亚胺

Apparent partition coefficient in octanol-water and binding percentage to BSA of ~(153)Sm-NTMP,~(153)Sm-HEDTMP,~(153)Sm-DCTMP,~(153)Sm-EDTMP,~(153)Sm-DTPMP,~(113,117) Sn~m-EDTMP,~(113,117) Sn~m-HEDTMP,~(113,117) Sn~m-DTPMP are measured. The results show that there is a linear relationship between the relative magnitude of the apparent partition coefficient in octanol-watetr and the relative magnitude of the binding percentage to BSA of these ~(153)Sm~(113,117Sn~m complexes.

测定了NTMP，HEDTMPN (羟乙基乙二胺基三亚甲基膦酸，DCTMP(1，2 环己二胺四亚甲基膦酸)，EDTMP(乙基二胺基四亚甲基膦酸)，DTPMP(二乙基三胺基五亚甲基膦酸)的153Sm配合物以及HEDTMP，EDTMP，DTPMP的113，117Snm配合物在正辛醇水中的表观脂水分配系数和在0 5%牛血清白蛋白水溶液中与BSA的结合率。

Through using Mythylene DinitrAmine as rude product, the knowledge of its reaction properties in different phases have been increased, Through using Mythylene BisAcetAmide as rude product, intermediates which include 1,3-Diacetyl -4,5-dihydroxy -1,3-diazacyclopentane and 1,3-Diacetyl- 4,5-diacetoxy-l,3-diaza cyclopentane have been obtained. 2,4,6,8-tetracetyl- 2,4,6,8-tetraaza bicyclo[3,3,0]octane which can be used to produce Bicyclo-HMX by nitrolysis was also produced. Through using Mythylene BisFormAmide as rude product, intermediates which include 1,3-Diformyl-4,5-dihydroxy- 1,3-diazacyclopentane and 1,3-Diformyl- 4,5-diacetoxy-l,3-diazacyclopentane have been abtained.

以亚甲基二硝胺为初始原料，加深了对亚甲基二硝胺在不同反应相反应特征的认识；以亚甲基二乙酰胺为初始原料，制备了中间体1，3-二乙酰基-4，5-二羟基-1，3-二氮杂环戊烷和1，3-二乙酰基-4，5-二乙酰氧基-1，3-二氮杂环戊烷，最终制备了可被直接硝解为双环HMX的2，4，6，8-四乙酰基-2，4，6，8-四氮杂双环[3，3，0]辛烷；以亚甲基二甲酰胺为初始原料，制备了中间体1，3-二甲酰基-4，5-二羟基-1，3-二氮杂环戊烷和1，3-二甲酰基-4，5-二乙酰氧基-1，3-二氮杂环戊烷。

It is found that the sample stained with silver methenamine instead of mercaptoacetic acid-osmium can prevent the false phenomena caused by the inappropriate use of mercaptoacetic acid.

摘 要：本文将六亚甲四胺银染色法作为加工毛发的电子染色剂得到较好的电子显微图像，并系统地比较了用巯基乙酸-锇法染色的羊毛样品和用六亚甲四胺银染色的人发样品的超微结构，认为对深加工过的毛发样品用六亚甲四胺银法替代巯基乙酸-锇法染角蛋白，可以防止巯基乙酸使用不当引起的假象。

The contents of putrescine and spermidine increased more obviously in high responding line and decreased significantly in low responding lines.

敏感型材料的游离脯氨酸、丝氨酸、精氨酸、丙氨酸含量水平明显比迟钝型材料的高。25d低温预处理后，敏感型材料的多胺总量比0d时的明显提高，腐胺和亚精胺的含量升幅特别显著；迟钝型材料的多胺总量比0d时的低，亚精胺和精胺的降幅较为明显。

The contents of putrescine were apparently higher than the control, then decreased with the increase of lead mass concentration and the time of treatment.

黄瓜幼苗叶片精胺和亚精胺在处理第5d时高于对照值，茎中精胺和亚精胺含量在处理第7d高于对照值，而其它时间内的都低于对照值，而且其含量均随铅质量浓度的增加而呈下降趋势；过氧化物酶活性变化与内源多胺含量（腐胺、精胺和亚精胺之和）的变化相似，表明铅胁迫能改变黄瓜幼苗内源多胺的含量和调节过氧化物酶活性，从而影响着黄瓜植株的生长。

Spermine and spermidine were detected in fairly high amounts in the muscle. In the liver and gonad putrescine was detected in the highest amounts, followed by spermidine and spermine.

肌肉中的多胺检出为精胺和亚精胺，肝脏和生殖腺中有较高浓度的腐胺及亚精胺和精胺检出。

Agmatine is the precursor of spermine and spermidine; however, neither of the two polyamines influenced morphine analgesia.

胍丁胺是精胺及亚精胺的合成前体。精胺和亚精胺均不影响吗啡的镇痛作用。

Three kinds of small molecular copper and zinc superoxide dismutase mimics were synthesized with N, N-bis (benzimidazol-2-ylmethyl) amine (N3), N, N-bis (benzimidazol-2-ylmethyl) methylamine(MN3) and N,N-bis (benzimidazol-2-ylmethyl) benzylamine(BN3) as ligands. The com-plexes were characterized by UV, IR and element analysis and the structures were proposed.

模拟铜一锌超氧化物歧化酶的活性中心，以二(2-苯并咪唑)丙烷为桥、二(2-苯并咪唑亚甲基)胺(N3)、二(2-苯并咪唑亚甲基)甲胺(MN3)及二(2-苯并咪唑亚甲基)苄胺(BN3)为配体合成了3种异双核的小分子模型化合物，并进行了紫外、红外表征及元素分析，推测了可能的结构。

Seven Schiff bases of N-(4-hydroxyphenylmethylene)-1-naphthylamine, N-(4-hydroxyphenylmethylene)-p-methoxyaniline, N-(4-hydroxyphenylmethylene)-benzylamine, N-(4-hydroxy-3-methoxyphenylmethylene) furfurylamine, N-(4-hydroxy-3-methoxyphenyl methylene)-p-methylaniline, N-(4-hydroxy-3-methoxyphenylmethylene)-p-methoxyaniline and N-salicylidene-4-aminoantipyrine were first synthesized by the one step solid phase reactions between aromatic aldehydes with phenolic hydroxyl and amines at room temperature without solvent.

分别以带酚羟基的芳醛与胺类反应，首次通过室温固相反应一步合成了N-（4-羟基苯基亚甲基）-1-萘胺、N-（4-羟基苯基亚甲基）-对甲氧基苯胺、N-（4-羟基苯基亚甲基）-苄胺、N-（4-羟基-3-甲氧基苯基亚甲基）糠胺、N-（4-羟基-3-甲氧基苯基亚甲基）-对甲苯胺、N-（4-羟基-3-甲氧基苯基亚甲基）-对甲氧基苯胺和N-亚水杨基-4-氨基安替比林7种Schiff碱，反应15min完成，产率均超过90％。

In this article, the method for detecting five kinds of biogenic amines by HPLC was established, and the contents of biogenic amines in Chinese rice wines and soy sauces were detected. In order to reduce the contents of BA, we inoculated Lactobacillus curvatus 6031 and Leuconostoc mesenteroides 51-5 D in sausage and the contents of BA and the microbial counts was studied during the fermention of sausage.

建立了高效液相色谱测定生物胺含量的方法，方法稳定性好、精密度高，回收率高，五种生物胺的回归方程分别为：y 尸胺=48.903x R 2=0.9996；y 组胺=36.105x R 2=0.9994；y 酪胺=29.865x R 2=0.9902；y 亚精胺=46.671x R 2=0.9967；y 精胺=31.239x R 2=0.9926，在2～40μg/ml的范围内R均大于0.99，检测限分别为：尸胺、组胺和亚精胺为0.05μg/ml，酪胺为0.1μg/ml，精胺为0.25μg/ml。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。