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光谱分析法

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The effect of acid, base and salt on the thermal stability of chlorinated natural rubber made from latex was analyzed by using chemical analysis, thermal aging experiments with UV spectroscopy analysis and thermal analysis.

采用热老化实验结合紫外光谱分析和热分析,分析了酸、碱及盐对胶乳法氯化天然橡胶热稳定性的影响,并讨论了酸、碱及盐对CNR热降解的影响机理。

The result of IR spectral analysis indicated that the categories of radicals found in cell walls after either ultrasonic method or cell autolysis are almost the same.

红外光谱分析结果表明,与Nocardia原菌相比,超声波法破碎和自溶法破碎后制得的Nocardia细胞壁所含有的基团类别基本相同。

The interfacial surface and properties of glass fiber reinforced PET was studied by using Fouier transform infrared spectrometer scaning electron microscopy, dynamic viscoelastometer differential scattering calorimetry and mechanical measuring methods, the effects of coupling agent on the property of PET and its interfacial adhesion were examined.

用红外光谱分析、扫描电镜、粘弹谱仪、差示扫描量热法及力学性能测试方法,考察了玻璃纤维增强聚对苯二甲酸乙二醇酯的界面情况及力学性能等,并分析了玻璃纤维表面处理剂对PET树脂及其界面粘结性的影响。

Machinable bioactive glass-ceramics containing mica and fluorapatite were prepared by high-temperature melting. The glass-ceramics were analyzed by means of X-ray diffractometry, scanning electron microscopy with energy dispersive spectrometer and Fourier transform infrared reflection spectrometry. The bending strength, hardness and fracture toughness of the materials were measured.

摘 要:采用高温熔铸法制备可加工生物活性云母/氟磷灰石玻璃陶瓷;用X射线衍射、扫描电镜和傅里叶变换红外光谱分析等手段对材料的相组成和微观形貌进行研究,测定材料的抗弯强度、硬度和断裂韧性等力学性能;采用体外模拟体液浸泡法测试材料的生物活性。

Machinable bioactive glass-ceramics containing mica and fluorapatite were prepared byhigh-temperature melting. The glass-ceramics were analyzed by means of X-ray diffractometry, scanning electron microscopy with energy dispersive spectrometer and Fourier transform infrared reflection spectrometry. The bending strength, hardness and fracture toughness of the materials were measured.

摘 要:采用高温熔铸法制备可加工生物活性云母/氟磷灰石玻璃陶瓷;用X射线衍射、扫描电镜和傅里叶变换红外光谱分析等手段对材料的相组成和微观形貌进行研究,测定材料的抗弯强度、硬度和断裂韧性等力学性能;采用体外模拟体液浸泡法测试材料的生物活性。

The yield of SCP is 22.3%, and the extraction ratio of the ultrasonic method was 36.58% more than that of the traditional method. The structures of sc by ultrasonic extraction do not change judging from the analysis by FTIR. The extracts of SCP exhibit strong antioxidant activity on lard and gingili. The sc and Vc on lard and gingili have synergic antioxidative effect.

辽五味子多糖的提取率可达到22.30%,超声波法提取比传统法的提取率高出36.58%,通过红外光谱分析,超声波浸提没有使辽五味子多糖的结构发生改变;辽五味子多糖对油脂具有较强的抗氧化性能,抗坏血酸对辽五味子多糖具有协同抗氧化作用。

For compilation of baseline geochemical maps, a recently developed multifractal inverse distance weighted interpolation method and spectral analysis was applied, using a new geochemistry dedicated GIS software.

为了编辑基线地球化学图,利用一个新的地球化学专用的地理信息系统软件,新近开发了一个多重逆距离加权插值法并采用了光谱分析。

In this study, different nano-hydroxyapatite particles,HAP_1(25-60nm), HAP_4(the additives is heparin, 15-50nm), HAP_5(the additives is bovine serum albumin BSA, 20-80nm) were prepared by homogeneous precipitation and used heavy-gauge hydroxyapatite as comparison,we determined amount of heparin, sialic acid ,BSA adsorbed on HAP_1,HAP_2,HAP_3 by Crystal Violet assay, Bialsche method,Bradford method respectively and analyzed the binding mechanism by infrared spectrum;After taking HAP_1,HAP_2,HAP_4,HAP_5 and RBC to co-culture in vitro,we studied RBC hemolysis test and detected RBC hematolysis rate by erythrocyte osmotic fragility test;observing the changes of morphous and locomotion of cell after coacting HAP_1,HAP_2,HAP_4,HAP_5 and RBC by light microscope and inverted phase contrast microscope;observing HAP_1,HAP_2,HAP_4,HAP_5 effecting on Ultrastructure of RBC.

本文用均匀沉淀法制备了HAP_1(25-60nm),HAP_4(添加剂肝素,15-50nm),HAP_5(添加剂牛血清白蛋白BSA,20-80nm)等纳米粒子,并用大尺寸的羟基磷灰石HAP_2(470-520nm),HAP_3(1906nm)作对照,分别利用结晶紫法、Bialsche法、Bradford法研究了肝素、唾液酸、血清白蛋白在HAP_1,HAP_2,HAP_3上的吸附量,用红外光谱分析其中的结合机理;在体外将HAP_1,HAP_2,HAP4_,HAP_5与红细胞共培养,进行了红细胞溶血试验的研究,并借助红细胞渗透脆性试验检测红细胞溶血率;运用普通光学显微镜和倒置相差显微镜观察了HAP_1,HAP_2,HAP_4,HAP_5与红细胞作用后细胞形态及运动的变化:透射电镜观察了HAP_1,HAP_2,HAP_4,HAP_5对红细胞超微结构的影响。

In the present paper, the silver-intermediate in development process of PTG material-disilver phthalate (Ag2PA) was prepared by the liquid deposition method, and Ag2PHZ2PA·H2O complex was synthesized successfully by liquid dispersion means using Ag2PA and phthalazine as the reactants. The composition of Ag2PA and Ag2PHZ2PA·H2O was determined by ICP-AES and elemental analysis,...

采用液相沉淀法合成了PTG材料热显成像过程的含银中间体邻苯二甲酸二银(Ag2PA),并进一步使其与酞嗪络合形成了Ag2PHZ2PA.H2O配合物,通过元素分析、电感耦合等离子体原子发射光谱分析对Ag2PA与Ag2PHZ2PA.H2O配合物的元素组成进行了确定,采用X射线粉末衍射分析、傅里叶变换红外光谱分析以及热分析等方法对Ag2PA与Ag2PHZ2PA.H2O进行了表征,实现了对PTG材料热显成像过程含银中间体的定性分析。

And precipitation rate of vanadium was higher than 98.5%. Five vanadium catalysts were made withγ-Al_2O_3 and the mesoporous molecular sieve MCM-41 as carrier, and were made by dipping method, intermingle process and functionalizing method respectively. The characterization of their pore size, crystal structure, specific surface area and V_2O_5 load of catalysts were studied by XRD, the adsorption /desorption of N_2 technique, Raman spectroscopy and XRF. The activities of the catalysts estimated by the synthesis of DPC with DMC and phenol.

钒催化剂的制备与表征及活性评价:是分别以γ-Al_2O_3和介孔分子筛为载体,采用浸渍法,掺杂法及官能化法制备了5种钒催化剂;分别对其进行了XRD分析、N_2吸附-脱附分析、红外光谱分析和荧光分析,对其孔径、晶型结构、比表面积和V_2O_5负载量进行了表征;以碳酸二甲酯和苯酚的酯交换合成碳酸二苯酯的典型反应为依据,对钒催化剂进行了活性评价。

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With Death guitarist Schuldiner adopting vocal duties, the band made a major impact on the scene.

随着死亡的吉他手Schuldiner接受主唱的职务,乐队在现实中树立了重要的影响。

But he could still end up breakfasting on Swiss-government issue muesli because all six are accused of nicking around 45 million pounds they should have paid to FIFA.

不过他最后仍有可能沦为瑞士政府&议事餐桌&上的一道早餐,因为这所有六个人都被指控把本应支付给国际足联的大约4500万英镑骗了个精光。

Closes the eye, the deep breathing, all no longer are the dreams as if......

关闭眼睛,深呼吸,一切不再是梦想,犹如。。。。。。