体甲

The angular shifting camo pattern of the SPI armor was one part legionnaire mail, one part tactical body armor, and one part chameleon.

SPI盔甲那个有棱角的变化伪装图案是军用铠甲的一部分，一部分是战术体甲，一部变色。

The constituents of bulb of F. puqiensis were studied. Five steroid alkaloids were isolated. The plane structure and stereoscopic configuration of 4 compounds were elucidated. They are named as puqienine A (FP-33), puqienine B (FP-3), N-demethyl-puqietinone (〓 FP-34) and puqietinone (〓, FP-9). Puqienine A and N-demethyl-puqietinone are new compounds. Puqienine B is as same as FPQ-3 elucidated by Prof.

对F.puqiensis鳞茎化学成份进行了研究，分得5个甾体类生物碱成分，并采用 UV、IR、EI-MS、1D-NMR，HHCOSY、CHCOSY、HMBC和X-RAY等光谱技术和理化常数测定，鉴定出4个化合物的平面结构和立体构型，分别为蒲圻贝母碱甲（puqienineA，FP-33）、蒲圻贝母碱乙（puqienineB，FP-3）、N-去甲蒲贝酮碱（N-demethyl-puqietinone，FP-34）和蒲贝酮碱（puqietinone，FP-9），其中蒲圻贝母碱甲和N-去甲蒲贝酮碱为新化合物。

Liaoning Medical University, Jinzhou 121001 China）Abstract:Objective To study the distribution and liver targeting of glycyrrhetinic acid derivatives (stearin glycyrrhetinic acid ester-3-O-galactosidase, Gal-GAOSt) modifying norcantharidin liposomes (Gal-GAOStNC-LP) in rats.

目的 研究甘草次酸衍生物（甘草次酸硬脂醇酯-3-O-半乳糖苷，Gal-GAOSt）修饰去甲斑蝥素脂质体(Gal-GAOStNC-LP)在小鼠体内的分布及肝靶向性。方法利用薄膜分散法制备甘草次酸衍生物修饰去甲斑蝥素脂质体后，经小鼠尾静脉给药，采用HPLC法检测去甲斑

AIM: To isolate bioactive secondary metabolites from the fruits of Schisandra rebriflora Rehd. et. Wils and study their effects on HIV-1 infectivity. METHODS: Inhibition of syncytia formation, HIV-1 reverse transcriptase and protease, protection of HIV-1 infected cells, level of HIV-1 p24 antigen,blockage of fusion were detected. RESULTS: A lignan compound, named rubrifloralignan A, was first isolated as a natural product with modest inhibition effects on syncytium formation and HIV- 1 replication and could protect HIV-1 infected cells with weak inhibition effects on fusion and RT, but it showed no effects on the replication of HIV-1 chronic H9 and PR. CONCLUSION: Rubrifloralignan A is an efficient anti-HIV-1 product with effect on early stage of HIV-1 replication.

目的：从红花五味子果实中寻找活性代谢产物，研究其抗HIV—1活性和作用机制方法：通过合胞体抑制、HIV-1感染细胞保护、HIV—1p24抗原测定、融合阻断、逆转录酶和蛋白酶活性分析等实验，检测分离化合物的抗HIV—1活性并探讨其作用机制一结果：红花五味子甲素能够抑制病毒诱导的合胞体形成，保护病毒感染细胞，抑制病毒在细胞内的复制对HIV-1感染细胞与正常CD4^＋细胞间的融合，逆转录酶活性有一定的抑制作用但是红花五味子甲素不抑制病毒在慢性感染细胞中的复制，也不抑制蛋白酶的活性、结论：首次从天然产物中分离得到红花五味子甲素，它对HIV—1病毒复制早期具有抑制作用

Results show that, by using thionyl chloride and N,N-dimethyl formamide as chlorinating reagent and dichloromethane as solvent and taking -15℃ as reaction temperature, Z-iomer crystals with pale white color and stable to temperature can be obtained with an overall yield of 70%.

以2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酸为原料，经盐酸化、氯代等反应合成了Z-2-（2-氨基噻唑－4-基）－2-甲氧亚氨基乙酰氯盐酸盐；氯代时以用亚硫酰氯和N，N-二甲基甲酰胺的混合物代替五氯化磷作氯化剂，并考察了温度和溶剂对氯代产物中Z-异构体和E-异构体收率的影响。

This work, concentrated on the asymmetric allylation of aldehydes controlled by different chiral auxiliaries prepared from rotational pure tartaric acid, can be divided into three parts.The first part aims to review the developments of chiral drugs and asymmetric synthesis, from which derived the present research topic backgrounds and works.Synthesis and applications of allylation from aldehydes are the second part of the thesis. By optimizing the reaction conditions, such as solvents, temperature, time and chiral auxiliaries like N,N\'-dibenzyl tartamide, N,N\'-p-dimethylphenyl tartamide, N,N\'-o-dimethylphenyl tartamide, N,N\'-o-dichlorophenyl tartamide, N,N\'-a-dinaphyl tartamide, N,N\'-dicyclohexyl tartamide and N,N\'-diphenyl tartamide, ideal experimenttal conditions are obtained according to HPLC monitoring, as well as the auxiliaries\' recoveries experiments. Starting from benzaldehyde and 3-bromopropaldehyde, N,N\'-dibenzyl tartamide is considered the best auxiliary in this reaction.

本文介绍了醛的不对称烯丙基化反应，以光学纯酒石酸为原料，研究了不同构型手性配体在醛的烯丙基化反应中的立体选择性，全文共分三部分十个章节：第一部分对当前手性药物和手性技术进行了概述，并由此展开了本文的研究背景和任务；第二部分为有机合成部分，对醛的不对称烯丙基化反应进行了深入探讨，以苯甲醛为原料对反应条件进行优化，在优化的反应条件下对制备的七种可回收手性酰胺配体(N-苄基酒石酸二酰胺、N-对甲苯基酒石酸二酰胺、N-邻甲苯基酒石酸二酰胺、N-邻氯苯基酒石酸二酰胺、N-a-萘基酒石酸二酰胺、N-环己基酒石酸二酰胺和N-苯基酒石酸二酰胺)进行筛选，优化配体回收实验条件，最终确定出N-苄基酒石酸二酰胺在苯甲醛的不对称烯丙基化反应中具有较大优越性，结晶回收的手性配体光学纯度保持不变。

Compared with the controls, both 10.0-10 000.0 μgL^(-1) of methamidophos and 100.0 μgL^(-1) of 17β-estradiol increased the mean population growth rate significantly.0.1-10 000.0 and 10.0 μgL^(-1) of methamidophos decreased significantly the average ratio of ovigerous to non-ovigerous females and the average mictic rate, respectively, and 1000.0 μgL^(-1) of 17β-estradiol decreased the total resting egg production significantly.

与对照相比，10.0~10000.0μgL^(-1)的甲胺磷和100.0μgL^(-1)的17β-雌二醇均使轮虫的平均种群增长率显著提高；0.1~10000.0和10.0μgL^(-1)的甲胺磷分别显著地降低了实验期间轮虫种群中的携卵雌体数／非携卵雌体数和混交雌体百分率的平均值；1000.0μgL^(-1)的17β-雌二醇显著降低了轮虫的休眠卵总产量。

Methamidophos affected the mean ratio of ovigerous to non-ovigerous females and the mean mictic rate significantly but had less effect on the total resting egg production, while 17β-estradiol was in adverse.

甲胺磷和17β-雌二醇对实验期间轮虫的平均种群增长率均有显著影响，但对轮虫种群中的混交雌体受精率的平均值无显著影响；甲胺磷对实验期间轮虫种群中的携卵雌体数／非携卵雌体数和混交雌体百分率的平均值均有显著影响，而17β-雌二醇则无显著影响；甲胺磷对实验期间轮虫的休眠卵总产量无显著影响，而17β-雌二醇的影响较显著。

That, and smashing trees with his ball and chain doesn't compare to the satisfying crunch it makes when it bashes into DECEPTICON armor.

还有就是，他感到当自己用流星锤痛击霸天虎时，那体甲的碎裂声远比砸烂树木的感觉更爽。

Synthesis and structural characterization of novel cycioplatinated complexes with 2-aryl imidazolines 2-arylimidazoline ligands 2a-2d were synthesized from benzoyl chloride or p-methoxybenzoyl chloride with aminoethanol or valinol and 2e was synthesized from 2-phenylimidazoline.

新型2-芳基咪唑啉环铂化合物的合成与结构表征以苯甲酰氯或4-甲氧基苯甲酰氯和氨基醇(2-氨基乙醇或外消旋的缬氨基醇)为原料，合成了四种2-芳基咪唑啉配体2a-2d，以2-苯基咪唑啉为原料合成了配体2e，其中2d为新化合物。

Neither the killing of Mr Zarqawi nor any breakthrough on the political front will stop the insurgency and the fratricidal murders in their tracks.

在对危险的南部地区访问时，他斥责什叶派民兵领导人对中央集权的挑衅行为。

In fact,I've got him on the satellite mobile right now.

实际上 我们已接通卫星可视电话了