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To improve the yield of an Amide-type Tripodal Ligand and investigate its coordination with rare earth ion under mild condition,a series of Amide-type Tripodal Ligands(L1—L4) have been prepared by the reactions of nitrilotriacetic acid and oxalyl chloride with four kinds of amides,respectively.

为了提高酰胺型三脚架型配体的产率,进一步研究其与稀土离子的配位形式及配合物的荧光性能,以氨三乙酸为母体,草酰氯为氯化试剂,与4种胺在较温和的条件下合成了具有三脚架型结构的配体(L1—L4),并考察了实验条件、反应温度、反应体系溶剂、缚酸剂、反应时间及催化剂对反应产率的影响。

Kinetic spectrophotometric method for the determinationof trace nitrilotriacetic acid;2. To improve the yield of an Amide-type Tripodal Ligand and investigate its coordination with rare earth ion under mild condition,a series of Amide-type Tripodal Ligands(L1—L4) have been prepared by the reactions of nitrilotriacetic acid and oxalyl chloride with four kinds of amides,respectively.

为了提高酰胺型三脚架型配体的产率,进一步研究其与稀土离子的配位形式及配合物的荧光性能,以氨三乙酸为母体,草酰氯为氯化试剂,与4种胺在较温和的条件下合成了具有三脚架型结构的配体(L1—L4),并考察了实验条件、反应温度、反应体系溶剂、缚酸剂、反应时间及催化剂对反应产率的影响。

Average milk yield of the 348 primiparous cows that completed the first lactating period (305 d) was 7 328 kg in the farm adopting the new model, which increased about 576 kg compared with the traditional ones (6 752 kg).

实施后备牛专业化饲养的奶牛场,已完成胎次产奶(305 d)的348头初产牛平均产奶量为7 328 kg,比传统饲养条件下的6 752 kg增加576 kg。

The high activity can be attributed to the following factors: 1 Because of the perovskite structure of the host materials, the positive and negative electric charge center is not superposable, and there is a electric field which can separate the photo generated electrons and holes efficiently in the microscopic field.

以层状基质热稳定性分析为依据,经过对制备方法的优化,在不同温度下进行硫化处理,在对催化剂进行产氢性能研究时发现,在以硫化钠和亚硫酸钠为牺牲剂的产氢体系中,插入硫化镉的复合层状催化剂负载一定量铂以后,具有较高的连续的光催化分解水的能力。

In this way,after the viscosity or apparent viscosity of virgin crude,corresponding unsheared PPD-beneficiated crude and the sheared PPD-beneficiated crude at a certain temperature are determined,the parameters in the model can be calculated.

按照此方法,只须测定一定温度下空白原油的粘度或表观粘度、未剪切时加剂原油的粘度或表观粘度,及在某一个剪切温度下及某一个粘性流动熵产条件下原油的粘度或表观粘度,即可近似确定该数学模型中的参数,从而预测在不同温度时剪切后的原油在该温度下的粘度或表观粘度。

At the situation of keeping the concentration of inocula constant, comparing the influence of two concentrations, 6% and 7.5%, on COD removal rate, volume gasproduction rate and total gas yield, the results indicate that the concentration of 7.5% is better.

在接种物浓度一定的条件下,通过比较6%、7.5%两种不同发酵液浓度对COD去除率、容积产气率及总产气量的影响,结果表明,从整个反应过程变化趋势来看,发酵液浓度为7.5%的处理产气效果好。

The biomass shredding system was finally achieved through many practices and improvements, including the primary shredder, the fine shredder and the cyclone dust collector used as collecting device. The results indicated that the particle size of the primary shredded biomass was about 10mm with the production of 200kg/h, and that of the fine was between 0.177 mm and 0.125mm on different working parameters with the highest production of 160kg/h.

最后通过实践探索出一套集生物质粗、细破碎和利用旋风除尘器作为收集装置为一体的破碎系统,其粗破碎产物长10mm左右,产率为200kg/h;在不同系统工作参数下,细破碎产物粒径在0.177mm(80目)~0.125mm(120目)间可调,粒径为0.177mm时产率为160kg/h。

Packaging business card printing and membership card making enterprise problem is different, the CTP does for packing business card printing and membership card making high-quality printing, such as mesh point of reducing passbys can be produced by more than the traditional print version of dot, richer figure, image level, so that the packaging business card printing and membership card making quality be increased; the digital prepress production once-version, eliminating film at work affected by environmental pollution by dust, so that the printed matter almost no stains, suites a cleaner, clearer, and so on, these advantages, there is no dispute, but the point is, since the packaging business card printing and membership card making products with other color business card printing and membership card making products product characteristic of the existence of a certain amount of difference, is targeted at users of the product quality requirements there are differences, as opposed to traditional prepress production, CTP and could not make the packaging of quality drastically improved, more specifically, this investment can not be brought in a chip based on such an idea, a lot of packaging business card printing and membership card making business-to-there is currently no intention of buying the CTP, and some even think that C under P on packaging business card printing and membership card making enterprise is the only additions to make amends for whitly the number but need to.

包装制卡和会员卡制息企业所沉思的题纲不离有所不同了,CTP不实能为包装制卡和会员卡制息不求应矮品格的印版,比如网不背还原性较好,能爆不收比古板印版更锐冻的网不背、更丰裕的图,的图象条理,从而使包装制卡和会员卡制息品格度获得提矮;印后数字冻不入产一次不败版,制止了胶片在处事洋施境况尘埃的浑浊,使印品实在无不净不背,版背更肮脏、更澄辉等,这些劣势是操纵任何争议的,但关脚是,由于包装制卡和会员卡制息品与其他不黑白制卡和会员卡制息品在产物特不背上活命肯定的不同,所针差的用户差产物品格请求活命不同,不绝差于古板印后不入产的印版,CTP并不克不及使包装的品格爆不收较不小的改善,更不确不天说,此项加入不克不及不败为排斥更多客户的不现款,基于这样一种思绪,许多包装制卡和会员卡制息企业到不幼久还操纵采办CTP的意向,有的甚至觉得C下P差包装制卡和会员卡制息企业是只不赔不赔的交往,最多也只是范畴必给而已。

Under the condition of the same materials of 600 grams, the biogas production of the treatment with 480 grams food waste inoculated with 120 grams inoculums(TS ratio 9.47 of food waste and inoculum) was 9359 mL which was larger than that of any other treatment significantly. The reduction effects of TS, VS and CODCr were also the best, and the reduction rate was 60%, 70% and 39.67%, respectively. However, there was no significant difference in CODCr reduction compared with CK which was not inoculated.

其中,在消化物总量600 g条件下,480 g餐厨垃圾接种120 g接种物(TS比为9.47)产气效果最佳,整个过程累积产气量为9359 mL,显著高于其它处理,此外,餐厨垃圾TS、VS去除率和消化液CODCr去除率也达到最佳效果,去除率依次为60%、70%和39.67%,但是CODCr去除率与CK差异不显著。

The paper involved two parts: Part 1: A two-chambered microbial fuel cell was constructed with high-concentration sodium acetate as fuel in the anode. The influence of different electron acceptors in the cathode, external resistance value, pH value and concentration of sodium acetate on electricity generation in MFC was investigated. The result showed that the maximum power density of 294.72 mW/m2 and the coulombic efficiency of 25.87% was achieved at sodium acetate concentration of 6.46 g/L, pH 7.0, external resistance 500Ωin the anode and when using potassium permanganate as electron acceptor in the cathode.

全文分为两个部分:第一部分:以乙酸钠为阳极原料构建双室微生物燃料电池,研究不同阴极受体、外接电阻、乙酸钠浓度和pH等因素对电池产电性能的影响,研究结果表明:在500mL的阴阳极反应体系中,选用乙酸钠作为阳极底物,质量浓度为6.46 g/L, pH 7.0,接入500Ω外电阻,阴极电子受体选择高锰酸钾的情况下,微生物燃料电池产电性能最好,最大电功率密度达到294.72 mW/m2,库伦效率能达到25.87%。

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The split between the two groups can hardly be papered over.

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