亚胺

The structures were identified by IR, UV,〓 NMR and element analyses. 2. Free radical 4-hydroxy-2,2,6,6-tetramethyl-1-piperidinyloxyl as catalyst, the phase transfer catalyzed method of oxidation eighteen semicarbazides to N-Aryl-2-Phenyl diazenecarboxamide with a solution of potassium ferricyanide in 2N aqueous sodium hydroxide and dichloromethane is described for the first time.

利用2，2，6，6-四甲基-4-羟基-1-哌啶氮氧自由基为相转移催化剂，在饱和铁氰化钾的2N氢氧化钠溶液与二氯甲烷的两相反应液中，催化氧化十八个取代氨基脲得到十八个相应的新型偶氮化合物N，2-二芳基二氮亚烯甲酰胺，均获得了较高的产率。

Methods: The protein and other impurity in the sample were precipitated by zinc acetate and potassium ferrocyanide after dipping of the sample. N,N-dichlorocyclohexylamine derived from sodium cyclamate by sodium hypochlorite in the filtrate was extracted by hexane. The HPLC separation was carried out with a phenomenex Gemini-C18 column using acetonitrile-water(7+3) or methanol-water (8+2) as mobile phase and detected by UV monitor at 314 nm. External standard method was used for quantification.

样品中甜蜜素浸提后，用乙酸锌和亚铁氰化钾试剂沉淀蛋白质等干扰杂质，过滤，用次氯酸钠将样品溶液中的甜蜜素转化为N，N-二氯环己胺经正己烷萃取后，在phenomenex Gemini-C18柱上，以乙腈－水(7+3)或甲醇－水(8+2)为流动相进行分离，HPLC-UV检测器在314 nm测定，外标法定量。

High absorption and retentions clinoptilolite /Starch/ PAANa composite was synthesized by water-solution copolymerization with clinoptilolite and acrylic acid as principal raw materials,with N N-methylene-bis-acrylamideand as crosslinker, and with potassium persulphate as initiator .

以丙烯酸、斜发沸石为主要原料，以N，N'-亚甲基双丙烯酰胺为交联剂、过硫酸钾为引发剂，采用水溶液聚合法合成了斜发沸石/淀粉/聚丙烯酸高吸水保水性复合材料。

Under mild hydrothermal synthesis conditions, we first successfully prepared threeindium phosphites with different organic amine molecules as template agents.

在水热条件下，以乙二胺为模板首次合成出1个具有一维正六边形孔道结构的亚磷酸镉微孔化合物。

Under mild hydrothermal conditions, using DETA as structure-directing agent,two three-dimensional gallium phosphites (H3DETA)Ga3(HPO3)4F4 (1) andGa2(HPO3)3 (2) have been synthesized and characterized by single crystal X-raydiffraction.

在合成方面，主要研究作为模板剂的有机胺类的改变对产物结构的影响；通过引入[HPO3]2-的结构基元代替传统的[PO4]3-结构基元，设计合成系列具有新颖结构的无机微孔材料并探讨亚磷酸盐和磷酸盐微孔材料在合成以及骨架结构方面的特点和差异。

An intramolecular α-addition of hydroxy or amine-substituted electron-deficient alkyns catalyzed by phosphines was developed. An intramolecular β-addition of hydroxysubstituted 2-alkynoates trigged by the tributylphosphine was also achieved.

在上面的研究中发现低活性的亚甲基取代的环内酰胺的[3+2]环加成反应也能顺利进行，因此我们研究并实现了β-位取代的贫电子烯烃的环加成反应，进一步拓展了叔膦催化的[3+2]环加成反应。

The compositions of high molecular weight glutenin subunits in 106 synthetic wheats were analyzed by using sodium dodecyl sulphate polyacrylamide gel electrophoresis.

利用十二烷基磺酸钠－聚丙烯酰胺凝胶电泳技术对106份人工合成小麦(2n=6x=42， AABBDD)的高分子量谷蛋白亚基组成进行了分析。

Through a comparative study of ~(99)Tc~m-DTPA and ~(99)Tc~m-OCT SPECT orbital imaging,evaluated the clinic significance of two imaging in estimating activity of TAO.The aim of this study was to develop a new method:simple,rapid and costefficient method for staging patients with TAO.

本研究采用~(99)Tc~m-二亚乙基三胺五乙酸~(99Tc~m-diethylene tri-aminepentaacetic acid，~(99)Tc~m-DTPA进行眼眶显像并与~(99)Tc~m-奥曲肽~(99Tc~m-octreotide，~(99)Tc~m-OCT眼眶显像进行比较，研究其在反映TAO患者眶周炎性程度的价值，旨在探索一种新眼眶显像方法：既经济又迅速，显像效果稳定又可靠。

Methods Male SD rats were given drinking water containing manganese chloride (MnCl24H2O 0.5g/L and 5.0g/L respectively) for 60 days. At the end of experiment, all the rats of the manganese-exposed groups and control group were decapitated after anaesthesia with 2% sodium phenobarbitone intraperitoneally, the brains were removed and activities of alanine aminotransferase, aspartate aminotransferase, alkaline phosphate, cholinestarase, monoamine oxidase, superoxide dismutase, nitric oxide synthase, and levels of glutathione, maleic dialdehyde, and proteins were biochemically analyzed.

大鼠经饮水连续染锰（MnCl24H2O 0.5g/L和5.0g/L）60d后，应用荧光光度比色法测定新鲜脑组织匀浆的谷丙转氨酶、谷草转氨酶、碱性磷酸酶、胆碱酯酶、单胺氧化酶、氧化亚氮合酶、超氧化物歧化酶活性和谷胱甘肽、丙二醛、蛋白质含量，并设生理盐水对照组。

Employing CuI(5 mol%), N,N-dimethylglycine hydrochloride(10 mol%) and K_2CO_3(2 equiv.) in refluxing THF as the optimized reaction conditions,the four-membered 4-alkylidene-2-azatidinones could be efficiently synthesized.

当以3-溴-3-N-苯基-丁烯酰胺为底物，在5 mol%CuI为催化剂，10 mol%N，N-二甲基甘氨酸盐酸盐为配体，2当量K_2CO_3作碱，THF回流的反应条件下，可以高效的合成2-亚甲基-4-氮杂环丁酮类化合物。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。