偶氮苯

Starting from 3-benzoyl-5-formyl-indolizine, 3-benzoyl-5-(2'2'-diacetylethenyl)-indolizines and analogs were obtained by the 〓mediated aldol condensation or Wittig reaction. These compounds,promoted by low-valent titanium, gave highly functionlizedcycl[3,2,2]azine derivatives. The coupling reaction proceeded betweenthe carbonyl group and the carbon-carbon double bond, a rare example inMcMurry reaction.

我们以3-苯甲酰基-5-甲酰基中氮茚为原料，通过三碘化钐促进的aldol反应和Wittig反应制备了3-羰基-5-羰基乙烯基中氮茚，随后经低价钛还原偶联，没有生成正常的分子内羰基-羰基偶联产物，而是得到反常的羰基与α，β-不饱羰基的双键偶联产物，较高收率地得到了含多官能团的CycI[3，2，2]azine衍生物。

In the presence of CPB, the chromogenic reaction of V with DPCO has been studied.

研究在溴化十六烷基吡啶存在下，钒与二苯偶氮羰酰肼显色反应的分析特性。

The controlled/living radical polymerization of methacrylates containing carbazolyl or 1,3,4-oxadiazolyl groups via RAFT polymerization was successfully demonstrated. Functional polymers poly, poly, poly, and poly with hole- or electron-transfer ability were synthesized with cumyl dithiobenzoate as a chain transfer agent and AIBN as an initiator in a benzene solution.

以合成的二硫代苯甲酸酯异丙苯酯为链转移剂、偶氮二异丁腈为引发剂，通过RAFT可控／活性自由基聚合方法成功地合成了侧链上悬垂空穴传输基团或电子传输基团(1，3，4-噁二唑基团)的光电功能聚合物：poly、poly和poly、poly。

Racemic backbones 2-amino-2'-hydroxy-6,6'-dimethyl-l,l'-biphenyl la and 2-amino-2'-hydroxy-4,4',6,6'-tetramethyl-l,1'-biphenyl 1b were synthesized from o-methylaniline and 2,4-dimethylaniline via nitration, diazotation/iodination, Ullmann coupling, selective reduction, diazotation/hydrolysis and hydrogenation.

从邻甲苯胺及2，4-二甲基苯胺出发，经过硝化，重氮化-碘代，偶联，单还原，重氮化-水解及还原反应合成了消旋体骨架2-氨基-2'-羟基-6，6'-二甲基-1，1'-联苯1a和2-氨基-2'-羟基-4，4'，6，6'-四甲基-1，1'-联苯1b。

The influences of groups -CH〓 and -Cl on the fluorescence analysis performance of aresenoxylphenylazo rhodanine class were mainly studied.

主要系统研究了-CH〓、-Cl基团对含胂酸基苯偶氮若丹宁衍生物荧光分析性能的影响。

EVA/LDPE/ CB conductive foam was made of EVA and LDPE as matrix,HG-1P CB and ACET CB as conductive filler,AC as foamer and DCP as crosslinker.

文章以乙烯-乙酸乙烯酯和低密度聚乙烯为主基体，特导炭黑(HG-1P)和乙炔炭黑为导电填料，偶氮二甲酰胺为发泡剂，过氧化二异丙苯为交联剂，制备了EVA/LDPE/炭黑导电泡沫复合材料。

Amphiphilic graft copolymers were synthesized by the copolymerization of polyoxyethylene macromer with butyl acrylate and methyl methacrylate in benzene using azobisisobutyronitrile as initiator.

以偶氮二异丁腈为引发剂，将大单体聚环氧乙烷与小单体丙烯酸丁酯、甲基丙烯酸甲酯在苯溶液中进行共聚，合成了两亲性接枝共聚物。

It is shown that the optimal conditions for the reaction of CADB with SESA are pH 12.0 and m:m=6:1.The product p-aminobenzart sulfanily ethyl CADBwas diazotized and linked with lipase.The optimal pH for lipase linked to diao-compound is 7.5.The link time is at last 12h.

试验结果表明：CADB与SESA反应的最适条件是pH＝12.0，SESA与CADB质量比为6：1，反应生成的对氨基苯磺酰乙基交联烯丙基葡聚糖凝胶经重氮化后与脂肪酶偶联的最适条件是pH7.5，偶联时间≥12h。

The polymer particles were prepared by copolymerization of phthalic aldehyde, allyl mercaptan and ethylene glycol dimethacrylate after heating. The fluorescence intensity of the polymer particles was very weak.

利用邻苯二甲醛与烯丙基硫醇、乙二醇二甲基丙烯酸酯在偶氮二异丁腈引发下热聚合制得了一种新型聚合物颗粒。

When 3-benzoyl-5-formyl-indolizine or ethyl 5-benzoyl-indolizine-3-carboxylatewere used as substrates, a novel coupling reaction occurred, givinghydroxy-cycl[3,2,2]azines. A mechanism of the reaction was proposed.

其中3-苯甲酰基-5-甲酰基中氮茚和5-苯甲酰基-3-中氮茚甲酸乙酯在低价钛试剂的作用下，发生了新奇的偶联反应，得到了用其它方法难以制备的Hydroxy-cycl[3，2，2]azine，并对此现象作了解释。

Do you know, i need you to come back

你知道吗，我需要你回来

Yang yinshu、Wang xiangsheng、Li decang,The first discovery of haemaphysalis conicinna.

1〕 杨银书，王祥生，李德昌。安徽省首次发现嗜群血蜱。