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54 cases' RA activity group compared with 20 cases' relief group and 25 cases' control group, then analyzed the index of patient's condition of RA patients' platelet parameter (ESR、CRP、IgG、IgA、IgM、C3、C4、RF), and associativity of clinical symptom such as arthralgia, arthrocele, subdermal induration, violet and dark oral lip, scaly skin, ecchymosis of corpus linguuae, frequency of petechia.

比较RA活动组54例,缓解组20例和正常对照组25例的血小板参数变化,分析54例活动期RA患者血小板参数与病情活动指标(ESR、CRP、IgG、IgA、IgM、C3、C4、RF)及临床症状(关节疼痛数、关节肿胀数、皮下硬结、口唇紫黯、肌肤甲错、舌体瘀斑或瘀点出现率)的相关性。

Three kinds of small molecular copper and zinc superoxide dismutase mimics were synthesized with N, N-bis (benzimidazol-2-ylmethyl) amine (N3), N, N-bis (benzimidazol-2-ylmethyl) methylamine(MN3) and N,N-bis (benzimidazol-2-ylmethyl) benzylamine(BN3) as ligands. The com-plexes were characterized by UV, IR and element analysis and the structures were proposed.

模拟铜一锌超氧化物歧化酶的活性中心,以二(2-苯并咪唑)丙烷为桥、二(2-苯并咪唑亚甲基)胺(N3)、二(2-苯并咪唑亚甲基)甲胺(MN3)及二(2-苯并咪唑亚甲基)苄胺(BN3)为配体合成了3种异双核的小分子模型化合物,并进行了紫外、红外表征及元素分析,推测了可能的结构。

Starting from 3, 5-dihydroxybenzoic acid, a total of 16 kinds of salicylicaldehyde derivatives have been synthesized by the esterification, substitution, reduction, formylation, condensation, brominate, functional group protection and deprotection reactions, of which 11 have not been reported yet. Enatiomerically pure 2-amino-2'-hydroxy-1, 1'-binaphthyl has been easily obtained from its racemic mixture by the eantioselective formation of inclusion crystals with N-benzylcinchoninium chloride.

树枝状大分子希夫碱三齿手性配体的设计与合成从3,5-二羟基苯甲酸出发,通过酯化、取代、还原、甲酰化、缩合、官能团的保护与去保护等反应合成了四个系列16种水杨醛衍生物,其中11中是未见文献报道的新化合物。

The influence of acidity on fluorescence and absorption spectra were investigated. Using quinine bisulphate as a reference, fluorescence quantum yield of aesculin in the condition of pH=4.96 was determined to be 0.76 at excitation wavelength 335nm, and in pH=9.40 was 0.80 at 375nm.

探讨了酸度与浓度对其荧光和吸光性质的影响,以硫酸奎宁为参比,测得秦皮甲素水溶液的两种强荧光型体的荧光量子产率,在pH=4.96,激发波长335nm条件下,荧光量子产率为0.76;在pH=9.40,激发波长375nm条件下,荧光量子产率为0.80。

The metalorganic complex NaEu4 is prepared by europium and Dibenzoyl Methane. The coordination polymers Eu-DBM-PAA and NaEu-DBM-PSAA are synthesized by the reaction of NaEu4 with polyacrylic acid M(subscript r=5000and copolymer of acrylic acid and styrene M(subscript r=3000.

研究了铕和二苯甲醯甲烷形成的有机配体NaEu4与聚丙烯酸M(下标 r=5000)、聚M(下标 r=3000发生配位反应分别得到配合物Eu-DBM-PAA和NaEu-DBM-PSAA,得率分别为89.7%和87.3%。

The dilative effects of acetylcholine on rat aorta precontracted with NE 0.62 μmol/L were investigated to reflect the changes of dilative functions.

用去甲肾上腺素诱发大鼠离体主动脉环的收缩,反映收缩功能的变化,主动脉环以0.62 μmol/L NE预收缩后用乙酰胆碱舒张对抗,反映舒张功能的变化。

The ultraviolet photosensitive initiating system is composed of 4,4"-bis(N,N"-dimethylamino) benzophenone, 2-chlorohexaarylbiimidazole and a hydrogen donor coinitiator n-dodecyl mercaptan.

用光敏剂4,4′-二(N,N′-二甲基-氨基)苯甲酮、引发剂邻氯代六芳基双咪唑和氢给体助引发剂十二烷基硫醇组成光敏引发体系。

The copolycondensation type polyamic acid was synthesized by using 3,3', 4,4'-Benzophenonetetracarboxylic dianhydride as the dianhydride monomer, 4,4'-Diamino diphenylmethane and 4,4'-Oxydianiline as the diamine monomer under microwave irradiation in Dimethylformamide.

在微波辐射条件下,采用3,3',4,4'-二苯酮四羧酸二酐、4,4'-二氨基二苯甲烷和4,4'-二氨基二苯醚为单体,N,N'-二甲基甲酰胺为溶剂,低温合成一种共缩聚聚酰亚胺的前驱体聚酰胺酸,化学亚胺化脱水环化生成BTDA型共缩聚聚酰亚胺。

O methoxy phenyl lithium reacts with 6,6 dimethyl fulvene to give ligand lithium (Cp ′Li,Cp ′ represents cyclopentadienyl with substituents).

邻甲氧基苯基锂和 6,6-二甲基富烯(或 6,6-二乙基富烯)反应得配体锂盐,Cp′ Li直接和 Cp Zr Cl3· DME反应生成 2个新的锆络合物 Cp′ Cp Zr Cl2 。

There occurred red tides of Gymnodinium sp.

在这个围隔实验的两个围隔体中,分别发生了一种裸甲藻(Gymnodinium sp。

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