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The structures were identified by IR, UV,〓 NMR and element analyses. 2. Free radical 4-hydroxy-2,2,6,6-tetramethyl-1-piperidinyloxyl as catalyst, the phase transfer catalyzed method of oxidation eighteen semicarbazides to N-Aryl-2-Phenyl diazenecarboxamide with a solution of potassium ferricyanide in 2N aqueous sodium hydroxide and dichloromethane is described for the first time.

利用2,2,6,6-四甲基-4-羟基-1-哌啶氮氧自由基为相转移催化剂,在饱和铁氰化钾的2N氢氧化钠溶液与二氯甲烷的两相反应液中,催化氧化十八个取代氨基脲得到十八个相应的新型偶氮化合物N,2-二芳基二氮亚烯甲酰胺,均获得了较高的产率。

Methods: The protein and other impurity in the sample were precipitated by zinc acetate and potassium ferrocyanide after dipping of the sample. N,N-dichlorocyclohexylamine derived from sodium cyclamate by sodium hypochlorite in the filtrate was extracted by hexane. The HPLC separation was carried out with a phenomenex Gemini-C18 column using acetonitrile-water(7+3) or methanol-water (8+2) as mobile phase and detected by UV monitor at 314 nm. External standard method was used for quantification.

样品中甜蜜素浸提后,用乙酸锌和亚铁氰化钾试剂沉淀蛋白质等干扰杂质,过滤,用次氯酸钠将样品溶液中的甜蜜素转化为N,N-二氯环己胺经正己烷萃取后,在phenomenex Gemini-C18柱上,以乙腈-水(7+3)或甲醇-水(8+2)为流动相进行分离,HPLC-UV检测器在314 nm测定,外标法定量。

The furnace is possessed of multi-function complex lining, adjustable sub-high speed burner, burner adopting symmetric arrange, naturally draining away fume from fume offtakes, pressing soft sealing with rail, combining control by hand or automatic way.

该炉型属于台车式热处理炉,具有多功能复合炉衬和可调型亚高速烧嘴,烧嘴采用&一&字形左右对称布置,烟道为低位多点分布自然排烟,弹性接触轨道压紧软密封,自动与手动控制方式相结合。

In the experiment focused on decadal changes, GCMs reproduce the observed NAO shifts in recent decades by imposing strengthening trends on stratospheric wind. The cooling belt extending from North Africa to subtropical Eurasia is simulated accompanying the strengthening of NAO. East end of this cooling belt reaches the eastern flank of Tibetan Plateau.

在强调年代际变化的实验中,通过在平流层中强迫出水平风场的线性增强趋势,大气环流模式可以模拟出近几十年间冬季NAO指数的年代际上升;伴随着NAO正位相的增强,模式可以再现北非至副热带欧亚大陆的冷却带,且其东端可以到达青藏高原下游地区。

A network of trade routes, the Silk Road linked the people and traditions of Asia with those of Europe.

作为一个贸易通道网,丝绸之路将欧亚两地的人民和传统相连接。

This experiment unified flow cytometry, the monoclonal antibody technology, the cell fluorescence chemistry technology and unilized the union principle of antigen and antibody to examine T lymphocyte subgroup, the B lymphocyte change in circumference blood of the mice through the flow cytometry; At the same time, the agarose gelatin electrophoresis examined bovine colostrum effect on programmed cell death of thymus.

本实验正是将流式细胞术、单克隆抗体技术、细胞荧光化学技术相结合,并利用抗原抗体结合原理,采用流式细胞仪检测了小鼠外周血的T淋巴细胞亚群和B淋巴细胞;同时采用琼脂糖凝胶电泳技术检测了牛初乳对小鼠胸腺细胞凋亡的影响。

Shadrach, Meshach, and Abednego, answered and said to the king, O Nebuchadnezzar, we are not careful to answer thee in this matter.

有人曾将这些话与亚述王西拿基立所说过的那些话相比较,&不要听你所依靠的上帝欺哄你&(赛37:10)。

Upper and middle Silurian formations are denuded in Tahe area, only lower Silurian Kepingtage Fomation and Tata' ai' ertage Formation develop here with 2 sedimentary subfacies which are tidal flat and continental shelf, and 3 microfacies which are mixed flat, sand flat, and continental shelf mud.

塔河地区志留系缺失中、上统,只保留了下统柯坪塔格组及塔塔埃尔塔格组,发育滨海-浅海碎屑岩沉积,包括潮坪、陆棚等沉积亚相和中潮坪、低潮坪、陆棚泥等3个微相。

A New York based client commissioned Rangr Studio to design a Caribbean get-away large enough to accommodate his family and groups of friends.

一个纽约的业主委托Rangr工作室设计一个加勒比海别墅,希望能够有足够的空间接待自己的家人和朋友,该别墅位于多米尼亚北海岸线郊区,设计师将现代住宅风格和当地建材相结合。

Conducted by the Liz Dawson,co-founder of the London Neuro Psychotherapy Group,the seminar confirms that the apparently unhinged behaviour in Shakespeare's bestknown comedies is consistent with scientist research.

这次研讨会由伦敦神经精神治疗组织的创始人丽兹。道森主持,会议得出的结论是莎士比亚两部经典喜剧中那些明显精神错乱的行为和科学研究结果相符合。

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Singer Leona Lewis and former Led Zeppelin guitarist Jimmy Page emerged as the bus transformed into a grass-covered carnival float, and the pair combined for a rendition of "Whole Lotta Love".

歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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