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Aiming at the problems occurred in the analytical process of determining the total phosphorus in industrial circulating cooling water by ammonium molybdate spectrophotometry and based on the experience summary,the original analytical method has been improved.

针对用钼酸铵分光光度法测定循环冷却水中的总磷在实际分析过程中遇到的一些问题,经过总结经验,改进了原有的分析方法,降低了测定中的干扰因素,提高了一次分析结果的准确可靠性,使分析结果更为准确可靠。

Methods:Spectrophotometry was selected to determine the phosphorus level in soya lecithin,based on the formation of the blue complex by phosphate with ammonium molybdate and Fiske-Subbarow reagent in acid solution.

将样品中的有机磷酸化合物分解转化为无机磷酸盐,再利用在酸性溶液中磷酸盐与钼酸铵及Fiske-Subbarow试剂作用生成蓝色的化合物,在660nm处用分光光度法测定。

Potassium persulfate was used to digest the sewage sludge from municipal wastewater treatment plant in the high pressure sterilizer at 120 ℃, and the ammonium molybdate spectrophotometric method was used to determine total phosphorus content in the sewage sludge.

在高压灭菌器中于120℃下,用过硫酸钾溶液消解城市污水处理厂污泥,采用钼酸铵分光光度法测定污泥中总磷的含量。

These methods include a photocatalytic degradation of methyl orange solution-spectrophotometric method to measure the degradation rate of organic matter by self-cleaning glass, a UV-Vis spectrophotometric scanning procedure to measure the transmittance and a hydrophility measuring method by using a contact angle meter.

详细研究了用以表征自洁净玻璃主要性能的各种测定方法:采用紫外光辐照降解甲基橙-分光光度法测定自洁净玻璃对有机物的降解效率即光催化活性;利用紫外可见光分光光度计扫描测量其透过率光谱曲线;用接触角测定仪测量其样品表面的亲水性。

The method showed a satisfactory results when antimony oxide samples were determined. The linear calibration curve range of P and Si was obtained within 0.01-300 mg/L, and the detection limits were obtained to be 0.07 μg/mL and 0. 04 μg/mL respectively.

在优化的实验条件下,当硅磷的含量在0.01~300 mg/L范围内时,其吸光度与硅磷浓度呈良好的线性关系,方法的检出限为Si 0.04 mg/L,P 0.07 mg/L。

Methods The pyrogllol auto-oxidation was adopted to produce superoxide anion O(superscript - subscript 2; the system H2O2/Fe(superscript 2+) was used to produce hydroxy radical through Fenton reaction; and spectrophotometry was used to detect the clearing functions of drugs with different concentrations against O(superscript - subscript 2) and OH.

采用邻苯三酚自氧化法产生超氧阴离子自由基O(上标-下标 2,采用H2O2/Fe(上标 2+)体系通过Fenton反应产生羟自由基,用分光光度法分别测定不同浓度的药物对O(上标-下标 2)是和OH的清除作用。

In this paper,the method for measuring water soluble Sulphate in soil by Barium Chromate Spectrophotometry is discussed as well as the experiment conditions about the rate of water soil and vibration time.

介绍铬酸钡分光光度法测定土壤中水溶性硫酸盐的分析方法,并讨论了水土比、振荡时间等实验条件。

Methods A series of improved experiments on barium chromate spectrophotometry without heating and the experiments of precision and accuracy,as well as comparison of experimental data between the improved method and the National Standard Method were carried out.

方法采用不加热方法,对铬酸钡分光光度法进行一系列改进实验,并进行了精密度及准确度试验,与国家标准方法的测定结果进行了比较实验。

In this study,the organic sulfur compound is decomposed in a oxygen flask;organic sulfur is turned into sulfate sulfur,and then the measure of sulfate is determined by Barium Chromate Spectrophotometer .

本文用氧弹燃烧法将煤中有机硫氧化成二氧化硫和三氧化硫,再将其转化成硫酸盐硫,建立铬酸钡光度法测定硫酸根的方法,从而间接得到有机硫的含量。

Solubility of barium chloride and barium oxide in hydrochloric acid, ethanol,acetone,ether and hydrochloric acid- ethanol,hydrochloric acid- acetone,hydrochlo- ric acid- ether has beeen studied and the separation of Ba O from Ba Cl\- 2 with hydrochloric acidethanol as the solvent has been proposed.

研究了氯化钡和氧化钡在盐酸、乙醇、丙酮、乙醚及盐酸-乙醇、盐酸-丙酮、盐酸-乙醚中的溶解性,提出以盐酸-乙醇为溶剂进行两者的分离。以 DBC- CPA为显色剂分光光度法测定氧化钡的含量,加料回收率为 98%~ 10 2 %,氧化钡含量为 0 。32 %时,平行测定 7次,相对标准偏差为 1。 58%。该法适于快速测定热处理盐浴中氧化钡的含量,对监控盐浴品质有指导意义

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