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We have studied the electrochemical oxidation reactions of bilirubin, biliverdin, bile-purpurin and choletelin in H〓O+DMF mixed solvent and found that the oxidation reactions of these bile pigments were greatly sped up by the introduction of water into DMF, and discussed the effect of water on their oxidation mechanisms too, and determined the reaction rate constants in the mixed solvent.

利用现场紫外-可见及时间分辨光谱电化学技术,研究了胆红素、胆绿素、胆汁红紫素及胆黄素在DMF+H〓O混合溶剂中的电化学氧化反应,发现由于水的引入,使上述胆汁色素在DMF中的氧化反应大大加快。研究了反应的动力学,首次求出了反应的速率常数。

Highly stable glucose oxidase multilayer films were fabricated on cystamine modified gold electrode surfaces by layer-by-layer self-reaction of periodate-oxidized glucose oxidase.

以胱胺修饰的金电极为基础电极,利用席夫碱反应使经高碘酸根氧化的葡萄糖氧化酶在该电极表面进行自身的层-层有序组装。

The dielectric material is annealed in an oxidizing environment to densify, the barrier layer inhibiting oxidation of the said second sidewall portion of the trench.

介电材料在氧化环境中退火使其致密化,阻挡层阻止沟槽的第二侧壁部分被氧化。

The epoxide-terminated oligomer having ether mesogenic unit wassynthesized for the first time by reacting the diphenol with epichlorohydrin. Theepoxy equivalent increased as the elongation of reaction time or the decrease of theinitial ratio of diphenol and epichlorohydrin, but effect of the reaction time wassmaller than that of the initial ratio.

首次采用直接环氧化的方法合成了含酯类液晶基元的环氧结构预聚物,环氧化反应中反应配比和反应时间会影响产物的环氧当量;缩小反应配比或延长反应时间会使产物的环氧当量增大,反应时间对产物环氧当量的影响较小。5。

Compounds 5, 7 and 8 were obtained from the genus Fraxinus for the first time. Compound 4 showed remarkable antioxidative activity, which was higher than that of VE (35%).

讨论:化合物5,7,8为首次从该属植物中分离得到,其中化合物4在10-6 mol·L-1浓度能使脂质过氧化产物MDA的生成抑制50%以上,强于阳性对照药VE(抑制率35%),具有显著的抗氧化作用。

Tetralin showed synergistic action with hexadecene, which accelerated the oxid ation and increased the hydroperoxide content up to 4.64wt% after 16hr oxidation .

四氢萘与十六烯共存有协同氧化作用,使体系中的氢过氧化物含量在16 h 高达4.64%,氧化深度增大。

The effects of the surfactants, trioctyl phosphine oxide, sodium dodecyl sulfonate and hexadecyl trimethyl ammonium bromide, on the extraction rate of Co^2^+ were investigated. The acceleration in the kinetics in contributed to the associated molecule~2 TOPO taking part in the extraction process directly. The decrement effects of SDS or CTMAB on the rate of extraction kinetics of Co^2^+ with HDEHP were also observed, which caused by the adsorption of molecules of SDS or CTMAB on the interface and decreased the interfacial adsorption amount of HDEHP. In addition, the extraction rate was reduced by a bigger margin in HDEHP-SDS system. This can be explained in terms of the formation of an electric field at the interface.

研究体系中加入不同表面活性剂所引起萃取速率的不同改变:三辛基氧化膦因与HDEHP形成可萃取的Co^2^+活性分子缔合物,降低了萃取过程活化能而使反应加速;十二烷基磺酸钠和十六烷基三甲基溴化铵因占据发生萃取反应的界面区,减小了HDEHP与Co^2^+反应的机会而使反应减速; SDS还因其在界面形成较强的负电场,造成Co^2^+的附加势能而使萃取速率有更大幅度的降低。

Experiment results show, in the HD process, the temperature of dehydrogenation process sets at about 580℃, can make the hydrid of Nd complete turning into NdH_2 which can resist being eroded and oxidation, so it increases the resistance to oxidation of the magnet powders.

研究结果表面,在氢爆HD工艺中,采用580℃左右的温度进行工艺中的脱氢过程,可以使富Nd相氢化物充分脱氢成稳定不易腐蚀氧化的NdH_2,增强了磁粉后续工艺中的抗氧化能力。

Using manganous sulfate solution as precursor, Mn2+ was converted to Mn2 by the addition of ammoni, then Mn2 was oxidized to Mn3O4 with microwave irradiation.The rea-brown Mn3O4 powder was obtained.

论文在微波辅助加热条件下,向净化后的硫酸锰溶液中滴加氨水,使溶液中的Mn2+沉淀为Mn2,利用空气氧化Mn2得到Mn3O4沉淀,过滤,洗涤,干燥后得到棕红色四氧化三锰固体。

Results showed that single ozone oxidation can only remove about 50% nitrobenzol, single active carbon absorption can reduce nitrobenzol to a standard index mark when empty-bed station time exceeded 15 minutes, but ozone oxidation-active carbon absorption technology can remove nitrobenzol completely when the time exceeded 10 minutes.

研究发现:单独采用0 氧化能去除约50%的硝基苯;单独采用活性炭吸附,在空床停留时间大于15 min时可使出水指标达到标准要求;而对于O 氧化一活性炭吸附工艺,当停留时间在10 min 以上时,可完全去除水中的硝基苯。

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This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

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There is no differences of cell proliferation vitality between labeled and unlabeled NSCs.

双标记神经干细胞的增殖、分化活力与未标记神经干细胞相比无改变。