儿茶

Purpose To study the electrochemical behavior of catechol at poly modified electrode and to establish a voltammetric method for the determination of catechol.

目的 研究儿茶酚在聚刚果红修饰电极上的电化学行为，建立儿茶酚的伏安测定方法。

PurposeTo study the electrochemical behavior of catechol at poly modified electrode and to establish a voltammetric method for the determination of catechol .

目的研究儿茶酚在聚刚果红修饰电极上的电化学行为，建立儿茶酚的伏安测定方法。

AIM: To study the quality standard on catechu and its extract.

目的 ：研究儿茶及儿茶提取物的质量标准。

A crystalline substance, C15H14O6, derived from catechu and used in tanning and dyeing.

儿茶酸一种晶体物质，c15h14o6，来源于儿茶，用于制革和染色

The inhibiting influenza A virus effect of catechu extract was observed by means of chick-embryo culture , and the inhibitory activity of catechu extract on influenza A virus in vitro was observed by the hemagglutination inhibition test.

用狗肾传代MDCK细胞培养法观察儿茶提取物抑制甲型流感病毒的致细胞病变作用；用鸡胚培养法观察儿茶提取物抑制甲型流感病毒增生的作用；用红细胞凝集试验观察儿茶提取物体外直接抑制甲型流感病毒的作用。

Effects of Tea Catechins, Epigallocatechin, Gallocatechin, and Gallocatechin Gallate, on Bone Metabolism

茶中的儿茶酚：表没食子儿茶素，没食子儿茶酸和没食子儿茶酸没食子酸盐对骨代谢的作用。

Results Eleven compounds were isolated and identified as:quercetin(1),kaempferol(2),quercitrin(3),protocatechuic acid(4),gallic acid(5),protocatechuic acid ethyl ester(6),ethyl gallate(7),vanillic acid(8),1,5,7-trihydroxyl-3methylan...

结果得到11个化合物，分别鉴定为：槲皮素(1)、山柰酚(2)、槲皮苷(3)、原儿茶酸(4)、没食子酸(5)、原儿茶酸乙酯(6)、没食子酸乙酯(7)、香草酸(8)、1，5，7-三羟基-3-甲基蒽醌(9)、琥珀酸(10)、5-羟甲基糠醛(11)。结论化合物6、7、9、11为首次从该属植物中分离得到。

To further study the chemical constitutes of lipophilic active parts, we prepared Alc95% and Alc50% according to original literature. 20 compounds were isolated by using macroporous resin, silica gel, polyamide, Sephadex LH-20, Rp-18, preparative TLC and preparative HPLC chromato-graphy. The structures of them were elucidated by means of physical and chemical properties, modern spectroscopic analysis techniques—UV、IR、 EI/MS、ESI/MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC. They are nine anthraquinones: chrysophanol (95-1), physcion (95-2), emodin (95-5), aloemodin (95-7), rhein (50-1), sennoside A or B (50-6),ω-hydroxylemodin (95-10), chrysophanol-8-0-β-D-glucoside (95-12), aloemodin-ω-0-β-D-glucoside (95-13); three phenanthaquinones: tanshinone ⅡA (95-3), cryptotanshinone (95-6), tanshinone Ⅰ(95-4); one isoflavone: 7, 3'-dihydroxyl-5' methoxyisoflavone (95-14) and protocaechuic aldehyde (95-9), protocaechuic acid (95-11), astragaloside Ⅳ(50-4), amygdalin (50-5), 2, 3, 5, 4'-tetrahydroxylstilbene-2-0-β-D-glucoside (50-3),-catechin (50-2), cinnamic acid (95-8). Among them, 3'-dihydroxyl-5' methoxyisoflavone (95-14) is a new compound.

经过溶剂萃取、大孔吸附树脂富集、Sephadex LH-20精制、制备TLC及Semi-pre HPLC等手段从中分离了20个化合物，利用理化性质和波谱技术(UV、IR、EI／MS、ESI／MS、〓H-NMR、〓C-NMR、DEPT、HMQC、HMBC)相结合鉴定了它们的结构，分别为9种蒽醌类化合物：大黄酚，大黄素甲醚，大黄素，芦荟大黄素，大黄酸，番泻苷A或B，ω-羟基大黄素(ω-hydroxylemodin)，大黄酚-8-0-β-D-葡萄糖苷(chrysophanol-8-0-β-D-glucoside)，芦荟大黄素-ω-0-β-D-葡萄糖苷(aloemodin-ω-0-β-D-glucoside)；3种菲醌类化合物：丹参酮ⅡA(tanshinoneⅡA)，隐丹参酮，丹参酮Ⅰ(tanshinone Ⅰ)；1种异黄酮：7，3'-二羟基-5'-甲氧基异黄酮（7，3'-dihydroxy-5' methoxyisofla-vone）以及原儿茶醛，原儿茶酸，黄芪甲苷(astragaloside Ⅳ)，苦杏仁苷，2，3，5，4'-四羟基二苯乙烯-2-0-β-D-葡萄糖苷（2，3，5，4'-tetrahydroxylstilbene-2-O-β-D-g1ucoside），Z—儿茶素，桂皮酸。

Therefore this research is to synthesize alkyl dialkyl o-hydroxyphenyl phosphate (8) as new lubricant additives.

所以本研究希望能结合磷酸酯与儿茶酚二者的优点以开发出新型态的润滑油添加剂---儿茶酚磷酸酯衍生物。

Abstract］ Objective To study a RP-HPLC methods that determined the protocatechuic acid content in Fuxuekang Jiaonang.

妇血康胶囊中原儿茶酸的含量测定［摘要］目的建立反相高效液相色谱法测定妇血康胶囊中原儿茶酸的含量。

Breath, muscle contraction of the buttocks; arch body, as far as possible to hold his head, right leg straight towards the ceiling (peg-leg knee in order to avoid muscle tension).

呼气，收缩臀部肌肉；拱起身体，尽量抬起头来，右腿伸直朝向天花板（膝微屈，以避免肌肉紧张）。

The cost of moving grain food products was unchanged from May, but year over year are up 8%.

粮食产品的运输费用与5月份相比没有变化，但却比去年同期高8％。