产物

Second, using DBU as the base for enolization of propargylic esters of unsaturated acids 18e-k, we developed a tandem Ireland-Claisen rearrangement /isomerization reactions. It has been shown that the reaction sequence affords triene molecules 42a-b and 43a-b in moderated to high yields. Interestingly, with allyl hexa-3,5-dienoates 18i-j as the substrate, the rearranged products underwent further aromatization to give uniquely substituted benzyl acids 44a-b.

其次，以含有活泼质子的烯酸炔丙酯18e-k为底物，在DBU为烯醇化碱、TMSCl为硅试剂的条件下，底物18e-h发生了Ireland-Claisen重排/异构化串联反应，得到完全共轭的三烯类化合物42a-b及43a-b；而以己二烯酸炔丙基酯18i-j为底物时，重排/异构化后的产物进一步发生电环化等反应最终得到芳构化产物——取代苯甲酸类化合物44a-b。

Thus, the mutant amplification products were made of mostly double-stranded DNA, while the wild-type products were made of mostly unconsumed single-stranded DNA.

突变型样品扩增产物中大部分是双链DNA；而野生型样品由于不能被顺利扩增，产物中大部分是单链DNA。

Fangzheng as understratum from the start of the RIP developers, after 30 years of unremitting efforts, the brand products fangzheng century RIP has become a domestic market mainstay RIP products are widely used in a variety of output Center, the seihan Center, Business card printing and membership card production plants and so on.

耿介作为从底层做起的RIP斥不天商之一，经过30年的不懈发奋，其品牌产物耿介世纪RIP还来成为长远国边阛阓上的干流RIP产物，普及搁置于各栽输不入洋心、制版洋心、制卡和会员卡制作厂等。

In this paper, the progresses acquired in the studies of natural analogy are summarized, including a comparison of structural properties, radiation damage and chemical composition between uraninite and UO2, combination and paragenesis of alteration products of uraninite, chemical composition of uraninite and its secondary phases, mobility of analogy elements in the process of uraninite alteration. In addition, the problems in next studies are pointed out, e. g., characterization of micro-structure of secondary uranium minerals, high-resolution analyses of trance elements distributed in original and secondary uranium minerals using laser microprobe analyzer, composition of underground water, simulation experiments.

系统地总结了天然类比研究的现状，包括沥青铀矿与UO2的可比性、沥青铀矿风化产物的共生组合和共生次序、沥青铀矿及其风化产物的化学成分特征、沥青铀矿风化过程中类比元素的迁移性等；并初步指出了进一步研究的方向，如铀酰矿物的微结构研究、类比元素在沥青铀矿和铀酰矿物中分布的激光探针研究、地下水成分分析、模拟实验等。

Urushiol can be used as the basic raw material to develop economic and practical coating with good resistance to high temperature alkaline solution. Thus the polymer precursor was prepared using the polymerization of urushiol and formaldehyde. Then the urushiol-titanium chelate polymer (urushiol-Ti resin) was synthesized by way of the reaction of tetrabutyl titanate with the polymer precursor. The prospective target product was analyzed by means of high-performance liquid chromatography and Fourier transformation infrared spectroscopy.

为开发经济实用的耐高温碱水漆酚钛清漆，以漆酚为基本原料，先通过漆酚与甲醛缩聚，再将钛酸丁酯与前期合成产物反应，从而合成出了漆酚－钛螯合高聚物，并通过高效液相色谱和傅立叶红外技术检测了预期产物的合成情况。

Veratrum aldehyde synthesis of many drugs intermediates, methyl aldehyde method for raw materials in Champlain, after dimethyl sulfate methylation available to 20% sodium hydroxide as the solvent, 10-11 in the PH value of the under the conditions of synthesis; microwave irradiation is the use of microwave radiation heating to replace the traditional approach to synthesis of a product of methylation reactions, this method does not require solvents, and less by-products, but still need to use 15% sodium hydroxide to adjust pH.

藜芦醛是许多药物合成的中间体，甲基化法以香兰醛为原料，经过硫酸二甲酯甲基化可得，以20%氢氧化钠为溶剂，在PH值为10-11的条件下合成；微波辐射法是利用微波辐射代替传统加热方式进行甲基化反应合成产物，这种方法不需要溶剂，并且副产物少，但仍需要用15%氢氧化钠来调节酸碱度。

The results of the rule of law with ordinary methylation by formaldehyde Veratryl three groups the average weight of 2.5609g, the average yield was 91.31%, the melting point of the three groups were 42.4 ~ 44.8 ℃, 41.5 ~ 45.2 ℃, 41.7 ~ 44.3 ℃, from the results of we can see that the three groups of the melt from the melting point greater than that which the product of the by-product of the detection of the melting point have a certain impact; and the legal system with microwave radiation by an average of Veratrum aldehyde quality 1.4016g, the average yield was 93.23 %, melting point of the three groups were 41.8 ~ 43.2 ℃, 41.3 ~ 42.6 ℃, 41.6 ~ 43.5 ℃, melting away from the three groups as compared with ordinary methods of measuring the melt-out from the small.

结果 用普通甲基化法制出来的三组藜芦醛平均质量为2.5609g，平均产率为91.31％，三组的熔点分别为42.4～44.8℃，41.5～45.2℃，41.7～44.3℃，从结果可以看出，三组熔点的熔距都比较大，证明产物当中的副产物对熔点的检测有一定的影响；而用微波辐射法制出来的藜芦醛平均质量为1.4016g，平均产率为93.23％，三组熔点分别为41.8～43.2℃，41.3～42.6℃，41.6～43.5℃，三组熔距较普通方法测出来的熔距小。

Porous and round particulates are related to the high temperature industrial process, strongly weathered minerals originate from crustal composition, and well-grown crystals may result from chemical reactions in the atmosphere.

矿物微形貌特点和矿物组成揭示了降尘组分主要来源于3种途径：与高温过程有关的工业活动排放的产物，自然成因和大气化学反应的产物。

Study on the factors affecting the productivity of porous silica powder prepared from wollastonite;2. The influence of current density on yield, productivity and degree of graphitization of .

研究了放电时的电流值对产物的产量和产率以及对产物石墨化程度的影响，结果表明在20A-50A范围内随着电流强度的增大OLFs的产量和产率都有不同程度的提高。

The optimum condition of PWF prepared fromliquefied wood is: actual pH of liquefied wood without extra acid, 105℃, 150min and 0.7～0.8of ratio of formaldehyde to phenol.

木材液化产物制备PWF的适宜工艺参数为：pH为木材液化产物的实际值，温度105℃，时间150min，n∶n=0.7～0.8。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。