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To avoid the serious electromagnetic interferer, the analog signals are transformed to frequency pulses which are transferred to the kernel of the system. In the measure of the groove voltage, the method of float-ground is adopted to avoid the high common signal and the range switch circuit is designed to solve the conflict of the wide dynamic range and the high precision. least square Curvefit is adopted to reduce the system error.

铝电解生产现场电磁干扰非常严重,为此我们将需要测量的模拟信号就近转换为频率脉冲后再传送到控制核心;采用浮地接入方式消除槽电压信号中的共模成分;设计了量程自动切换电路以解决槽电压的动态范围宽和测量精度高的矛盾;用最小二乘法进行曲线拟和以降低测量的系统误差。

The company has a 30- year history of producing electrolytic Manganese Dioxide.

公司有30余年的电解二氧化锰生产历史,公司以先进的生产技术为基础,以丰富的锰矿资源为依托,加上廉价的劳动力成本,产品深受用户好评。

In this process, the discharge process of single point to point contact is transformed to the process of both point to point contact and the overall surrounding contact of sphere Ni through the self redox reaction, thus making a highly efficient electron transfer process. In this dissertation, the catalytic electrolysis mechanism is discussed. The influence of various parameters (e.g. kind and concentration of catalyst, reaction temperature and electrolysis duration) on electrolysis were investigated.

本文首次提出了以KMnO_4为代表的高锰酸盐作为电解过程电子传递的媒介,通过锰盐自身氧化还原反应的参与,在阳极和溶液中的球形Ni_2之间建立起高效的电子转移过程,使球形Ni_2和阳极之间单一的固体之间的点点接触放电,转变为点点接触放电和球镍与溶液全方位包围接触放电过程,大大提高了电解过程的效率。

We used ITO glass substrate and high purity(99.99%) titanium , put to use sputtering process, add to high purity O2 make it complete the best structure film and the thickness about 1400 . By way of 500℃ anneal could got a better anatase phase, this result could easy reaction with electrolyte to increase electron-transferred. Used as spin casting covering PR on ITO substrate, transferring patterns of array circular shapes on a mask to photography, used optimize temperature and time to hard bake. Finally used HCl to etching underexposed TiO2 area, and acetone to tripper top PR, make it to accomplish pillars shape TiO2 electrode.

本研究使用ITO玻璃基板为底材在以高纯度钛(99.99%)为靶材,利用溅镀方式通入纯氧使其行成高纯度TiO2镀於ITO基板上行成厚度约1400的薄膜,且经500℃高温烧结使其行成最强的锐钛矿结晶相,此晶相有利於与电解液反应进而增加电子的转移,提升太阳能电池最佳的效率,在以旋转涂布方式铺上光阻,以矩阵排列的圆孔光罩曝光、最佳的温度及时间来烘烤、显影后;使用盐酸以等向性湿蚀刻方式蚀刻未曝光之TiO2区域,最后利用鈵铜将最上层光阻去除,使其行成柱状TiO2的电极。

Effects of water,low-concentration calcium lignosulphonate and nitric acid pretreatments on electrokinetic processes of electroplating sludge were investigated.

以风干电镀污泥为电动处理试验材料,水为阳极电解液,柠檬酸-柠檬酸铵缓冲液为阴极电解液,施加25 V直流电压条件下电动运行5 d,研究了水、低浓度木钙和硝酸等预处理对电镀污泥电动过程的影响。

The anodization utilizes an electrolytic solution which etches out oxidized portion as soon as it is formed as a result of the anodization, to thereby develop a porous layer in a pattern in match with the anode pattern.

阳极化利用了电解液,一旦由于阳极化而形成氧化部分,电解液即蚀刻掉氧化部分,由此以与阳极图案相匹配的图案产生多孔层。

According to the spirit of the CPC Central Committee 11th Five-Year Plan, the construction of a harmonious society, the construction of a conservation-oriented, sustainable development, appointed in accordance with the spirit of national wall materials innovation, protection of land cancellation clay brick, the protection of land resources, development of energy-saving and environment-friendly, high-strength lightweight wall Materials, the company's newly developed hollow plaster mold block and complete sets of equipment, in my mature technology companies plastic-and complete sets of equipment, in my mature technology companies plastic | mold and complete sets of equipment, to a mature technology company Plastic mold material, not the characteristics of gypsum, one stroke Zhigao Dian occupied the same industry, the technology to declare national patent for power plants, DAP plants, steel, electrolytic aluminum plant, the flow from gypsum, phosphogypsum, Fly ash, to solve a difficult problem, recycling-and created a good profit.

根据党中央十一五规划精神,建造和谐社会,建造节约型,可持续发展国家,根据国家墙改委精神,保护土地取消粘土砖,保护土地资源、发展节能型,环保型,轻质高强墙体材料,本公司最新研制的空心石膏砌块模具及成套设备,以我公司成熟的技术塑胶聚及成套设备,以我公司成熟的技术塑胶|模具及成套设备,以我公司成熟的技术塑胶模具材料,不占石膏的特点,一举占领了同行业至高点,本技术以申报国家专利,为发电厂、磷酸二铵厂、钢厂、电解铝厂、脱流石膏、磷石膏、粉煤灰,解决了一大难题,变废为宝,创造了可喜的利润。

Simulated wastewater of reactive light-yellow K-4G dyes was treated by manganese ore cooperated with electrochemistry.

以活性嫩黄K 4G模拟废水为处理对象,采用软锰矿与电化学协同法,分别在不同软锰矿加入量、电流密度、pH值、电解时间、染料初始浓度条件下进行电解实验,考察了各种因素对脱色率的影响。

Respectively proceeding with bromine complexing agent of anode, modified membrane and electrolytic additive of cathode, mainly referring to specific power of battery, ratio of self-discharge and zinc dendrite, this paper has studied the influences of different anode additive and modified membrane on specific energy of battery by means of charge and discharge curves, and the influences of electrolytic additive(NH4+, OP-10, TX-10 and dodecyl trimethyl ammonium bromide) on zinc dendrite by means of current-time curve and microscopic morphology observation.

本文分别从正极溴络合剂、隔膜改性和负极的电解液添加剂入手,以电池的比能量、自放电率以及锌枝晶生长情况为主要的性能指标,用电池充放电曲线等方法研究不同正极添加剂和隔膜改性对电池比能量的影响;用电流-时间曲线以及微观形貌观察等方法研究电解液添加剂(NH_4~+、OP-10、TX-10以及十二烷基三甲基溴化铵)对锌枝晶生长的影响。

The main research work of this dissertation is as follows: Based on the chemical reaction engineering theory and the nitrobenzene electroreduction mechanism, the plate and frame electrolyzer was designed and applied to the process of electroreduction nitrobenzene to p-aminophenol. This dissertation measured the residence time distribution data of the electrolyzer by means of the pulse response method and studied the rule of flow pattern along with the current capacity change. Under different conditions ,this dissertation studied the cyclic voltammetry properties of nitrobenzene on different electrodes by means of the dynamic cyclic voltammetry method and the electrode materials applied to the NB electroreduction have been selected primarily.Baseed on the results of cyclic voltammetry tests, this dissertation used p-electrode systems to measure the steady-state- polarization curves of nitrobenzene on different electrodes in H-type diaphragm cell, and obtained each primary factor s influence rule and the exchange current density value of each electrode.And then on the basis of the conclusions of fundamental researchs upword, the effects of influence factors on the the yield of p-aminophenol and the current efficiency,such as electrode material, current density, quantity of electricity circulated, nitrobenzene concentration . sulpuric acid concentration and so on, have been studied in detail in the systems of hign temperature , strong acidity and oxygen-poorthrough a series of electrolysis experiments in this paper.After all using Pb as anode Monel metal as cathode Dupont Nafion 417 cation-exchange membrane as membrane, this dissertation obtained the optimum technological condition: reaction temperature about 85C, current density 500A m-2, sulphuric acid concentration 20%wt.

论文的主要研究工作为:运用化学反应工程理论,结合硝基苯的电还原机理,设计出用于硝基苯直接电还原合成对氨基苯酚实验的板框式电解槽,并利用脉冲响应法测定了该板框式电解槽的停留时间分布数据,研究了流型随流量变化的规律;通过动态循环伏安法研究了硝基苯在不同电极上、不同条件下的循环伏安特性,初步评选出了用于硝基苯电还原的电极材料;结合循环伏安的测定结果,在H型隔膜电解槽中采用三电极体系测定了硝基苯在不同电极上、不同条件下的稳态极化曲线,得到了各主要因素的影响规律及硝基苯在各个电极上电还原的交换电流密度数值;在基础研究结论指导下,采用板框式电解槽,在高温、强酸、贫氧系统中,进行了一系列的电解实验,分别考察了电极材料、电流密度、通电量、硝基苯浓度、硫酸浓度等因素对收率及电流效率的影响,最终选择以蒙乃尔合金电极作为阴极、铅合金为阳极、Dupont Nofion 417阳离子交换膜为隔膜,得到由硝基苯直接电还原制对氨基苯酚的最佳电解工艺条件:反应温度85℃,电流密度500A·m~(-2),硫酸浓度20%wt。

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