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The relationship among stray light,absorbance error and absorbance true value for UVVISS was discussed in this paper.

本文研究了紫外可见分光光度计UVVISS的杂散光S.L.Strary Light与吸光度误差和吸光度真值之间的关系导出了S.L。

The relationship among stray light,absorbance error and absorbance true value for UV/VISS was discussed in this paper.

本文研究了紫外可见分光光度计的杂散光 S.L。与吸光度误差和吸光度真值之间的关系;导出了S.L。

The relationships between absorbance error and absorbance true value for 14 stray light values were further calculated,and the 12 correspording curves were drawn.

下,吸光度误差与吸光度真值的关系,并绘制了12条误差曲线同时对如何使用计算公式和有关的误差曲线、如何控制和选择UVVISS的S.L。

Significant processing steps can include: a phase changes involving either the desired molecule or the solvent, inert carrier or vehicle, e.g., dissolution, crystallization, evaporation, sublimation, distillation or absorption; b a phase separation such as filtration or centrifugation; c any chemical change involving the desired molecule, e.g., removal or addition of water of hydration, acetylization, formation of the salt; d an adjustment of the solution containing the molecule such as adjustment of pH or pO2; e a precision measurement of contained or added BPC components, in-process solutions, recycled materials is performed, i.e., weighing, volumetric measuring, optical rotation, spectrophotometric determinations, etc.; and f changes occur in surface area, particle size, or lot uniformity, e.g., milling, agglomeration, blending.

意义较大的步骤可能会包括:a相变化,包括指定分子或溶剂,惰性载体或溶媒,如溶出作用,结晶,蒸发,升华,蒸馏或吸附;b相分离,如过滤或离心;c涉及指定分子的任一化学变化,如结晶水的除去或添加,乙酰化作用,成盐;d包含分子的溶解的调节,如调节pH或pO2;e 含有或添加原料药组分,过程内溶液,回收物料的精密测量,如,称重,体积测量,旋光度,分光光度测定,等和f 表面,粒度,或批一致性的变化,如磨碎,凝块,混合。

A new catalytic kinetic spectrophotometric method for the indirect determination of trace sulfide has been studied. The method was based on the inhibition of sulfide on the iron catalyzed oxidation of xylenol orange by hydrogen peroxide in NH3 medium.

在氨水介质中,硫离子可阻抑Fe催化过氧化氢氧化二甲酚橙褪色,并且催化体系和阻抑体系在570nm处吸光度的差值与硫离子浓度呈线性关系,据此建立了阻抑动力学光度法间接测定痕量硫离子的新方法。

With the same zirconium concentration,the absorbance of zirconyl oxyhalide solution (λ=664nm)prepared in HCl was larger than that from pure zirconyl oxyhalide solution.

发现对于相同锆浓度的溶液,高酸度的锆贮备溶液中的锆与偶氮胂Ⅲ形成的化合物的吸光度(λ=664nm)要大干仅由氧氯化锆配制的锆贮备溶液中的锆与偶氮胂Ⅲ形成的化合物的吸光度

Anthocyanidin extract in methanol showed 3 absorption peaks, at 270, 340 and 520 nm, in the UV-vis spectrum, with bathochromic and hypsochromic shift with methanol+AlCl3 and methanol+AlCl3+HCl, respectively; the ratio of the absorbance at 440 nm to that at 520 nm was 0.29. No fluorescence occurred under UV irradiance, and 5 absorption peaks occurred at 270 nm after HPLC. Five molecular ion peaks occurred on MS: 595, 381, 611, 587 and 571, respectively, and monosaccharides in the extract were identified as rhamuose and glucose on HPLC.

一品红花色素的甲醇溶液分别在270、340 和520 nm 处有 3 个吸收峰;在 440 nm 吸光度与可见光最大吸收波长 520 nm 吸光度的比值为0.29;花色素的甲醇溶液中加入AlCl3后发生红移,再加入HCl后发生蓝移;色素溶液在紫外光下无荧光;色素样品经液相色谱分离后在 270 nm检测有 5 个比较明显的吸收峰;质谱中得到 595、611、381、571 和 589 等对应的分子离子峰;花色素酸解液高效液相色谱图谱和鼠李糖、葡萄糖的出峰时间一致。

In order to provide some scientific data for judging biological toxicity and bioavailability caused by heavy metals in sediments in Guilin, China, for the first time, the authors sampled sediments in different water areas in Guilin, and determined AVS by P-Amino dimethyl aniline dihydro chloride photometry through a set of acidification-ventilation-absorption AVS reaction unit, determined copper, lead, zinc, cadmium and nickel with tomic absorption spectrophotometry, mercury and arsenium with atomic fluorescence, and cipangopaludina cathayensis was selected as the tested species for bioavailability experiment.

首次以桂林水系沉积物为研究对象,通过酸化-吹气-吸收装置,用对氨基二甲基苯胺光度法测定沉积物中AVS含量,用原子吸收分光光度法测定SEM和间隙水中Cu、Pb、Zn、Cd、Ni含量,用原子荧光法测定Hg、As含量。

The contents of Mn, Cu, Fe, Zn in the leave, flower, seed of Impatiens balsamina induced by space flight are determined by flame atomic absorption spectrometry. The measure parameters for FAAS are optimized.

采用火焰原子吸收分光光度法测定了航天诱变凤仙花的茎、叶、花、种子中Mn、Cu、Fe、Zn四种微量元素的含量,优化了原子吸收分光光度法测定参数。

The cloud should then have an infrared luminosity thousands of times the sun's bolometric luminosity.

云的红外光度应为太阳热光度的几千倍。

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