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光度测定

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With the sample dissolved in 0.1NNaOH solution and bovine serum albumin used as the standard protein, the Percentage of proteins in the sample is given by spectrophotometric method with biuret reagent.

该法使用0.1NNaOH溶液溶解样品,以大牛血清白蛋白作为标准蛋白质,利用缩二脲试剂分光光度测定样品中的蛋白质含量。

Another group of students is recording movements of celestial objects using the telescope on Mallorca. They chose to study asteroid photometry.

另一群学生,正在用马罗卡的望远镜,纪录天体的运行,他们选择研究行星的光度测定

The paper indicated the remarkable effects on health caring liquor, which was made from Cynomorium songaricum cleared by clarifying agent s, and combined kieselguhr and gelatin and PVPP.

以锁阳为原料采用硅藻土、明胶和PVPP复合澄清处理配制的保健酒,在204nm处吸光度衡量有效物质含量,520nm处吸光度测定色度,880nm处透光率测定澄清度,结果发现各澄清剂对澄清度、有效物质及稳定性的作用显著,其中明胶与PVPP、硅藻土与明胶复合对稳定性有明显提高,其中明胶1g/L+PVPP1g/L为最佳组合。

The invention discloses a method for measuring seawater chemical oxygen demand by photometry, wherein the seawater exemplar is first pre-processed, then using the basic potassium hypermanganate as reaction system, the potassium permanganate is deacidized quantitatively by organics to produce manganate, using pure water or margin solution as reference ratio, measuring the absorbance an of the manganate at its maximum absorbing wave length 430 nm, drafting the A-COD value operating curve, obtaining the concentration of the organics in the water, i.e.

本发明公开了一种对海水化学需氧量进行测定的光度测定法,该方法首先将海水样品进行预处理,再以碱性高锰酸钾为反应体系,这样海水中的有机物在强碱性介质中与过量的高锰酸钾迅速反应,高锰酸钾被有机物定量还原后生成锰酸盐,以纯水或空白溶液作参比,在锰酸盐的最大吸收波长430nm处测其吸光度A,该吸光度A与海水样品中的有机物的含量具有正相关关系。

A new method based on the spectrophotometric system of nitrite N and safranin\|T has been developed for the determination of nitrite in this paper.

研究了在酸性条件下,亚硝酸盐氮与番红 T体系的分光光度测定,提出了一种测定亚硝酸盐氮的新方法。

Significant processing steps can include: a phase changes involving either the desired molecule or the solvent, inert carrier or vehicle, e.g., dissolution, crystallization, evaporation, sublimation, distillation or absorption; b a phase separation such as filtration or centrifugation; c any chemical change involving the desired molecule, e.g., removal or addition of water of hydration, acetylization, formation of the salt; d an adjustment of the solution containing the molecule such as adjustment of pH or pO2; e a precision measurement of contained or added BPC components, in-process solutions, recycled materials is performed, i.e., weighing, volumetric measuring, optical rotation, spectrophotometric determinations, etc.; and f changes occur in surface area, particle size, or lot uniformity, e.g., milling, agglomeration, blending.

意义较大的步骤可能会包括:a相变化,包括指定分子或溶剂,惰性载体或溶媒,如溶出作用,结晶,蒸发,升华,蒸馏或吸附;b相分离,如过滤或离心;c涉及指定分子的任一化学变化,如结晶水的除去或添加,乙酰化作用,成盐;d包含分子的溶解的调节,如调节pH或pO2;e 含有或添加原料药组分,过程内溶液,回收物料的精密测量,如,称重,体积测量,旋光度,分光光度测定,等和f 表面,粒度,或批一致性的变化,如磨碎,凝块,混合。

By means of GPC,IR,GC-MS,~(13)CNMR,~1HNMR,Methylation analysisetc,structural properties of PST-1 were identified as follows:The Mwof PST-1 was 3.44×10~6 Da and its optical rotation was _D~(20)=+0.110°(c0.1, H_2O); PST-1 constituted 8 simple sugars and the molar ratio was 2,4-Dimethoxy-Mannose:Rhamnose:Ara-binose:Xylose:Galactose:D-Galacturonic acid:Mannose:D-glucuronic acid=2%:5%:24%:9%:3%:1%:46%:10%;The chief bone of PST-1 was 1,3,6-linked-β-D-Man residue and the side chains contained Furanoid and Pyranoid residues.

结合GPC、旋光度测定、IR、GC-MS、~(13)CNMR、~1HNMR、高碘酸氧化法、Smith降解以及甲基化方法等分析测试方法,得到PST-1的单糖组成及结构表征,实验结果如下:红豆杉多糖PST-1是重均分子量为3.44×10~6 Da的支链多糖,旋光度为20D=+0.110~0(c0.1,H_2O);PST-1单糖组成为:2,4-Dimethoxy-Mannose:Rhamnose:Arabinose:Xylose:Galactose:D-Galacturonic acid:Mannose:D-glucuronic acid=2%:5%:24%:9%:3%:1%:46%:10%;PST-1的骨架结构为:具有1,3,6-连接的β-D-甘露糖残基骨架,侧链分枝包括非还原末端的呋喃型α-L-阿拉伯糖残基、吡喃型α-L-阿拉伯糖残基、β-D-木糖残基、β-D-甘露糖残基、2,4-二氧甲基-β-D-甘露糖残基和α-D-葡萄糖醛酸残基;侧链的糖残基也可能存在2,5-二氧-取代呋喃型α-L-阿拉伯糖基、3-氧-取代的β-D-木糖残基、6-氧-取代的α-D-半乳糖醛酸残基、6-氧-取代的α-D-半乳糖残基、4-氧-取代的α-D-葡萄糖醛酸残基和2-氧-取代的α-L-鼠李糖残基,同时后者也可能穿插在主链上。

Applied with test of potted plant and measurement absorbency for study physiological response of activity of cell defense enzymes and lipid peroxidation of slash pine's half-sib under water stress. There are 7 families comparison with general slash pine. The contents of superoxide dismutase, catalase, antioxidant, malondialdehyde and the rate of superoxide anion(-O2) generating are mensurated under normal water condition while soil water content is 70% and light water stress while soil water content is 55% to 60% and medium water stress while soil water content is 35% to 40% and heavy water stress while soil water content is 20% to 25%. The test result indicate that either water grads or families of contents of SOD,CAT,AsA,MDA are mighty notable difference. The rate of -O2 generating is notable difference within families. The rate of -O2 generating is mighty notable difference within water grades.

为研究湿地松优良半同胞家系保护酶及脂质过氧化作用对水分逆境的生理响应,采用盆栽试验和吸光度测定结合的方法,以普通湿地松种子为对照,测定了七个湿地松半同胞家系在正常水分状态(土壤相对含水量为70%)、弱度水分胁迫(土壤相对含水量为55%~60%)、中度水分胁迫(土壤相对含水量为35%~40%)和强度水分胁迫(土壤相对含水量为20%~25%)条件下的SOD、CAT、AsA、MDA的含量和-O2产生速率,研究结果表明:无论是不同水分梯度还是不同家系水平,SOD、CAT、AsA活性和MDA含量的差异均达极显著水平,不同家系水平间-O2产生速率有显著差异,不同水分梯度间-O2产生速率差异达极显著水平。

Applied with test of potted plant and measurement absorbency for study response of the contents of photosynthetic pigments of slash pine's half-sib under water stress. There are 7 families comparison with general slash pine. The contents of photosynthetic pigments are mensurated under feebleness water stress while soil water content is 55% to 60% and moderate water stress while soil water content is 35% to 40% and heavy water stress while soil water content is 20% to 25%. The test result indicate that either water grads or families of chlorophyll and chlorophyll a and chlorophyll b and Chla/Chlb and carotenoid and Caro/Chl are mighty notable difference. The Chl and Chla and Chlb and Chla/Chlb little drop from normal soil water to initial water stress. Then drop obvious with increased water stress. The Caro and Caro/Chl little drop firstly from normal soil water to initial water stress,then up in metaphase water stress,after drop in evening water stress. The Chl and Chla and Chlb and Chla/Chlb and Caro of slash pine'half-sib are over general slash pine. The Chl and Chla and Chlb and Chla/Chlb and Caro of 464 and 1027 are over average value of slash pine's half-sib under water stress. The Caro/Chl of 609 and 46 are over average value of slash pine's half-sib under water stress.

为研究湿地松半同胞家系光合色素对水分逆境的响应,采用盆栽试验和吸光度测定方法,以湿地松普通种子为对照,测定了七个湿地松优良半同胞家系在弱度水分胁迫(土壤相对含水量为55%~60%)、中度水分胁迫(土壤相对含水量为35%~40%)和强度水分胁迫(土壤相对含水量为20%~25%)条件下的光合色素,对湿地松优良半同胞家系在不同水分胁迫条件下的光合色素进行了研究,结果表明:无论是不同水分梯度还是不同家系水平,Chl、Chla、Chlb、Chla/Chlb、Caro、Caro/Chl均有极显著差异;从正常水分至水分胁迫初期Chl、Chla、Chlb、Chla/Chlb稍微下降,后随着水分胁迫程度的加深下降较快,从正常水分至水分胁迫初期Caro、Caro/Chl先稍微下降,胁迫中期上升,胁迫后期下降;所有半同胞家系的Chl、Chla、Chlb、Chla/Chlb、Caro高于普通种,在水分胁迫条件下家系464、1027的Chl、Chla、Chlb、Chla/Chlb、Caro高于家系的平均水平,家系609、46的Caro/Chl值高于家系的平均水平。

Objective To introduce a new method for determination of urinary iodine by using ammonium persulfate digestion, this method was modified from the national standard method of chloric acid digestion.

目的 介绍修订后的尿碘测定标准新方法,即尿中碘的过硫酸铵消化。砷铈(As3+、Ce4+)催化分光光度测定方法,建议各级实验室应尽快应用。

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