交酯

Calcium carbonate and soluble glass and so on were confected as alkaline antifouling agent. The Infrared Spectrometry results showed that 2275-2250 cm~(-1) diagnostic absorb wave crest in part A and 3390-3200 cm~(-1) in part B and 1730 cm~(-1) in coating film strongly proved polymers reacted just as the reacting mechanism, that means polysiloxane which offer low-surface-energy property linked Polyurethane system by —OH groups reacting with —NCO groups. Relative molar mass of part A and part B was determined by Gel Permeation Chromatography and the results were appropriate. Surface-energy was determined and results were between 33.6-47.17 mN/m and it increased when alkaline antifouling agent was put into the coating. Alkaline antifouling agent was releasing steadily when the coating film was dipped in seawater. As time gone, the pH value of seawater was increasing. Solubility parameter and results showed that there was no corrasive phenomenon between the polyethylene strand and the coating.

红外光谱分析结果表明，出现在A组分中的2275～2250cm~(-1)处的异氰酸酯特征吸收峰、B组分中的3390～3200cm~(-1)处硅羟基的特征吸收峰及出现在固化后涂膜中的1730cm~(-1)处氨基甲酸酯基团的特征吸收峰证明了涂料成膜物质交联固化符合本文的设计要求，即赋予涂膜低表面能特性的有机硅组分通过—OH基团与—NCO基团的反应已经链接到聚氨酯体系中；凝胶渗透色谱结果表明，成膜物质的A、B组分均为低分子量，符合预聚物的要求；涂膜表面能的测算结果表明，涂膜的表面能在33.6～47.17mN／m之间；加入碱式防污剂后涂膜的表面能略有升高；碱式防污剂的释放平稳，随着涂膜在海水中浸泡时间的增长，pH值有增加的趋势；用溶解度参数原则来评价涂料与网绳的涂装，结果表明，本试验研制的防污涂料对聚乙烯网绳无溶蚀作用。

It was found that ARA was composed of esterification products of (2-HEA)-ester with pimaric acid, dehydroabietic acid, abietic acid and two isomers of acrylpimaric acid. ARA is a good crosslinking agent which can copolymerize with most vinyl monomers. The properties of solvent-resistance and heat resistance of the copolymer were improved considerably by the use of ARA.

实验结果表明：ARA主要由海松酸、脱氢枞酸、枞酸和丙烯海松酸的二种异构体的丙烯酸－2-羟基乙基酯的酯化产物组成，ARA是一种良好的交联剂，可与大多数乙烯基单体共聚合，其与MMA的共聚物的耐溶剂性和耐热性均得到了较大幅度的提高。

In this thesis betulin was purified by recrystallization with chloroform and methanol mixture, and orthogonal design had been taken to optimize the conditions of recrystallization including the volume and ratio of chloroform and methanol mixtures.

在白桦酯醇的纯化方面目前比较成熟的方法是氯仿+甲醇混合溶剂重结晶来纯化白桦酯醇，本文通过正交设计，得到最优化的溶剂比例和用量。

The effect of carboxy methyl cellulose, high ester pectin and propy leneglucolalginate were significant, and we experienced the synergic effect of them by positive cross assay.

增稠剂羧甲基纤维素钠、高酯果胶及藻酸丙二醇酯能够显著提高调酸果奶的稳定性，并通过正交试验进行增稠剂的复配。

The effect of carboxy methyl cellulose, high ester pectin and propy leneglucolalginate were significant, and we experienced the synergic effect of them by positive cross assay.

增 稠剂羧甲基纤维素钠、高酯果胶及藻酸丙二醇酯能够显著提高调酸果奶的稳定性，并通过正交试验进行增稠剂的复配。

Multiple-walled carbon Nanotubes were used as carrier to load cerous sulfate catalyst for catalytic synthesis of n-butyl propionate Single factor and orthogonal experiment methods were applied to investigate the effects of the molar ratio of butyl alcohol to propionic acid, cerous sulfate mass fraction and reaction time on the conversion of propionic acid and the optimal technical conditions were determined as:ratio of butyl alchhol and propionic acid 1.5:1, cerous sulfate mass fraction 15% and reaction time 70 min.

以多壁碳纳米管作载体担载硫酸铈催化合成丙酸丁酯。分别采用单因素和正交实验方法考察了醇酸摩尔比、硫酸铈质量分率和反应时间等主要因素对丙酸丁酯得率的影响，并确定了最佳工艺条件为：醇酸摩尔比1.5：1、硫酸铈质量分率15%和反应时间70 min。

With the yield of methyl monochloroacetate as evaluating standard,the synthesized condition of methyl chloroacetate was optimized through orthogonal experiment.

以氯乙酸母液和甲醇为基本原料，固载磷钨酸为催化剂，通过连续酯化的方法制备了氯乙酸甲酯；以氯乙酸甲酯的质量收率为基准，采用三因素三水平正交实验的方法对酯合成的条件进行了优化。

The synthetic process of dialkyl phosphate by reaction of long -chain alcohol with phosphorus oxychloride was studied. The influence of molar ratio of reactants, reaction temperature, reaction time on process of esterification and hydrolysis was investigated too.

研究了以三氯氧磷与正构偶数高碳醇为原料合成磷酸二长直链烷基酯(C10～16-DAP)的工艺条件，考察了物料配比、反应温度和反应时间等因素对酯化反应与水解反应进程的影响，通过正交实验方法，确定了优化的合成工艺条件。

In this paper, the thermally reversible crosslinking reaction and the properties of synthesized TPE based on the reactions of chlorine containing polymers such as PVC , chlorined polyethylene , epichlorohydrin rubber and acrylic rubber with salts of dicyclopenladienyl dicarboxylate crosslinking agents were studied.

本研究以环戊二烯二酸盐衍生物作热可逆共价交联剂，通过与聚氯乙烯、氯化聚乙烯、氯醚橡胶和丙烯酸酯橡胶等含氯聚合物的脱MX酯化反应来实现共价关联，并制取相应的新型TPE。

APUHD was prepared with PEPUD acted as emulsor and reactive seeded emulsion in polymerization of acrylate monomer.

利用可聚合自乳化聚氨酯水分散体作为乳化剂和反应性的种子乳液与丙烯酸酯等单体共聚，其优点在于能调节聚氨酯水分散体侧链上参与共聚的双键数目，使聚氨酯和丙烯酸酯两相聚合物体系间直接化学键合增强，相容性提高，增加体系内部交联密度，合成得到具有核壳间互穿网络结构的丙烯酸聚氨酯杂合水分散体。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。