交酯

MATERIALS: Paclitaxel degradable material (PLLA:PGA=9:1) were offered by Changchun Applied Chemistry Institute of Chinese Academy of Science. Human umbilical arterial smooth muscle cells were purchased from Baster, Wuhan, China.

材料：紫杉醇可降解材料（左旋丙素酯与聚乙交酯的比例为9：1）由中国科学院长春应用化学研究所提供。

When lactide was purified byethyl acetate for 4 times, it was pure enough to polymerize to be PLA.

以乙酸乙酯作为重结晶溶剂，当重结晶次数达到四次后，其纯度已达到丙交酯聚合的基本要求。

This paper describes the studies on consistency of directed interesterified oil in medium scale production test for producing margarine and shortening by directed interesterification method with lard and rapeseed oil, palm oil and rapeseed oil, chinese vegetable tallow and rapeseed oil, as well as lard itself.

本文对猪油与菜油、棕榈油与菜油、乌桕油与菜油以及猪油为原料的定向酯交换法生产人造奶油、起酥油中间试验产品，交酯油的稠度进行了研究。作者按照IUPAC中熔化膨胀法，测定了55个试样的熔化膨胀度；然后把必要的值换算成SFC，并做出了SFC曲线。

The synthesis, characterization and polymerization of a new cyclic 6-(N-isopropyl acylamine ethylidene)-ε-caprolactone were reported.

研究了官能团化新型己内酯单体的合成及其与丙交酯无规共聚物的降解性能。

Firstly, D,L-lactide was synthesized from D,L-lactic acid with zinc powder as catalyst,and glycolide from glycolic acid using Sb2O3 as catalyst.

首先以乳酸为原料，锌粉为催化剂合成了丙交酯；以乙醇酸为原料，三氧化二锑为催化剂合成了乙交酯。

The resulted D,L-lactide and glycolide were found to have ring structure by fourier transform infrared spectrometry and proton nuclear magnetic resonance(1H NMR) spectrometry.

通过傅立叶红外光谱和氢核磁谱(1H NMR)测试表明所合成的丙交酯和乙交酯具有环状结构。

Then two star-shaped oligomers with designed molecular weights 5000 g mol-1 and 10000 g mol-1, respectively, were synthesized from D, L-lactide and glycolide as raw materials and pentaerythritol as initiator under catalysis of dibutyltin oxide.

以合成的丙交酯和乙交酯为原料，季戊四醇为引发剂，氧化二丁基锡为催化剂合成出设计分子量为5000和10000两种预聚物。

The PDLLA with a viscosity average molecular weight beyond 20×10~4 was obtained under the optimum synthesis conditions of the lactide after being recrystallized 4 times as the monomer,the vacuum level of 0.098 MPa,reaction temperature of 150-160 ℃,reaction time of 6-8 h,and using 0.1%-0.18% stannous octoate as catalyst.

实验结果表明，重结晶4次后的丙交酯作为单体，在辛酸亚锡摩尔分数为0.1%—0.18%，真空度0.098 MPa，聚合温度150—160℃下聚合6—8 h可获得粘均相对分子质量Mη大于20×104的聚D，L-丙交酯。

The morphologies formed were characterized by SEM and DLS methods, and spherical particles with various sizes were observed.5. To obtain a amphiphilic dumbbell-shaped copolymer, we successfully synthesized dendritic-linear-dendritic triblock copolymers composed of linear polystyrene and poly dendrons.

树枝状共聚物最外层PSt-PNAS链段利用乙二胺和NAS活性酯的取代反应交联，同时，中间的聚丙交酯段被降解，得到纳米空心球，用SEM和DLS进行观测和表征。5。

In the preparation method, primary soybean oil and deep hydrogenation soybean oil, or primary rapeseed oil and deep hydrogenation rapeseed oil are adopted as raw materials; sodium methoxide is selected as a catalyst; the consumption of the catalyst is 0.1 percent to 0.5 percent; the reaction temperature is 70 DEG C to 110 DEG C; therefore, the primary soybean oil and the deep hydrogenation soybean oil, or the primary rapeseed oil and the deep hydrogenation rapeseed oil have randomized lactide reaction for 10 min to 90 min, so as to change the composition of mixed oil triglyceride and obtain the low/zero trans fatty acid base oil with different melting points and the characteristics of solid fat.

本发明以一级大豆油和极度氢化大豆油，或一级菜籽油和极度氢化菜籽油为原料，选择甲醇钠为催化剂，催化剂用量0.1％～0.5％，反应温度70～110℃，使一级大豆油和极度氢化大豆油，或一级菜籽油和极度氢化菜籽油之间进行随机交酯化反应，反应时间10～90min，从而改变混合油甘三酯组成，得到具有不同熔点和固体脂肪特征的低/零反式脂肪酸基料油。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。