光度测定

By synthetically analysizing the physical and chemical properties of all components and particle size, the content of F2641 in the JOB-iC is determined by gravimetric analysis after F2641 is seperated from HMX,TATB and PNP through ? alkali reflux. Determination conditions is set as follows the sample is boilingly refluxed for six hour in a constant temperature bath after adding lOOm! 8.0 ?? 0.1% NaOH. The solvent DMF saturated by TATB is used for extracting HMX,F21 and PNP from the sample and TATB is seperated by crucible filter G4. The mass precent of TATB is determined by extraction fractionation. The mass percent of PNP is measured by multiwavlength linear regression ultraviolet spectrophotometry. The testing conditions are set as follows:multiwavlength constitution: X=267nxn, 275nm, 283nm, 29mm, 299nm,the application scope of the Lambert-Beer law: the concentration of PNP is O.005?0.O25mgIml, the concentration of HMX is 0.060.3Omg/ml,absorption coefficents of PNP and HMX are solved by the slope of linear regression curve of absorbency- concentration of standard solution of PNP and HMIX for measuring wavelengthes,on the basis of the Lanibert-Beer law and absorbancy additivity principle, the slope of linear regression curve of A/E(1) and E1 of PNP and HMX solution is regarded as the concentration of PNP in the solution.

根据传爆药中各组分的物理、化学性质及主体炸药的粒度大小，进行综合分析，确定了采用碱回流重量法测定JOB-1C 中F_(2641)的含量，测定条件：加入100ml浓度为8.0±0.1％的氢氧化钠，在恒温水浴中煮沸回流6h；采用溶剂萃取法测定JOB-1C中TATB的含量，选择TATB饱和的二甲基甲酰胺为萃取溶剂，用G4坩埚式过虑器进行萃取分离；采用多波长线性回归紫外分光光度法测定JOB-1C中PNP的含量，通过实验确定了多波长组合：λ=267nm，275nm，283nm，291nm，299nm；朗波—比耳定律的适用范围为PNP浓度：0.005～0.025mg/ml，HMX浓度：0.06～0.30mg/ml；在测定波长下，对PNP、HMX标准溶液的吸光度—浓度进行线性回归，由回归曲线的斜率得出PNP、HMX的吸收系数；根据朗波—比耳定律和吸光度加和性原理，在测定波长下，对PNP、HMX 两组分混合溶液A_i/E_HMX(i与E_PNP(i/E_HMX(i进行线性回归，回归曲线的斜率即为混合溶液中PNP的浓度。

A novel method for determination of benzoyl peroxide with spectrophotometry was developed. Inclusion ratio of β cyclodextrin to dibenzoy peroxide and benzoic acid is obtained with spectrophotometry.The mechanism of the inclusion was studied,too. The results showed that β-CD react with dibenzoyl peroxide to form a 1:1 or 2:1 host-guest complex, with the apparent formation constants of 5.0× 10~2and 2.5× 10~4 , respectively.β-CD reacts with benzoic acid to form a 1:1 host-guest complex with the apparent formation constant of 6.9 × 10~2 after the dibenzoyl peroxide was reduced by hydroxyl ammonium chloride.

建立了用β环糊精测定过氧化苯甲酰的分光光度法，并测定了β环糊精与过氧化苯甲酰和苯甲酸的包结比，随着β-CD浓度的增大，可与BPO分别形成1：1或2：1的包容络合物，包结常数分别为5.0×10~2和2.5×10~4，与苯甲酸形成1：1的包容络合物，包结常数为6.9×10~2；由于包结物的吸光度值比过氧化苯甲酰的吸光度值大大增加，建立了一种当β-CD存在下，在水溶液中测定过氧化苯甲酰的方法。

spectrophotometric method with phenol disulfonic acid ; ultraviolet spectrophotometer ; nitrate nitrogen ; comparison

本文通过对常用的酚二磺酸光度法和紫外分光光度法进行实验比对，同时调查云南省内两种分析方法考核的情况，从而找出两种方法的优缺点，供分析人员在实践中借鉴。l原理1.1酚二磺酸光度法测定的原理方法依据：GB7480一87《水质硝酸盐氮的测定酚二磺酸分光光度法》。用浓硫酸与苯酚作用生成酚二磺酸

In this cone, phosphoric acid medium, a violet-red compound was formed between chromotropic acid and formaldehyde which is photometrically determined at 570nm.

在浓磷酸介质中，甲醛与变色酸反应生成紫红色化合物，于570nm波长处作光度测定。

The culture filtrate of strain LN-176 was tested for light absorption at 260nm and 280nm, and the results showed that the protein content in the culture filtrate significantly increased. After ammonium sulphate precipitation, the supernatant and the precipitation were separated to testify their antagonistic activity, and it was found that the precipitation was inhibitory to Ustilago hordeum , but the supernatant not.

LN-176菌株的发酵液在260nm和280nm下进行吸光度测定，结果表明发酵液中蛋白质含量明显升高；发酵液经硫酸铵盐析后，取上清液和沉淀物分别做抗菌试验，发现沉淀物对青稞散黑穗病菌有拮抗活性而上清液无活性。

The effect of several factors of air agitation such as pore distance, air distributor length Lbp,wind quantum Q,time t and the tube distance of two-tubes distribution on U was measure.

本文对槽内溶液空气搅拌的浓度场进行了研究。在一长方体的有机玻璃的空气搅拌槽内，加入色素，选择有代表性的12个点，定点、定时取样，再作光度测定。这些定性及定量的结果，为优化生产设计提供了一些经验规律和理论上的依据

A highly sensitive method for the spectrophotometric determination of microamounts of aluminum by salicylfluorone and cetyltrimethyl- ammonium bromide is proposed.

本文提出一种用水杨基萤光酮和溴化十六烷基三甲基铵分光光度测定微量铝的高灵敏方法。

Zenith telescopes, spectrographic instruments and attachments, micrometers, photometers, comparators, coelostats of at least up to 65 cm diameter, and sundials of up to at least 90cm diameter rounded out the product line.

还有大到65 cm物镜直径的天顶仪、摄谱仪及配件、测微计、光度测定器、测远仪、定天镜(注：观测或拍摄天体时镜面与地轴一同转动可使图像固定不动)，大到90 cm物镜直径的日昝仪都出现在蔡司的生产线上。

The industrial magnesia and vitriol are used to produce magnesium sulfate in this paper, and the simulated wastewater is prepared using magnesium sulfate and kaolin. The flocculating effect of polyacrylamide, cationic polyacrylamide and anionic polyacrylamide is studied and compared through measurement of absorbency by spectrophotometer.

利用工业氧化镁和硫酸制备一定浓度的硫酸镁，结合高岭土配制氧化镁烟气脱硫的模拟废水，通过分光光度计吸光度测定了聚丙烯酰胺、阳离子型聚丙烯酰胺和阴离子型聚丙烯酰胺在模拟废水中的絮凝效果。

To establish a method for detection of mercuric chloride hydride in the air of workshop.

目的 建立车间空气中氯化汞的氢化物原子荧光光度测定法。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了