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Combined crystallization kinetics analysis obtained via rheometry and morphological observation of crystals growth performed on POM, two different mechanisms of shear-enhanced crystallization for PP/ grafted MWCNTs composites were suggested:(1) at low temperature, strong heterogeneous nucleation plays a dominant role on the. crystallization behavior, which would be saturated at a higher filler content, and the effect of shear-enhanced crystallization was weak;(2) at high temperature, the effect of heterogeneous nucleation was substantially depressed, and the crystallization of the composite was obviously accelerated by pre-shear and the thread-like crystallites were generated earlier than the spherulites.

结合流变测试结果和热台偏光显微镜观察的结晶形貌发展过程,对于PP/G—MWCNTs体系得到了两个不同的剪切影响机理:(1)在低温条件下,强烈的异相成核作用对结晶行为的影响占主导优势,而剪切作用对结晶的影响十分微弱,同时,在填料含量较高是,异相成核作用具有饱和性;(2)在高温条件下,异相成核作用被抑制,复合体系的结晶主要受到预剪切作用的影响,并且纤维状晶体较球晶更易生成。

An amphiphilic graft copolymer was obtained using a macromonomer method and its aggregate behavior and phase structure in aqueous solutions were studied by tensionmetry, polarized micrography, rotation rheometry and small-angle X-ray diffraction.

采用大分子单体法制备接枝型两亲共聚物,通过表面张力仪、偏光显微镜、旋转流变仪和小角X射线衍射研究了两亲共聚物在水溶液中的聚集行为及其相结构。

The main point of this paper lies in the research on the microstructure of the mullite—cordierite sagger, which has been used in the production of Jingdezhen ceramic industry in large quantities for many years, by means of a polarization microscope with ultrathin section together with close connection of the process in the sagger manufacture.

本文主要是利用偏光显微镜和超薄光薄片并紧密结合匣钵的制造工艺,对景德镇市多年来一直在陶瓷生产上大量使用的&莫来石—堇青石质匣钵&进行了显微结构的研究,发现这种匣钵材料的主晶相是堇青石,次晶相是刚玉和莫来石,并发现其中各晶相成团聚状分布;另外在磨制超薄光薄片过程中,发觉其结构较疏松。

The photographs of polarizing microscope showed the number of spherocrystal was increased and the diameter was decreased after saponification reaction which was agreed with the studies of DSC.

试样的偏光显微镜观察结果表明,醇解后,球晶数目增加、直径减小、完善程度降低。

Microfissures on the rocke moutonnées from the Halasi River Catchment and the source of Urumqi River were observed on the hand-specimen of the bedrock from the ice-rock interface directly and under the polarized microscope and SEM. Parallel microfissures dorminates on the stoss and the top-surface; while irregular microfissures dorminates on the lee.

根据天山乌河河源的羊背石和阿尔泰山哈河流域的羊背石表层岩石手标本上微裂隙直接观察,以及在偏光显微镜下SEM的超微裂隙观察,&阿羊&上的微裂隙多,迎冰面和顶冰面以平行裂隙为主,背冰面以不规则裂隙为主(已剔除可能由构造运动产生的裂隙)。

MAIN OUTCOME MEASURES: Differential scanning calorimeter was used to detect thermotical property; polarizing microscope was utilized for the microstructure observation; Antimicrobial activity and slow-release effect were determined by in vitro bacteriostasis and release, respectively.

主要观察指标:差示扫描量热仪表征其热学性能,偏光显微镜观察微观结构;通过体外释放及抑菌实验检测抗菌活性和缓释效果。

Their thermotropic liquid crystal properties were studied through polarized optical microscopy and differential scanning calorimetry.

通过偏光显微镜和差示扫描量热法对这些化合物的热致液晶性进行了研究。

Their thermotropic liquid crystal properties were studied with polarizing optical microscopy and differential scanning calorimetry.

通过偏光显微镜和差视扫描量热法对这些化合物的热致液晶性进行了研究。

The crystalline morphology of a thermotropic aromatic copolyester with flexible spacer has been studied by microscopy techniques.

采用偏光显微镜、扫描和透射电镜从不同层次的结构水平上研究了含柔性间隔基热致液晶性共聚酯的结晶形态。

The nematic thermotropic liquid crystalline behaviour of ten kinds of PEAs obtained was studied by polarizing microscope , DSC and X-ray diffraction.

用热台偏光显微镜,DSC和X光衍射方法研究了热致液晶的相转变行为,确认了这十种聚酯酰胺均为向列型热致液晶。

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