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In this paper, under the condition of systematic discussing the endangerment of waste water including phenol ,the present treatment method, the mechanism of photocatalytic of TiO2 semiconductor and the reaction of magnetic chymistry, a new method of taking off phenol is proposed:photocatalytic degradation of phenol by TiO2 coupling with magnetic field.

本文在系统的论述了含酚废水的危害及其处理技术、半导体TiO2光催化和磁化学反应的机理的基础之上,提出了磁场-TiO2光催化耦合降解水中苯酚的新方法。

The results: the phase transferring range of TiO2 is between 600-750℃; with the doping of tourmaline, the UV-VIS adsorption spectrum of Nd/TiO2 was basically not affected, and showed a gradual Einstein shift with the increase of calcined temperature between 300-750℃; OH intensity of Nd/TiO2 could be enhanced both in irradiation and in no irradiation when tourmaline was added in it; the doping of 0.6% tourmaline led to the best photocatalytic activity of Nd/TiO2 and the best photocatalytic effect appeared when calcined at 600℃.

结果发现TiO2的相变转化区间在600~750℃范围内;电气石掺入对Nd/TiO2材料的光吸收范围基本没有影响,在300~750℃范围煅烧后,随温度升高UV-VIS图谱有逐渐红移现象;电气石的加入使得Nd/TiO2材料在光照及未光照条件下都起到增强OH强度的作用;在Nd/TiO2材料中掺入0.6%的电气石获得最好的光催化活性,600℃下煅烧光催化效果较优。

The result was compared with oxidations of cyclohexene without irradiation and at irradiation without catalyst.

另外,本文还研究了各种类型的催化剂在中压汞灯下光催化环己烯的氧化反应,结果表明,无论上述的哪种催化剂,在中压汞灯下光催化环己烯氧化反应,都得不到环氧环己烷,生成的产物主要为水和二氧化碳。

In this paper TiO2/minerals have been prepared using natural minerals as carrier and the industrial metatitanic acid and the industrial sulfate titanium liquid as the raw material based on the effects such as loading capacity of TiO2, specific surface area of minerals, different mineral source and preparation cost.

本研究以天然矿物对TiO_2的负载能力、比表面积、矿物来源、材料成本等因素为依据,通过对天然矿石载体的活化工艺研究和工业偏钛酸、工业硫酸钛液为原料制取TiO_2/天然矿物复合材料的制备工艺研究,以及样品光催化降解有机物的研究,最终制得了具有光催化活性的TiO_2/天然矿物复合材料。

The research result also showed that aminoalkylferrocene and new ferric alkyldithiocarbamate were effective initiators of the two kinds of biodegradation of the PE film; and new nickelous alkyldithiocarbamate could effectively control the initial process of its biodegradation; and PE film with them had better environmental degradability.

其中聚 酯、聚酰胺和聚氨酯等聚合物是通过H'或 OH_催化的水解降解引发过程,而聚乙烯、聚丙烯和聚苯乙烯等聚烯烃主要是通过光、热、氧和过渡金属离子催化的光一氧降解引发过程。但它们的最终可被生物吸收的产物都是低分子量的羧酸。

Nano titanium dioxide is of favorable biological and chemical inertness, strong oxidizability, low cost and long-term stability against photocorrosion and chemical corrosion. Nano TiO_2 and TiO_2/SiO_2 thin films are used photocatalysis degradation materials and self-cleaing materials, and can kill bacteria and virus.At present it is the hot spot in the research of photocatalysis, and it is of great value in the practical applications.

由于纳米TiO_2具有良好的生物和化学惰性、较强的氧化性能、低成本、以及对光腐蚀和化学腐蚀的稳定性等,故其薄膜不仅能用作光催化降解和自洁净材料,还能杀死细菌及病毒,是目前光催化材料的研究重点,具有广阔的应用前景。

Morphological structures of TiO2 such as crystal structure, particle size, surface area and surface state properties which influence photoactivity of the catalyst have been discussed.

本文介绍了TiO2多相光催化剂的作用机理及其结构特性对光催化活性的影响,并对TiO2的晶相组成、晶粒尺寸、比表面积、表面形态与光催化活性的关系作了综述。

TiO2 photocatalyzer supported on glass were prepared with sol-gel method. The photocatalytic degradation of methylene blue was studied including the effect of the factors such as reaction time, the initial concentration and pH value on the photocatalytic degradation.

采用溶胶-凝胶法制备了玻璃负载的TiO2薄膜光催化剂,研究了该催化剂对亚甲基蓝溶液的光催化降解,考察了反应时间、水样的初始浓度、溶液的pH等对光催化降解效果的影响。

Some products such as: diisobutyl phthalate, cyclohexylmethyl tridecyl oxalate and 2-isopropylcyclohexanol that have not been reported in the directly oxidation of alkane by traditional method have been obtained, and all the products are used in fuel, leather, textiles, cosmetics and so on.(3) Metal-promoted superacids SO_4~(2-)/SnO_2-M_XO_Y (M= Ce, Co, V, Mo, Ti), which were highly active for this reactions, were investigated in order to improve its acid sites activity, selectivity and stability.

这一在常温常压下以锡系超强酸为催化剂催化氧化碳氢化合(来源:ABCca8cca论文网www.abclunwen.com)物的反应还未见报道:(3)金属改性锡系固体超强酸SO_4~(2-)/SnO_2-M_XO_Y(M=Ce,Co,V,Mo,Ti)在催化氧化反应中表现出很好的催化活性,通过研究表明金属改性剂的加入提高了催化剂酸性,选择性和稳定性;(4)具有光催化活性金属Ti的引入极大的提高了催化剂SO_4~(2-)/SnO_2的比表面积。

So it is most important to set up the relations between the organics, the catalyst and the reactor parameters for industry application.

因此,以实际应用的角度,建立有机物光催化特性与催化剂条件、反应器参数之间的联系,是目前光催化技术发展的重要工作。

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