亚碘的

The method was based on the inhibition effect of iodine on the nitrite catalyzed oxidation of cresol red by potassium bromate catalyzed by nitrite in dolute sulfuric acid medium.

研究了在稀硫酸介质中，痕量碘离子对亚硝酸根催化溴酸钾氧化甲酚红的阻抑作用，建立了测定痕量碘离子的阻抑动力学光度分析的新方法。

Methods The modified method of Watkinson's was used for the kinetic colorimetric determination of iodine in food with I catalytic arsensous acid and cerous sulfate.

用亚砷酸-硫酸铈法测定食品的碘含量，根据1992年黑龙江省营养调查推算出哈尔滨市市区人均日碘摄入量。

Treatment of dials with N-tert-butanesulfinamide, all biaryl dials were successfully converted into the corresponding bis-imines which were then treated with samarium diiodide to afford diamine products. The absolute configurations of all the intramolecular coupling products were determined by X-ray crystallography.

轴手性二醛与N-叔丁基亚磺酰胺缩合得到相应的亚胺，其为一对非对映异构体。N-叔丁基亚磺酰亚胺在二碘化钐条件下得到的偶联产物，经X-衍射也确定了其立体构型。

This dissertation is mainly focused on the reactivity of methylenecyclopropanes and comprises six parts. 1 The reactions of methylenecyclopropanes with phenylsulfenyl chloride, phenylselenyl chloride and diphenyl diselenide; 2 The coupling reactions of the ring-opening products derivated from methylenecyclopropanes; 3 The palladium-catalyzed ring-enlargement of mono-aryl group substituted methylenecyclopropanes to cyclobutenes. 4 The gold-catalyzed domino ring-opening and ring-closing hydroamination of methylenecyclopropanes with sulfonamides; 5 The Lewis acid-catalyzed reactions of mono-aryl group substituted methylenecyclopropanes with diethyl ketomalonate in the presence of water; 6 The iodobenzene diacetate mediated novel 1,3-dipolar cycloaddition of methylenecyclopropanes, vinylidenecyclopropanes, and methylenecyclobutane with phthalhydrazine.

本论文主要研究了亚甲基环丙烷类化合物的一些化学反应性能，共由以下六部分组成：1、亚甲基环丙烷类化合物与苯硫氯、苯硒氯及二苯基二硒的反应；2、亚甲基环丙烷类化合物开环产物的偶联反应；3、单芳基取代的亚甲基环丙烷类化合物在钯催化剂作用下的扩环反应；4、金化合物催化磺酰胺对亚甲基环丙烷类化合物的串联开环关环氨氢化反应；5、路易斯酸催化亚甲基环丙烷类化合物与丙酮二羧酸二乙酯在有水存在下的反应；6、醋酸碘苯促进的亚甲基环丙烷类化合物、亚乙烯基环丙烷类化合物及亚甲基环丁烷类化合物与邻苯二甲酰肼的新型1，3-偶极环加成反应。

Universal salt iodization promotes the growth of children and corrects the sub-clinic damage of IDD.

全民食盐加碘对儿童生长发育有促进作用并使原有的缺碘亚临床损伤得到改善。

The results showed polymeric diaryliodonium salts were effective aryl ion transfer reagents. Thirdly, a new type polymer supported hypervalent iodine reagents poly { [4-Hydroxy iodo] styrene} has been developed. It was an effective oxidative reagent, and could be applied to the one pot synthesis of 4-arylthiazoles.

然后，我们以聚苯乙烯羟基对甲苯磺酰氧基碘苯为原料，成功制备了一类新型聚合物高碘试剂—聚苯乙烯负载的炔基碘盐，并研究了其作为炔基转移试剂的有效性：(1)该试剂可对硫、氮、硒等负离子进行亲电炔基化反应，合成炔基亚砜、0，0-二烃基二硫代磷酸炔基酯、1-苯乙炔基苯并噻唑以及炔基硒醚。

METHODS: Rat mesenchymal stem cells at passage 3 were obtained under sterile condition, and divided into groups A-F. In group A, iodine ion was not added. In groups B-F, iodine ion at mass concentrations of 2, 55, 90, 125 and 2 500 mg/L was added respectively. An additional blank control group was established, and simultaneously the cells were induced into neuron-like cells with dimethyl sulphoxide.

无菌条件下取大鼠第3代间充质干细胞，分为A~F组：A组不加碘离子，B~F组中分别加入质量浓度为2，55，90，125和2 500 mg/L的碘离子，另设空白对照组，同时加化学诱导剂二甲基亚砜向神经元方向诱导分化。

Objective In order to study the testing numerical value of urine iodine and hair iodine is stable or not.

广告载入中。。。广告载入中。。。张春之，吴小科，凌志强，邓兰，陆罗萍，姚敏，张梅亚目的探讨尿碘和发碘测定值的稳定性。

Subjects who had taking iodine-containing preparations or thyroid hormone were also excluded.2.2 MethodsSerum levels of triiodothyronine ( T3 ), thyroxine ( T4 ), free triiodothyronine ( FT3 ), free thyroxine ( FT4 ) and thyrotropin were determined by immunochemiluminometric assay for ninety-fifth patients with atrial fibrillation and one hundred and thirty nine controls matched for age and sex.2.3 StatisticsAll statistical procedures were performed with SPSS 10.0 software package.

同时根据甲状腺功能指标的测定把心房颤动患者分为①正常组：TSH、FT3和 FT4水平均正常②甲状腺功能亢进组：TSH水平降低，FT3和 FT4水平升高③亚临床甲状腺功能亢进组：TSH水平降低，FT3和 FT4正常。2.2方法入选者于清晨空腹静脉取血 2 ml，采用免疫化学发光法分别测定血清中的三碘甲状腺原氨酸（T3）、甲状腺激素（T4）、游离三碘甲状腺原氨酸（FT3）。

Firstly, phenyliodine diacetate was immobilized to the 2% cross-linked polystyrene or the liner polystyrene resin. The more iodine the resin had, the lower conversion to phenyliodine diacetate. We made our endeavor to extend the range of useful application of polystyrene supported phenyliodine diacetate in organic synthesis:(1) the reagent was used as an effective reagent of carbonyl regeneration from oximes and semicarbazones of ketones.(2) the reagent was also applied to the synthesis of 1, 3, 4-oxadiazoles, 1, 3-disubstituted-2-pyrazoline, 2-arylbenzoxazole from aldehyde N-acylhydrazones, aldehyde hydoazones and phenolic Schiff's bases respectively.

首先，我们以2％交联的聚苯乙烯和线性的聚苯乙烯树脂为载体，制备了聚合物负载的二醋酸碘苯，通过研究发现：(1)聚苯乙烯二醋酸碘苯是酮肟、缩氨脲有效的去保护试剂，不仅芳香酮，脂肪酮和α，β不饱和酮的肟、缩氨脲也能顺利转化为相应的酮，实现酮基的再生；(2)我们还利用此试剂，分别与醛的N-酰基苯、N-酰基苯腙及邻羟基芳亚胺反应，在温和的条件下发生成环反应，以良好的产率生成1，3，4-噁二唑、吡唑啉和二取代苯并噁唑等杂环化合物；(3)聚苯乙烯二醋酸碘苯还可有效地将邻羟基芳酮的酰腙经氧化、重排成1，2-二酰基苯。

This one mode pays close attention to network credence foundation of the businessman very much.

这一模式非常关注商人的网络信用基础。

Cell morphology of bacterial ghost of Pasteurella multocida was observed by scanning electron microscopy and inactivation ratio was estimated by CFU analysi.

扫描电镜观察多杀性巴氏杆菌细菌幽灵和菌落形成单位评价遗传灭活率。