night, it will be a natural stage for artists to perform heartily. Visitors from everywhere also leave unforgettable exclamation points for this attractive art performance with the culture-rich land.

号快速道路的橙色倍力桥,成为了十鼓村南端大草原上澄桥的绝佳自然布景,笔直耸立的台糖老烟囱,和横跨在远方的澄桥,两两相呼应著,一直一横的造型,恰巧是十鼓的精神象徵,在这片大草原的促拥下,夜晚的老烟囱加上澄桥,将是艺术家们,尽情演出的天然舞台,而八方游客们,也将为这场动人的艺术演出,与这块富含文化迹痕的土地,留下难忘的惊叹号。

After stints at Rijeka and Livorno, the lad knows this is his big chance to show what he's worth and confirm the good impression he gave in the last two years in Italy and when playing for his national team, after the doubly unlucky experience at Euro 2008 (the injury for him and Croatia being knocked out in such a dramatic fashion by Turkey).

在里耶卡和利沃诺踢球后,这名青年知道这是展示他的价值的最大良机,他要一如既往地表现出过去两个赛季在意大利给人的印象以及他的国家队比赛的神勇,在2008欧锦赛经历了双倍打击后(受伤令他没法代表克罗地亚出战,而他的国家也在八强输给土耳其)。

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As she looked at Warrington's manly face, and dark, melancholy eyes, she had settled in her mind that he must have been the victim of an unhappy attachment.

每逢看到沃林顿那刚毅的脸,那乌黑、忧郁的眼睛,她便会相信,他一定作过不幸的爱情的受害者。

Maybe they'll disappear into a pothole.

也许他们将在壶穴里消失

But because of its youthful corporate culture—most people are hustled out of the door in their mid-40s—it had no one to send.

但是因为该公司年轻的企业文化——大多数员工在40来岁的时候都被请出公司——一时间没有好的人选。