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光谱分析

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Anion exchange resin was not suitable for the separation as stationary phase due to the strong adsorption toward catechol.The chemicals of eluates were measured by UV and IR.Terpene-catechol resin can be used for preparing copolymeric coating from terpene-catechol resin with raw lacquer.

通过对洗脱液进行紫外光谱分析,表明用中性氧化铝作固定相,分别用汽油、乙醇和NaOH-乙醇溶液洗脱,能较好地分离萜烯树脂和萜烯-邻苯二酚树脂。

With increasing of sulfonicgroup content,the decreasing extents of both 〓 and 〓are weakened.

硫含量分析和红外光谱分析的结果表明它们的磺酸基团含量的大小顺序为:SHA 5。

In the second chapter , it talks about the theory of gas testing , spectrum analysis of chemicals as well as its appliance in fire fighting . And it also introduces a new technique—LIBS.

第二章叙述气体检测、化学物品光谱分析的原理及在消防方面的应用,并引入激光感应频谱分析技术。

The paper introduces the application of infrared spectroscopy in the process of testing fire-retardant materials.

介绍了红外光谱法在表征阻燃材料与防火涂料结构及研究其阻燃性能方面的应用,讨论了红外光谱分析技术在材料阻燃分析中的应用前景。

A method of mixed gas component infrared spectrum recognition based on SVM regression model .

基于SVM的混合气体红外光谱分析关键技术研究。

In view of that spectrum quantitative analysis of component concentration,and qualitative analysis of component recognition can not be carried out using the same model simultaneously during infrared spectrum analysis of the mixed gas,a method of mixed gas component infrared spectrum recognition based on SVM regression model is proposed.

针对混合气体红外光谱分析中无法采用同一模型同时进行混合气体组分浓度的定量分析和组分种类的定性分析的问题,本文提出了基于SVM回归模型的混合气体组分种类光谱识别方法。

MnO_x catalytic gauzes are analyzed using BET、SEM and IR before and after treatment. The result shows that the specific surface area, total pore volume and average pore size of MnO_x reduce dramatically, and the infrared absorption band of N-O enhances. The removal mechanism of NO_2 using MnO_x catalyzer is preliminarily believed as absorption-catalysis process.

对使用前后的MnO_x催化网进行线性扫描和红外光谱分析,得到使用后催化剂比表面积、总孔容和总孔面积明显减小,N-O键增多,初步分析认为NO_2被MnO_x催化网去除的机理为先吸附后发生催化反应为酸。

It was shown that the absorption peaks of amine and amide groups of gelatin were shifted in HDPE/PE-g-MAH/Gelatin blends because of the reaction of PE-g-MAH with gelatin. The addition of PE-g-MAH made the increase of HDPE glass transition temperature. The compatibilizing effect of PE-g-MAH was due to the crystal compatibility produced by forming the co-crystals of HDPE, PE-g-MAH and PE-g-MAH-g-gelatin. The blends of EAA and gelatin were prepared by melting process and the compatibility of the blends was also studied.

红外光谱分析结果表明:体系中明胶的氨基吸收峰、酰胺Ⅱ带吸收峰峰位发生了明显的变化;二甲苯和水抽提实验表明,在熔融共混过程中EAA与明胶发生了反应;DMA测试共混物的玻璃化转变温度发现:两组分的玻璃化转变温度差值减小;SEM的实验结果表明,共混物中明胶的表面有接枝物形成。

The blends of PE-g-MAH and gelatin were prepared by melting process and the compatibility of PE-g-MAH and gelatin in blends were characterized. The results of FTIR showed that the characteristic absorption band peaks of amine and amide groups of gelatin were shifted in PE-g-MAH/Gelatin blends, the equilibrium values of torque were higher with the increase of blending temperature, which proved that graft copolymer PE-g-MAH-g-gelatin was formed during the preparation process, and the amount of PE-g-MAH-g-gelatin was increased with increasing the amount of PE-g-MAH. SEM micrographs exhibited that there was PE-g-MAH-g-gelatin formed in surface of gelatin phase.

通过红外光谱分析、HAAKE流变分析、抽提等实验证明:共混物中明胶的氨基、酰胺基团吸收峰峰位发生了明显的变化;在熔融共混过程中,随着温度的提高,平衡扭矩增大;明胶与PE-g-MAH发生了反应形成PE-g-MAH-g-明胶接枝共聚物,而且随着PE-g-MAH用量的增加,形成接枝共聚物的量也提高;SEM的实验结果表明,在明胶的表面确有接枝物形成;通过DMA测试共混物的玻璃化转变温度,发现两组分的玻璃化转变温度差值减小,二者的相容性提高,实现了共混体系的自增容。

It was shown that the absorption peaks of amine and amide groups of gelatin were shifted in HDPE/PE-g-MAH/Gelatin blends because of the reaction of PE-g-MAH with gelatin. The addition of PE-g-MAH made the increase of HDPE glass transition temperature. The compatibilizing effect of PE-g-MAH was due to the crystal compatibility produced by forming the co-crystals of HDPE, PE-g-MAH and PE-g-MAH-g-gelatin. The blends of EAA and gelatin were prepared by melting process and the compatibility of the blends was also studied. The FTIR results showed that absorption peaks of amine and amide groups of gelatin were shifted in EAA/Gelatin blends.

通过红外光谱分析、HAAKE流变分析、抽提等实验证明:共混物中明胶的氨基、酰胺基团吸收峰峰位发生了明显的变化;在熔融共混过程中,随着温度的提高,平衡扭矩增大;明胶与PE-g-MAH发生了反应形成PE-g-MAH-g-明胶接枝共聚物,而且随着PE-g-MAH用量的增加,形成接枝共聚物的量也提高;SEM的实验结果表明,在明胶的表面确有接枝物形成;通过DMA测试共混物的玻璃化转变温度,发现两组分的玻璃化转变温度差值减小,二者的相容性提高,实现了共混体系的自增容。

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