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The optimum conditions to synthesizeβ-carboxyethyl organogermanium sesquioxide were established through orthogonal test: the time from beginning to adding sodium hypophosphite was 0.5h; the molar ratio of germanium dioxide, hydrochloric acid and sodium hypophosphite was 1:7.4:1.4; addition reaction time was 1.5h.

用正交试验确定了最佳工艺条件:从反应开始到加次亚磷酸钠的间隔时间0.5h;n:n:n=1 : 7.4 : 1.4;加成反应时间1.5h。

The thermodynamics and the dynamics mechanism have been studied.The results show that it is advisable for the HCHO and NaH_2PO_2 as the reduction due to the electrode potential of the reduction is more negative than that of Cu~ 2+ from the analysis of data in thermodynamics.It is advantage for the reaction of electroless copper in the alkaline solution. According to the analysis of Tafel slope of a cathodal polarization curve,...

结果表明:从热力学数据分析看,还原剂的电极电位皆比铜离子负,用甲醛、次亚磷酸钠做还原剂还原Cu2+在热力学上是可行的,在碱性溶液中对化学镀铜反应有利;从阴极极化曲线的Tafel斜率分析看,Cu2+=Cu+步骤为阴极反应的速度控制环节;从镀液的旋转圆盘电极测试结果分析看,电子跃迁步骤H2CO-ad rdsHCOOH+1/2H2+e-为镀液中阳极反应速度的控制性步骤。

The proposed electrooxidation mechanism well explains the effects on voltammetric behaviour of the factors such as potential sweep rate, temperature of medium and hypophosphite concentration.

所述机理可以较好地解释电位扫描速度、介质温度及次亚磷酸根浓度对伏安行为的影响。

Diethylphosphite was prepared from ethanol and phosphorus trichloride at mole ratio of 3.3:1 with the droping temperature at 5-10℃, and reacted under room temperature.

以无水乙醇和三氯化磷为3.3:1的投料量,5~10℃下滴加,室温下反应,制备亚磷酸二乙酯。

Antioxygen 168 schemical name is tri (2, 4-di-butylphenyl)sulfite ester, which is made from 2, 4-di-butyl phenol and phosphorus trifluoride .

抗氧剂168化学名称为三(2,4-二叔丁基苯基)亚磷酸酯,由2,4-二叔丁基苯酚与三氯化磷反应制得。

The inhibitory performance of triphenyl phospite in naphenic acid to the corrosion of A3 steel was investigated by the mass loss method.

采用静态挂片和SEM方法,考察了亚磷酸三苯酯在环烷酸腐蚀体系中对A3钢的缓蚀性能。

Triphenyl phosphite provided prominent stabilization only when used in combination with other stabilizers. Good results have been obtained for both polyether-urethane and nitrate esters when using 2,6-di-t-butyl-4-methyl-phenol as stabilizer.

亚磷酸三苯酯单独使用时效果较差,但与其它种类的稳定剂混合使用能得到较好的效果。2,6-二叔丁基-4-甲基酚对硝酸酯和聚氨酯粘结剂均具有良好的稳定作用。

Influences of factors, such as the dose of TPP and water, alkalization time and way of adding sodium hydroxide, on the degree of substitution, uniformity of substitution groups distribution and the viscosity were studied..

综合水 溶液粘度和取代度及其分布两因素,得到优化的工艺配方:在20℃下,加入8wt%亚磷酸三苯酯量,氢氧化钠和纤维素的摩尔比为3。

The difference of ammonia, amido, amino group and quaternary ammonium salt, some common wrong expressions on them, and the valence state of phosphorus in some of its oxyacid were pointed out.

指出了氨、氨基、胺基及季铵盐的区别及其常见错误表述,以及磷的几种含氧酸中磷的价态,并着重指出没有&次亚磷酸&的叫法。

Under high dilution,the cross-coupling reactions of 4,5-dicyano-1,3-dithiol-2-one(6) and dithia crown-ether annulated tetrathiafulvalenes(3a~3c) in toluene gave asymmetrical dicyano tetrathiafulvalene derivatives(7a~7c) in the presence of triethyl phosphite.The compounds 7a~7c were characterized by(~1HNMR,EA,MS and IR.

在甲苯溶液中,在亚磷酸三乙酯存在下,采取高度稀释的方法,使4,5-二氰基-1,3-二硫杂环戊二烯-2-酮分别和多缩硫杂冠醚进行交叉偶联反应,成功地得到了不对称的2,3-二氰基四硫富瓦烯衍生物。

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According to the clear water experiment, aeration performance of the new equipment is good with high total oxygen transfer coefficient and oxygen utilization ratio.

曝气设备的动力效率在叶轮转速为120rpm~150rpm时取得最大值,此时氧利用率和充氧能力也具有较高值。

The environmental stability of that world - including its crushing pressures and icy darkness - means that some of its most famous inhabitants have survived for eons as evolutionary throwbacks, their bodies undergoing little change.

稳定的海底环境─包括能把人压扁的压力和冰冷的黑暗─意谓海底某些最知名的栖居生物已以演化返祖的样态活了万世,形体几无变化。

When I was in school, the rabbi explained everythingin the Bible two different ways.

当我上学的时候,老师解释《圣经》用两种不同的方法。