光谱分析法

The polarization fatigue mechanism and the effect of donor doping Bi〓 on ferroelectric properties of PZT thin films are also revealed. The system of zirconium oxynitrate—tetrabutyl titanate—lead acetate anhydrate—ethylene glycol is adopted to prepare stable PZT sol.

本文采用X射线衍射分析、X射线光电子谱分析、透射电镜、原子力显微镜、扫描电镜、红外光谱分析以及铁电性能测试等研究了溶胶-凝胶法制备PZT铁电薄膜的成胶机理及PZT铁电薄膜的微结构、界面结构及铁电性能，并考察了施主掺杂Bi〓对薄膜铁电性能的影响规律，提出了铁电极化疲劳机制。

Three flavonoids compounds: kaempferol *!, quercetin *, and isoquercitrin *# were isolated from the leaves of Cyclocarya paliurus Batal.

采用溶剂萃取及多种色谱技术分离纯化，根据理化性质和光谱分析方法鉴定其结构，确定从青钱柳中分离得到山柰酚、槲皮素和异槲皮苷 3个黄酮单体化合物，并用反相高效液相色谱法对其含量进行了测定，测得各自在甲醇和水提取物中的含量：山柰酚 0 。

The spectrum and electrochemical adsorption behavior and mechanism of diethyl dithiocarbamate on jamesonite were investigated by spectrum analysis and constantpotential step.

采用光谱分析及恒电位阶跃法，研究了乙硫氮在脆硫锑铅矿表面吸附的光谱电化学行为及作用机理。

The electrochemical adsorption behavior and mechanism of diethyl dithiocarbamate on the surface of marmatite, which are different from the mixed potential model of flotation electrochemistry, were studied by spectrum analysis, CA voltammetry and constant potential step.

采用光谱分析、循环伏安及恒电位阶跃法，研究了乙硫氮在铁闪锌矿表面吸附的电化学行为及机理，该机理与浮选电化学的混合电位模型并不一致。

The electrochemical adsorption behavior and mechanism of diethyl dithiocarbamate on the surface of marmatite, which are different from the mixed potential model of flotation electrochemistry, were studied by spectrum analysis, CA voltammetry and constant potential step.

摘 要：采用光谱分析、循环伏安及恒电位阶跃法，研究了乙硫氮在铁闪锌矿表面吸附的电化学行为及机理，该机理与浮选电化学的混合电位模型并不一致。

Under acidic condition, the dimer diethyldithiocarbamate （D2） is formed on marmatite through the electrochemical adsorption of diethyl dithiocarbamate at 0 - 200 mV.

采用光谱分析、循环伏安及恒电位阶跃法，研究了乙硫氮在铁闪锌矿表面吸附的电化学行为及机理，该机理与浮选电化学的混合电位模型并不一致。

The glass and crystalline glass-solders of Li2O-ZnO-SiO2 system were prepared by conventional melt technology. The various factors effecting on glass ceramics and glass were investigated,which include glass chemical composition and heat-treatment and so on. And then by means of XRD, DTA, IR and SEM, the structure and properties of the glass and glass-ceramic were studied. The coefficient of linear expansion , transform temperature and soft temperature wer measured. And then the factors that effect the mechanical strength of glass-ceramic were discussed and the fluxion property was determined and the crystallization course and mechanism were discussed, which can provide certain therial reference value for practice producing and glass seals to glass, ceramics and metal.

用高温熔融法制备了Li_2O-ZnO-SiO_2系统玻璃及其结晶型玻璃焊料，探讨了各种因素(包括玻璃组成、热处理制度等)对微晶玻璃的结构和性能的影响；利用X射线衍射分析、DTA、红外光谱分析以及扫描电镜等现代测试手段，对玻璃的结构与性能进行研究，测定了玻璃及微晶玻璃的线膨胀系数、转变温度和软化温度，同时对影响微晶玻璃的强度的因素进行了探讨，并对该体系玻璃的流散性进行了测定，对它的析晶过程和析晶机理进行探讨，为实际生产和与玻璃、陶瓷及金属封接提供了一定的理论参考价值。

Various test conditions and effect factors for determination of mercury by flow injection-atomic absorption spectrometry were discussed and a method for the determination of mercury in Tricholoma giganteum has been developed.

探讨了流动注射还原气化—冷原子吸收光谱法测定微量汞时的最佳条件，建立了大白口蘑中痕量汞的流动注射还原气化—冷原子吸收光谱分析方法。

Firstly, by using DSC, we analyzed the effect of the type and content of initiators on the curing reaction, Then, through FTIR, we discussed the final degree of cure of the cured resin and the performance of the cured resin by testing the static mechanical performance and DMTA, found that moderate content and ratio of the initiators system can cause the moderate cure temperature, increase of exotherm and the final degree of cure result from the cooperation effect of the two kinds of initiators, and found that the cooperated initiators system can effectively increase the final degree of cure even in low content.

通过差示扫描量热法分析了不同固化剂体系对树脂固化行为的影响，用红外光谱分析了不同固化剂体系下的浇铸体的固化度，并对树脂浇注体静态力学性能及动态机械热分析，认为不同活性的固化剂联用存在协同效应，使固化反应温度适中，固化反应更加充分，提高树脂固化度和扩大聚合物网络，使树脂浇注体拥有良好的力学性能和耐热性。

Firstly, the different effect of rectorite modification for the mechanical property of E-51 system were compared; the effect of organic clay for the viscosity and Gel-time of pure E-51 epoxy resin were checked separately; the influence of organic clay for hardening process was studied with FTIR technology; And, the infection of organic rectorite content in matrix for the mechanical property thermal-wet tolerance property aging resistance property and medium endure property for the both of two system were studied relatively. The effect of organization for the inter-layer distance of clay was denoted by XRD technology; To probe into the thermodynamics status about reaction, we investigated the heat discharging of reaction system in the help of DSC. The impact and crooking of solidifying system was observed with the SEM to investigate the decentralization of organic clay, and, at the base of this ,we discuss the mechanism of clay toughing-buildup polymer matrix.

分别考察了有机粘土对树脂体系粘度和凝胶特性的影响，利用红外光谱分析技术研究了有机粘土的加入对体系固化工艺的影响；分别考察了有机粘土含量对二体系的力学性能、耐湿热性能、耐老化性能以及耐介质性能等的影响；采用X-衍射实验表征复合材料中有机粘土层间距的变化；用视差扫描量热法考察了体系的放热情况，以探讨反应的有关热力学状况；通过扫描电子显微分析技术对浇注体的弯曲、冲击断口进行观察分析，以考察、表征有机粘土的分散情况，并在此基础上探讨了有机粘土改性环氧树脂的机理。

With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务，乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐，因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。