亚线性

MethodsIn the solvent of 1 mol/L NaOH, using the reaction of the water-soluble phenolic acidity in Radix Salviae Miltiorrhizae and the NaNO_2-Al(NO_3)_3, the total components of water-soluble phenolic acidity in Radix Salviae Miltiorrhizae injections and drip solution(calculated with protocatechualdehyde) were determined by colorimetric s...

方法利用丹参中水溶性酚酸类成分与亚硝酸钠和硝酸铝溶液在碱性条件下的显色反应，比色法测定该两种制剂中水溶性酚酸的总量。结果原儿茶醛在3.336~14.46mg/L范围内呈良好的线性关系，回归方程为：A=0.02777C+0.01279(r=0.9996)，加样平均回收率为100.8%，RSD为0.96%。结论该法简便快速，结果准确，重现性好，可用于该制剂的质量控制。

Part 6 explores the reaction system containing O-phthalate, Mn〓 and α,α'-diimine, and yields six novel complexes 16～20 possessing binuclear and tetranuclear matello-crown aether as well as 1-D linear structures, indicating that O-phthalate is a potentially useful ligand to give manganese species in a discrete form.

研究了邻苯二甲酸/锰/双齿亚胺（2，2'-联吡啶和1，10-邻二氮杂菲）的反应体系，合成出6个新颖的双核、四金属冠醚和一维线性结构的化合物16至20，表明邻苯二甲酸是合成有限核数锰簇的有用配体。

The resulting polymers showed good thermal properties and excellent organosolubility even in common low boiling point solvents, such as acetone, chloroform and 1, 1, 2-trichloroethane, yielding a polymer solution with solid contents over 10wt%.

聚合物膜的紫外-可见光吸收阀值波长低于350nm，比线性类似物的（450nm）低许多，得益于超支化结构导致的酰亚胺环结构的疏松堆积，有利于以其为大分子骨架的光敏材料在365nm紫外工作波长的光刻。

A competitive ELISA kit for detect ENR was developed with ENR mAb and its traits were tested.Two hybridoma lines were filtered and the best one was 4G1-B3,which secreted ENR mAb with indirect ELISA titers of 1∶1.024×10~6 in ascites.Isotype of the two mAb was IgG_1.ENR mAb had a high affinity constant with 9×10~(10)L/mol.The ENR-Kit had the linear detection range of 0.05～101.6μg/L,the sensitivity of 0.05 μg/L and a good sensitivity with an IC_(50) of 1.1μg/L to ENR,cross-reactivity to other compounds less than 0.01%.The average recoveres of ENR spiked in chicken,liver,fish and milk were 81.5%,87.6%,84.3% and 95% respectively.The coefficient variation was below 10%.

结果表明：筛选出的2株杂交瘤细胞，单抗亚类均为IgG1型，其中4G1-B3株的ENR mAb间接ELISA效价为1：1.024×106，亲和常数为9×1010L/mol；竞争ELISA试剂盒的线性检测范围为0.05~101.6μg/L、灵敏度0.05μg/L、半数抑制浓度(IC50)1.1μg/L，与其他化合物的交叉反应率均小于0.01%，鸡肉样、鸡肝样、鱼肉样和牛奶样的平均添加回收率分别为81.5%8、7.6%、84.3%和95%，不同基质添加恩诺沙星标准品做竞争ELISA对ENR-Kit检测结果影响小，试剂盒保存期6个月以上。

Iodine in the test solution was oxidized to IO-3 by excessive amounts of potassium permanganate solution and sodium hypochlorite solution,and excess of the oxidants was removed by reacting with sodium sulfite solution.

采用过量联合氧化剂高锰酸钾-次氯酸钠氧化试液中碘至IO3-，剩余的高锰酸钾和次氯酸钠用过量的亚硫酸钠反应除去，利用IO3-的电活性，建立了在四硼酸钠-吐温-80底液中的线性扫描伏安法测定微量碘的方法。

Firstly, phenyliodine diacetate was immobilized to the 2% cross-linked polystyrene or the liner polystyrene resin. The more iodine the resin had, the lower conversion to phenyliodine diacetate. We made our endeavor to extend the range of useful application of polystyrene supported phenyliodine diacetate in organic synthesis:(1) the reagent was used as an effective reagent of carbonyl regeneration from oximes and semicarbazones of ketones.(2) the reagent was also applied to the synthesis of 1, 3, 4-oxadiazoles, 1, 3-disubstituted-2-pyrazoline, 2-arylbenzoxazole from aldehyde N-acylhydrazones, aldehyde hydoazones and phenolic Schiff's bases respectively.

首先，我们以2％交联的聚苯乙烯和线性的聚苯乙烯树脂为载体，制备了聚合物负载的二醋酸碘苯，通过研究发现：(1)聚苯乙烯二醋酸碘苯是酮肟、缩氨脲有效的去保护试剂，不仅芳香酮，脂肪酮和α，β不饱和酮的肟、缩氨脲也能顺利转化为相应的酮，实现酮基的再生；(2)我们还利用此试剂，分别与醛的N-酰基苯、N-酰基苯腙及邻羟基芳亚胺反应，在温和的条件下发生成环反应，以良好的产率生成1，3，4-噁二唑、吡唑啉和二取代苯并噁唑等杂环化合物；(3)聚苯乙烯二醋酸碘苯还可有效地将邻羟基芳酮的酰腙经氧化、重排成1，2-二酰基苯。

In the experiment focused on decadal changes, GCMs reproduce the observed NAO shifts in recent decades by imposing strengthening trends on stratospheric wind. The cooling belt extending from North Africa to subtropical Eurasia is simulated accompanying the strengthening of NAO. East end of this cooling belt reaches the eastern flank of Tibetan Plateau.

在强调年代际变化的实验中，通过在平流层中强迫出水平风场的线性增强趋势，大气环流模式可以模拟出近几十年间冬季NAO指数的年代际上升；伴随着NAO正位相的增强，模式可以再现北非至副热带欧亚大陆的冷却带，且其东端可以到达青藏高原下游地区。

CTAB could form well-stabilized films on the surface of HPAM solution, this process is dependent on the linear density and conformation of the polymer chain; it is reasonable to suppose that a complex, which is surface active, was formed between CTAB and HPAM.

阳离子表面活性剂能在HPAM水溶液的表面成膜，表面活性剂的成膜能力与它本身的HLB有关，还与亚相中HPAM的线性电荷密度以及高分子在溶液中的分子构象有关。

For a big chunk of credit-card losses; the number of filings (and thus charge-off rates) would be rising again, whether

年美国个人破产法的一个改动使得破产登记急速下降，而后引起了信用卡大规模的亏损。

Eph. 4:23 And that you be renewed in the spirit of your mind

弗四23 而在你们心思的灵里得以更新