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Furthermore,using oxaldehyde,make the emulsion crosslinked and form a kind of net structure,thus a new kind of water-resistant adhesive is created.

通过醋酸乙烯酯共聚改性的方法,用醋酸乙烯与丙烯酸系单体共聚,采用无皂乳液聚合,然后用乙二醛交联,使乳液形成网络结构,制备了一种新型耐水性胶粘剂,研究了共聚单体对乳液性能的影响,并采用DSC、透射电镜等对乳液结构及性能进行了测试。

A new kind of non-formaldehyde water-resistant emulsion is prepared by modifying polyvinyl acetate with the surfactant-free copolymerization to polymerize vinyl acetate and the acrylic acid monomers,and then by using oxaldehyde to make the emulsion crosslinked to form a kind of net structure.

通过醋酸乙烯酯共聚的改性方法,用醋酸乙烯与丙烯酸系单体共聚,采用无皂乳液聚合,后用乙二醛交联,使乳液形成网络结构,制备了一种无甲醛的新型耐水性乳液。

Ti-PILCs were also obtained with pillaring agent prepared from Ti(n-C4H9O)4 and HC1 by Sol-Gel, using purified Na-montmorillonite in Hubei as the starting clay.

以鄂东钙基膨润土经提纯钠化后所得的精制钠基蒙脱石d_(001=1.28nm为基质粘土,以钛酸正丁酯[Ti(n-C_4H_9O)_4]为钛源,采用溶胶—凝胶法制备了一系列钛交联蒙脱石纳米复合材料;并对Ti/土比、H/Ti摩尔比和盐酸浓度等主要合成条件进行了讨论。

Coating-sand bonding strength is further increased through the esterification linking reaction between polyhydric alcohol and polyacrylic acid.

通过多元醇与聚丙烯酸的酯化交联反应使涂砂结合强度进一步提高。

The in vitro degradation of the crosslinked composites formed by unsaturated polyphosphoester N-vinyl pyrrolidone and β-tricalcium phosphate was investigated and the surface morphology of degradation sample was imaged by scanning electron microscopy.

研究了不饱和聚磷酸酯、N-乙烯基吡咯烷酮与β-磷酸钙交联复合体系的体外降解过程,并用扫描电镜观察了降解一定时间后试样表面的形貌结构。

The in vitro degradation of the crosslinked composites formed by unsaturated polyphosphoester、N-vinyl pyrrolidone and β-tricalcium phosphate was investigated and the surface morphology of dagradation sample was imaged by scanning electron microscopy.

研究了不饱和聚磷酸酯、N-乙烯基吡咯烷酮与β-磷酸钙交联复合体系的体外降解过程,并用扫描电镜观察了降解一定时间后试样表面的形貌结构。

In this paper, the orthogonal experimental analysis method is used to study on the effects of molar ratio of the unsaturated vinyl monomers, with carboxylic groups or sulphonic groups or polyoxyethylene side chain groups,etc., and the effects of the mean degree of polymerization in PEO side chains.

根据聚羧酸系高效减水剂的结构特点,采用正交试验分析法,分别研究了带羧基、磺酸基、聚氧化乙烯链酯基等活性基团的不饱和单体的物质的量之比及聚氧化乙烯链的聚合度等因素对聚羧酸系减水剂性能的影响,从而得出合成聚羧酸系高性能减水剂的一种最佳配方,并对试制产品进行了性能试验。

The mechanical properties ofP/PU SEN increase synergically,compared with thatof composition superposition when PU content is high.

力学性能测试结果表明,在各种交联剂量下,聚丙烯酸丁酯/蓖麻油聚氨酯SEN均在蓖麻油聚氨酯含量较高时力学性能呈协同增加。

Three results are obtained by an orthogonal experiment. The main components of essential oil in separating containerⅠare terpenoid, terpeneless compound is in separating container Ⅱ. Through second-level separation the technological conditions of de-terpene are: pressure 7MPa, temperature 32℃ in separating containerⅠ;pressure 4~5MPa, temperature 32℃ in separating containerⅡ. The optimum technological parameters of obtaining two essential oils are: particle size 0.60mm, pressure 10MPa, temperature 36℃, operating time 90 minutes. There are 1.46% and 1.88% essential oil in separating containerⅠand Ⅱ respectively.

通过正交试验表明:分离器Ⅰ中精油的主要成分是萜烯烃类化合物,分离器Ⅱ中精油的主要成分是由高级醇类、醛类、酮类、酯类等组成的含氧化合物;二级分离脱萜的适宜参数是:分离器Ⅰ的压力为7MPa,分离器Ⅱ的压力与循环压力相同,温度都为32℃;同时得到萜烯烃类精油和低萜精油的最优工艺组合是粒度0.60mm,萃取压力10MPa,萃取温度36℃,萃取时间90min,精油得率分别为1.46%和1.88%。

The dehydrating agent and the dehydrating condition on removal of trace water in the synthetic solution of triethyl orthoformate were investigated.

研究了原甲酸三乙酯一步法合成反应中脱除微量水分的脱水剂和脱水条件,通过正交实验确定了脱水的最优化工艺条件。

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