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Compounds 3a-3d, 4a-4d, 5a-5d, 6a-6e and 7a-7e were prepared with a new efficient method, in which the aromatic amines were diazotized with isoamyl nitrite in EtONa/EtOH under refluxing condition, and mono -, bis -and tetrakis -substituted calix [4] arenes were obtained respectively as main product by diazo-coupling in different molar ratio to calix [4] arene.

一,提出了一个有效的新方法合成含有芳香偶氮基团的杯[4]芳烃衍生物3a-3d;4a-4d;5a-5d;6a-6e和7a-7e:即在非水溶剂乙醇中用亚硝酸异戊酯,在强碱乙醇钠存在下对芳香胺进行重氮化,得到芳香重氮酸盐沉淀,过滤,然后加入杯[4]芳烃的四氢呋喃溶液,通入CO〓气体调节溶液的pH值为7-9,使其发生偶联反应。

Such a process includes the preparation of an initial stabilized peptized solution including a titanium precursor material, an organic solvent, an acid agent, the mixing of said initial solution with a large amount of water, the pH of the obtained intermediate solution being less then 3, subjecting said intermediate solution and its dispersion to a heat-treatment, the exchange of water by an organic solvent with low surface tension to obtain a final solution that is finally dispersed.

这样一种方法包括制备包含钛母体材料、有机溶剂、酸介质之开头的稳定化胶溶溶液,将此起始溶液同大量水混合,所得到中间溶液的pH小于3,使此中间溶液及其分散体系经受热处理,用低表面张力的有机溶剂更换水来获得末了加以分散的最终溶液。

The low temperature will make the Tannin dull while the high temperature veers the wine into a sour soup.

低温会使红酒中的丹宁钝化而高温又会把葡萄酒变成酸汤。

Ceramic bearings can produce oxidation-ho, silicon carbide, silicon nitride and so on, diameter from 3mm-50mm, precision Machinable P0, P6, P5 level; its performance characteristics are: high temperature, oil-free self-lubricating, acid, alkali and salt corrosion , wear resistance, low noise, insulating diamagnetic, since high-speed operation; metal nano-ceramic bearing its production process for a new generation of high content of nano-particles in the heat and pressure infiltration of metal surface is activated to fill the cracks and pits the metal so that 3-5 micron metal surface is more smooth solid surface, greatly reduce the friction, improve Chennai base metals, and greatly increased the life span of bearings, and its characteristics are: long life (as an ordinary stainless steel bearings 2 -- 10-fold), low noise (as an ordinary stainless steel bearings, 70%), wear-resisting, acid, alkali, salt corrosion, high temperature, load large; ceramic bearing and metal nano-ceramic bearing design and development to meet the needs of the market for high-speed, low - noise, high load, the demand for corrosion-resistant; Machinery Production Department to produce aircraft rod end joint bearing, linear guide bearings, the fuel tank of earrings, plastic bearing, non-standard side bearing components, glass door hardware, such as high-precision control products; and provide CNC machining.

陶瓷轴承可生产氧化镐、碳化硅、氮化硅等,内径从3mm-50mm,精度可加工P0、P6、P5级;其性能特点为:耐高温、无油自润滑、耐酸、碱、盐腐蚀、耐磨、低噪音、绝缘抗磁、起高速运转;金属纳米陶瓷轴承其生产工艺为新一代的高含量纳米级微粒在热和压力的作用下被激活渗入金属表面,填补金属缝隙和凹坑,使金属表面3-5微米表面更光滑坚固,大大降低其摩擦力,提高金属的奈酸碱性,并大大提高了轴承的寿命,其特性为:长寿命(为普通不锈钢轴承的2-10倍)、低噪音(为普通不锈钢轴承的70%)、耐磨、耐酸、碱、盐腐蚀、耐高温、负载大;陶瓷轴承与金属纳米陶瓷轴承的设计开发以满足市场对高转速、低噪音、高负载、耐腐蚀的需求;机械生产部以生产机杆端关节轴承、直线导轨轴承、油缸耳环、塑料轴承、非标端轴承零部件、玻璃门控五金等高精度产品;并对外提供数控加工。

Resistance to atracurium as a result of increased drug binding to 1-acid glycoprotein is associated with increased inducible nitric oxide synthase activity and increased nitric oxide levels in plasma.

对于阿曲库铵的阻滞是由于增加了诱导性氧化亚氮合酶活性和氧化亚氮在血浆中的水平从而使阿曲库铵与1-酸糖化蛋白的结合增加的结果。

Upon FGF binding, specific membrane receptors dimerize and autophosphorylate, then activate several downstream signaling pathways including Ras-MAPK.

FGF通过结合细胞表面的FGF受体,使其二聚化并自体磷酸化,活化后的FGF受体具有酪氨酸激酶活性,进而活化胞内下游多条信号通路。

In the case of decorative zinc electroplatings, a further enhancement of the appearance of such substrates in addition to the corrosion resistance imparted is achieved by the passivate film which ranges from a clear bright to a light blue bright appearance simulating that of a chromium deposit or alternatively, a clear light-yellow appearance simulating that obtained by use of prior art hexavalent chromium solutions.

可选择的治疗方法,可进一步遏制卤化物包括氟离子、氯化物和溴化物离子进一步增加了硬度钝化膜以及一个或多个兼容为实现高效润湿剂接触基板对待。现在的发明特别地可适用但是不限制在碱而产生酸非氰化物的锌的治疗使电解沉积传授对被对待的基体改良的腐蚀抵抗和装饰的外表。

The nitrate and chlorate, very volatile, give off brilliant crimson flames and are used in flares, fireworks, and tracer bullet s.

卤化锶、硝酸锶和氯酸锶极易挥发,并能使火焰呈亮猩红色,用于各种照明弹、烟花和曳光弹中。

Feeding for 24h by third instar larvae of the maize stalk borer induced farnesyl pyrophosphate synthase gene expressing, but had no effect on expression of AOC, BX9, PAL and PR2a genes and DIMBOA content.

3玉米螟3龄幼虫处理24h能诱导玉米根中法呢烯基焦磷酸合成酶基因表达,但不能诱导丙二烯氧化物环化酶、β-1,3葡聚糖酶基因(PR2a)、糖基转移酶(BX9)、苯丙氨酸转氨酶基因表达,同时对第二叶和根中丁布含量无显著影响,使第二叶对羟基苯甲酸及第三叶丁布、对羟基苯甲酸、香草酸含量显著降低。

While the sample was dissolved in nitric acid and hydrofluoric acid, the silicon in sample was removed through evaporating in the form of silicon fluoride. As a result, the matrix interference was eliminated, and meanwhile the high blank value as well as the influence on the life span of graphite tubes due to perchloric acid was avoided.

使用硝酸和氢氟酸消解样品,使硅生成氟化硅蒸发掉,消除了基体的干扰,也避免了使用高氯酸作为消解试剂所引起空白值高及对石墨管寿命的影响。

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The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应,而且减少跟风的可能性。

The new PS20 solar power tower collected sunlight through mirrors known as "heliostats" to produce steam that is converted into electricity by a turbine in Sanlucar la Mayor, Spain, Wednesday.

聚光:照片上是建在西班牙桑路卡拉马尤城的一座新型PS20塔式太阳能电站。被称为&日光反射装置&的镜子将太阳光反射到主塔,然后用聚集的热量产生蒸汽进而通过涡轮机转化为电力