亚胺

Nanosized titania particles consisting of anatase, rutile and brookite phases were synthesized under solvothermal conditions with different alcohols as solvents, hexamethylene tetramine as precipitant as well as precursor of titanium trichloride.

采用不同的醇溶剂，以六亚甲基四胺为沉淀剂，以TiCl3为前驱体，通过溶剂热的方法控制合成出纳米级的锐钛矿型、金红石型和板钛矿型的二氧化钛。

Chloride of lime at 15~30 mgL^(-1), potassium permanganate at 20~30 mgL^(-1), and 40% Yubao at 50~75μLL^(-1) coming next are recommended to be applied to the tobacco float seedling system TMY inactivation in water.

生产上池水TMV消毒可选择下列消毒剂：质量分数30%有效氯漂白粉15~30 mgL^(-1)和质量分数98%高锰酸钾20~30 mgL^(-1)，其次为体积分数40% N-羟乙基亚甲胺多聚物75~100μLL^(-1)。

The local lesion assay indicated that: contacted with TMV infected leaf juice dilution over 12 h, the disinfestants whose inactivation ratio of TMV above 80% are as follows: 7% sodium hypochlorite at 10 μLL^(-1), 30% chloride of lime at 15 mgL^(-1), 40% Yubao at 75 μLL^(-1) and 98% potassium permanganate at 20 mgL^(-1), 10% chlorine dioxide at 25 mgL^(-1) inactivation ratio of TMV less than 50%.

结果表明，与TMV病叶汁液2万倍稀释液接触12 h，体积分数7%有效氯次氯酸钠10μLL^(-1)、质量分数30%有效氯漂白粉15 mgL^(-1)、体积分数40% N-羟乙基亚甲胺多聚物75μLL^(-1)和质量分数98%高锰酸钾20 mgL^(-1)对TMV的抑制率高于80%，质量分数10%二氧化氯粉剂25 mgL^(-1)对TMV的抑制率低于50%。

Target compounds have been synthesized by condensation of the aromatic nucleus and amino heterocylcle with acyl isocyanates or acylisothiocyanates in absolutely anhydrous and aprotic solvent.

为了寻找高活性的农药品种，利用生物等排原理和亚结构连接法，对脲类化合物的母体结构进行了修饰，将芳氧羧酸类及吡唑环引入酰基脲母体结构中，利用酰基异氰酸酯与杂芳环胺类化合物在无水非质子溶剂中发生亲核加成反应，合成了四个系列21种新的酰基脲类目标化合物。

Using potassium persulfateas initiator and N, N′-methylenebisacrylamideas crosslinker, the graft copolymerization of acrylic acidonto modified cornhusk fiber was carried out.

将玉米秸秆进行提纯改性，采用过硫酸钾为引发剂、N，N-亚甲基双丙烯酰胺为交联剂，使其与丙烯酸接枝共聚合成农用高吸水树脂，通过试验对比最终确定最佳条件为改性玉米秸秆与丙烯酸的质量比为1∶6、丙烯酸中和度为70%、反应时间为4h、烘干温度为60°C；对最佳条件下制备的树脂进行了吸水倍率的测试；对秸秆预处理前后及接枝产物进行了红外谱图分析。

In this study novel materials based on epoxy and cyanate ester containing siloxane and imide groups were investiged.

在这本篇论文研究中，我们发展出新型含矽氧烷及亚醯胺基环氧树脂和氰酸酯化合物。

Chapter two 4-Hydroxybenzoic acid is connected with PEG6000 through defoliant DCC at rooom temperature, then the product is refluxed with chloroacetic acid in acetone to afford PEG-bound phenyloxyacetic acid, which is reacted with thionyl chloride, ammonium thiocyanate and arylamines in turn to give PEG-bound disubstituded thioureas. After the cleavage with sodium methoxide in methanol, the eleven disubstituted thioureas are obtained.

第二章 利用PEG6000作载体，通过脱水剂DCC在室温下将对羟基苯甲酸以酯键连接在PEG6000上，再与氯乙酸在较温和的条件下生成PEG6000支载的芳氧乙酸，然后，依次与亚硫酰氯、硫氰酸铵、芳胺反应，生成PEG6000支载的硫脲，最后用甲醇钠的甲醇溶液切割PEG，得到了十一种1，3-二取代硫脲。

This method is based on the diazotization of sulfadiazine with sodium nitrite in acidic medium and the coupling reaction with α-naphthylamine.

在盐酸介质中，利用磺胺嘧啶－亚硝酸钠－α-萘胺的重氮化－偶合反应，建立了流动注射光度法测定磺胺嘧啶的新方法。

The influence of each condition on the reaction speed and yield was studied, and the optimal conditions were: the ratio of the amount of substance of aromatic amine and heptafluoro-isopropyl iodine was 1:1.1~1.5, the amount of substance of sodium dithionite, sodium bicarbonate, aniline compounds were respectively 1.1~1.3, the amount of substance of phase transfer catalyst TBAB and aniline compounds was 0.05~0.1, the concentration of aniline compound was 0.5~1.0 mol/L, reaction temperature was 10~20 ℃, and the solvent was aether.

最佳结果为：芳胺与七氟异丙基碘的物质的量比1：1.1~1.5，连二亚硫酸钠、碳酸氢钠与苯胺的物质的量分别为1.1~1.3，相转移催化剂四丁基溴化铵与苯胺的物质的量比在0.05~0.1，溶剂总用量使苯胺浓度在0.5~1.0 mol/L；反应温度10~20℃；溶剂采用乙醚。取代基供电子性越强，反应时间越短，产率越高；氨基的对位优先反应，氨基的邻位较难发生反应；且七氟异丙基总是优先取代在芳环电子云密度较高的位置上。

Its commercial technologic processes and products,such as Acetic Acid Production by Carbonylation of Methanol,Formyl Morpholine,Steam Reforming Catalyst,Low Pressure Methanol Synthesis,Dimethyl Formamide Production by Dehydrogenation of Methanol,Dimethyl Ether Synthesis by Methanol Dehydration,Hydrogen Production by Methanol Cracking,Methanol Synthesis Catalyst,PSA Gas Separation Devices, and etc.,have been applied in more than 800 plants over fields including chemical industry,petrochemical,food, metallurgy,machinery,military industry.Many technological products were exported to American,European,Asian countries as well as Hong Kong,Macao and Taiwan.Remarkable economic and social benefits are achieved.

甲醇羰基化合成醋酸，甲酰吗啉，转化催化剂，低压合成甲醇，甲醇脱氢制二甲基甲酰胺，甲醇脱水制二甲醚，甲醇裂解制氢，合成甲醇催化剂，变压吸附制氢等成套工业装置和产品应用于全国800多家化工，石化，食品，冶金，机械，军工等企业，并出口美国，欧州，亚州等国及港，澳，台地区。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。