光度测定

The optimum condition of spectrofluorimetric determination of uranyl ion in pyridine 2,6 dicarboxylic acid β cydodextrin system is studied.

研究了吡啶 2 ，6 二羧酸β环状糊精体系荧光分光光度法测定铀酰离子的最佳条件以及某些稀土共存离子对荧光体系的干扰，并应用于人工样品的测定。

The progress in determining the minim Gallium which includes absorptiometric analysis is introduced, and various analytical approaches are discussed such as spectrophotofluorimeter, atomic absorption spectrophotometry and polarographic method etc.

介绍了近年来微量镓的分析测定方法的进展，微量镓的分析测定方法主要有光度分析法、电化学分析法和原子发射光谱法等，同时对样品的分离富集方法也进行了评述

Guangdong college of pharmacy,guangzhou,guangdong 510006,china;henan university of traditional chinese medicine,zhengzhou,henan 450008,chinaabstract:objective to establish a method for the determination of the content of total alkaloid in nao mai tong recipe.methods acid dye colorimetry was used in the determination with bromocresol green buffer solution as the color developing agent with absorbance was determined at the detection wavelength of 417 nm.results the calibration curve of the absorbance was linear with the concentration of ligustrazine in the range of 0.031～0.153 mg/ml(r=0.9998).the average recovery of ligustrazine was 100.95％,rsd=1.75%.

作者单位：广东药学院中药化学与分析教研室，广东广州 510006；河南中医学院，河南郑州 450008 目的建立脑脉通有效部位中总生物碱的含量测定方法。方法采用酸性染料比色法，以溴甲酚绿缓冲液作为生物碱的显色剂，测定样品溶液在417 nm波长处的吸收度。结果对照品川芎嗪质量浓度在0.031～0.153 mg/ml的范围内与吸光度呈良好的线性关系，r=0.9998。平均回收率为100.95％，rsd为1.75％。精密度和稳定性良好。

Rats was cannulated for in situ recirculation. UV and HPLC methods were used to determine the concentrations of phenolsulfonphthalein and scopoletin, respectively.

采用大鼠在体胃、小肠吸收实验模型，以高效液相色谱法测定灌注液中药物的浓度，紫外分光光度法测定酚红的浓度。

Effect of different surfactants on the UV intensity of Al(superscript 3+)-MXFX have been studied. Is Cetyl Trimethy-lammonium Bromide can increase the UV intensity of Al(superscript 3+)-MXFX is discovered. Based on this reaction, the reaction conditions in detail and proposed a simple, rapid and sensitive new method for the determination of MXFX by UV method is inve stigated. This method has been applied for the determination of MXFX in tablet with satisfactory results.

通过研究不同表面活性剂对Al(上标 3+)-莫西沙星体系紫外特性的影响，发现十六烷基三甲基溴化铵对该体系有显著的增敏作用；系统研究了CTMAB-Al(上标 3+)-MXFX反应体系的紫外特性，利用这一反应体系，建立了简单、快速、灵敏的测定莫西沙星的紫外分光光度法，选择了最佳实验条件，并将此方法用于莫西沙星片剂的测定，结果满意。

A spectrophotometry method, which based on the reaction of diacetyl monoxime and urea in acidic solution, was established for determination urea in bovine milk.

根据二乙酰一肟与在酸性条件下尿素的反应，建立了一种分光光度法快速测定牛奶中尿素含量的方法，该方法可以定性和定量测定牛奶中尿素含量。

According to the yogurt's complex ingredients and the particular content of diacetyl , this article studied the determination of diacetyl in yogurt with ultraviolet spectrophotometer.

本文根据乳品中的成分的复杂性及双乙酰含量的特殊性，研究了以鲜奶为溶剂制作双乙酰标准曲线和紫外分光光度法测定乳品中双乙酰含量的测定方法。

The antifungal activities of these materials were investigated and build foundation to develop low poison plant antifungal products. In experiment, polyphenols were extracted by reflux ectraction method which applyed petroleum ether to degrease and methyl alcohol solvent. Phenolic hydroxyl were examined and inspected by colour-developing reaction and the content of total polyphenols was determined by UV-spectrophotometry. Screening test were performed to the antifungal activities of polyphenol extraction by the tube dilution method to the selected ten pathogenic fungus such as Dothiorella gregaria, Rhizoctonia solani, Phyllosticta pirina, and the minimal inhibitory concentration were measured. The column chromatography and thin layer chromatography were applyed to separate and analyse cortex extracts of Dracaena cochinchinensi Lour.

实验部分采用以石油醚脱脂，甲醇为溶剂的回流提取法来提取植物多酚，用显色反应检识酚羟基；采用紫外分光光度法对多酚粗体物进行总多酚含量的测定；选取了聚生小穴壳菌、立枯丝核菌、梨叶点霉等10株常见农林业致病真菌，采用试管液基稀释法对多酚粗提取物进行了抗真菌活性筛选试验，并测定其最低抑菌浓度；采用柱层析法和薄层层析法对其中抑菌效果较好的龙血竭进行分离分析，根据其中3种化合物的光谱数据UV、IR、~(13C-NMR、1H-NMR和MS鉴定其结构。

In order to detect product\'s quality and to adjust the synthetic conditions, UV and RP- HPLC methods for the determination of the target product were established according to the components of products in the electrosynthesis course, by which target product were able to be simply, fast and accurately determined without separation in advance. And satisfactory results were obtained when they were applied to the determined of the product\'s content.

本研究为检验产品质量，调整合成工艺条件，根据电合成过程中生成物的组成情况，首先建立了无需进行分离就能够简单、快速、准确测定目标产物的紫外分光光度法和反相高效液相色谱法，并将其应用于产品含量的测定，获得令人满意的实验结果。

To determine the uncertainty of the content of arsenic in monosodium glutamate with Hydrid Atom-fluorometry.

目的 确定氢化物原子荧光光度法测定味精中砷的不确定度主要来源，从而提高测定的准确性。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。