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It is a organic hexahydric weak acid. In different acidity, the dissociation degree and the color of reagent solvent were different also. Determined and draw the absorption curve of reagent in varies acidity, and figured out the dissociation constant by Perisic-Janjic method; the complex ratio of the reagent and bismuth was determinated by mole ratio method and continuous variation method; The apparent stability constant of the complex was calculated, the mechanism of dissociation and coordination were discussed.

2,6—二溴4—硝基偶氮氟胂是本实验室合成的测定铋的一个较好的试剂,对其进行了进一步的研究,在用柱层析法对其进行了提纯后,测定了试剂在不同酸华东师范大学硕:l:学位论文摘要度下的吸光度和最大吸收波长,绘制了其吸收曲线,用Perisic一Janjic法计算了试剂的六级离解常数;用摩尔比法和连续变化法测定了试剂与秘形成的配合物的络合比:计算了配合物的表观稳定常数,研究了其离解和配合机理,为筛选高效有机显色剂提供了理论依据。

To determine the uncertainty of the content of arsenic in monosodium glutamate with Hydrid Atom-fluorometry.

目的 确定氢化物原子荧光光度法测定味精中砷的不确定度主要来源,从而提高测定的准确性。

Methods Hydrid Atom-fluorometry was applied to determine the uncertainty of arsenic content.

采用国家标准GB/T 5009.11-2003氢化物原子荧光光度法对味精中砷测定的不确定度进行评定。

These are main problems of eutrophication.In this paper we selected alga that suits to grow under different concentration of nutrition, after selecting seed, domesticating, culturing alga purely in the lab, we gained Hydrodictyon reticulatum and microalga, most of which are Miorocystis and chlorella.

本文选取在不同营养水平条件下适合生长的藻类物种,在实验室进行选种、驯化和纯化培养,得到水网藻和微藻(主要为微囊藻Miorocystis、小球藻chlorella);以实验室培养的生长速度快、生产能力高的水网藻为原料,制备一系列环境友好性光敏物质——叶绿素及其衍生物,运用光敏氧化分光光度法测定活性氧(O_2~-,H_2O_2,·OH,和~1O_2),根据其光敏产生活性氧效率,进行光敏物质的筛选;选用叶绿素铜及其钠盐,以微藻为实验控制对象,以Cu~(2+)作培养对照,在相同光照、营养条件下进行控藻实验。

Extraction of edible red pigmengt from solanum nigrum fruit by optimum seeked process conditions, determined single factor condition, designed orthogonal layout, and measured absorbance at 527nm wavelength, weighed up the pigment extracting effect and stability. The most favoured extracte conditions were determined as follows: The extracting regent was citric acid hydrotropic solution, pH was 1.72, the quantities of added sample to the solution was 3.35g/100mL, the temperature was 60℃, the extracting time w...

以成熟的龙葵果为原料提取食用红色素,通过优化工艺、确定单因素条件、设计正交试验,以527nm波长的吸光度值衡量色素提取效果和稳定性;最优化的提取条件为:柠檬酸水溶液提取剂pH为1.72,样品加量3.35g/100mL,提取温度60℃,浸提时间60min;龙葵红色素提取液长期接触光、空气和Fe3+,稳定性下降,因此,在提取、干燥和储存时要尽量避免长时间接触光和空气、避免与铁制容器直接接触。

From the UV-vis absorption spectra data, we can obtained: a Intruduce a 3-sulfopropyl into thiacyanine makes λ〓 red shift 1nm; b For the anionic thiacyanines, the substituent at the 5-position of the benzene ring has influence on λ〓· Acroding to the sequence F, Cl, CH〓, OCH〓, 4, 5-benzo,λ〓 red shift. Strong electron-withdrawing group CF〓 makes λ〓 hypsochromic shift 1nm.

选取三个系列的15个染料在乳剂中作增感实验,并用摄谱仪测定了乳剂的感色峰,结果表明:吸电子取代基不利于增感,给电子取代基有利于增感;噻菁染料的加入扩大了乳剂的感色范围,弥补了卤化银乳剂在465~505nm范围内感光度的不足。

The concentration of shikimic acid in Illicium verum Hook.f.was determined with ultraviolet spectrophotometry.

采用紫外分光光度法对9批不同产地的八角茴香样品中的莽草酸进行了含量测定。

Methods UV was used to detect the absorption force and tannis in Carbonized Imperata Cylindrica by different kinds of processing methods.

:目的筛选茅根炭炮制的最佳工艺。方法采用分光光度法,测定不同工艺炮制的茅根炭吸附力的大小和鞣质含量。

In this experiment, we made a comparison and analysis of peroxidase total activity and isozymes of Paulownia trees with and without witch's broom by using spectrophotometer and incontinuous polyacrylamide gel electrophoretic methods.

分别采用分光光度法和不连续聚丙烯酰胺凝胶盘状电泳法,比较分析了感病与未感病泡桐树木的过氧化物酶总活性与同工酶的变化。

Observation with transmission electron microscope showed that interalveolar septa were widened with increased amount of collagen in the MP infected rats while there were no obvious abnormalities in the other two groups.(2) Positive expression of bFGF mRNA were found in alveolar walls of MP infected rats. No expression of bFGF mRNA was found in control animals. In the rats infected with MP but treated with erythromycin positive expression of bFGF mRNA was found to be scarcely distributed in alveolar walls.

2感染组动物肺泡壁见明显的bFGF mRNA阳性表达颗粒,对照组基本未见bFGF mRNA阳性表达,感染加红霉素治疗组仅见散在分布的少许bFGF mRNA阳性表达;定量分析结果表明,感染组bFGF mRNA阳性表达的积分吸光度为41.32±10.44,与对照组(0.30±0.13)和感染加红霉素治疗组(6.03±2.41)比较,差异有显著性( P <0.01)。

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