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Dealcoholization temperature markedly influences the surface area and porosity of the resultant MAO-supports. When the support was pretreated at lower or higher temperature, the corresponding MAO-support shows very low surface area; 2.XRD and IR analyses indicate that MAO has reacted with the residual ethanol in the supports, which is an important manner to get MAO fixed on the carrier. Morever, XPS analyse indicates that MAO can also be coordinated with MgCl_2, which is another way to get MAO fixed on the support; 3.ICP and EDX analyses indicate that dealcoholization temperature not only determined the element content on the solid catalyst, but also influences the element distribution on the carrier; 4.The activities of the supported phenoxy-imine catalysts and the properties of resultant polymers are strongly dependent on the dealcoholization temperature. The support (MSP-5) obtained by treating MgCl_2·2.56C_2H_5OH at 160℃for 4 h, then modified by MAO is very effective for immobilizing complex 3, the resultant solid catalyst (MSPC-5) shows very high activity in ethylene polymerization, and its kinetics of polymerization is stable during the reaction process. Finally, PEs with spherical morphology and high bulk density (over 0.35g/ml) were obtained, without reactor fouling; 5.In this work, polymerization conditions such as alkylaluminums, Al/Zr ratio, temperature and H_2 had a pronounced effect on the activity of MSPC-5 and properties of PE;(3). New MgCl_2-Supported Single-Site Catalysts for Ethylene Polymerization In this work, a kind of new MgCl_2 support was obtained by anhydrous MgCl_2 co-milled with solid MAO, and it is a creative contribution. Then some single-site catalysts were supported on the new MgCl_2 support, and the resulted solid catalysts were tested in ethylene polymerization, the results indicated that: 1.XRD and IR analyses indicate that MAO does be coordinated with MgCl_2, which is in good agreement with the results obtained by XPS; 2.co-mlling time had no obvious effect on the texture of support after 12 hours; 3.In this work, MgCl_2 was co-milled with solid MAO for different hours, and then complex 3 was supported on these co-milled supports. It was found that co-milling time markedly influences the activity of solid catalysts, but it had negligible effect on the kinetic profile and the properties of resultant PE.

XPS研究结果表明,MAO不仅仅只和乙醇作用,MAO还与MgCl_2本身有一定的作用,这是一个极为重要的发现; 3、通过ICP和EDX表征,发现载体的脱醇温度直接影响着元素在固体催化剂中的含量及分布; 4、脱醇温度极大地影响着负载苯氧基亚胺类催化剂的活性和聚合物的性能,特别是原始载体经160℃活化4小时制备得到的固体催化剂MSPC-5的活性明显高于其他脱醇温度条件下制得的固体催化,并且催化剂寿命长,表现出稳定的动力学行为,最终获得了高堆密度(大于0.35g/ml)的球形聚乙烯颗粒; 5、本文选择MSPC-5为研究对象,考察了聚合反应参数对催化剂的活性及其聚合物的影响,研究发现:不同的烷基铝对催化剂具有非常重要的影响,特别足TIBA对MSPC-5的助催化活性最高,烷基铝的加入量有一个较佳值,聚合温度为80度时活性最高,H_2的加入使催化剂的活性明显降低且聚合物的分子量也减小;、新型氯化镁载体负载单活性中心催化剂催化乙烯聚合本文创造性采用固体MAO与无水氯化镁直接进行共研磨,制备出了一种的新型的氯化镁载体,并将该载体用于多种单活性中心催化剂的负载化研究,研究表明: 1、通过BET、XRD的表征,再次证实了MAO与MgCl_2之间具有直接作用,与XPS的研究结果相一致; 2、当研磨时间高于12小时时,延长研磨时间对载体的结构没有显著的影响; 3、将配合物3负载于共研磨时间不同的一系列载体上,乙烯聚合结果表明,尽管共研磨时间对负载催化剂的活性具有明显的影响,但是它对聚合物的性能以及催化剂的影响不明显。

By exchanging the carboxyl termini of NR2A and NR2B subunit, surface NR2B-containing NMDA receptors occurred more in a clustering manner,whereas NR2A-containing ones more diffusedly.

然而,NR2亚单位中与这些支架蛋白相结合的功能区却无法直接解释NR2A与PSD-95蛋白之间的这种特异性的相互作用。

Based on the dynamic equation, the transport and acceleration of out-flowing ionospheric ions in the magnetosphere are studied by means of finding the ion distribution function. They include two parts: the study of static ion distribution with analysis and numerical compute; the study of ion acceleration by induced electric feild in the period of dipolarization of taillike geomagnetic lines in the substorm expansion phase with the numerical simulation of the ion distribution function.

本文在磁层中上行离子的加速与传输理论研究领域中,采用动力论方程,用求解离子分布函数的方法来研究问题:(1)用解析求解和数值计算的方法,对上行离子在不同Kp指数条件下磁场位形中的定态分布进行了研究;(2)用数值模拟计算分布函数的方法,对上行离子在亚暴膨胀相磁场向偶极形驰豫过程中受磁尾的感应电场加速进行了研究。

Molecular data place Empetrum and its relatives firmly within the Ericaceae, and in particular within the subfamily Ericoideae, in agreement with phytochemical and palynological data, and there they are best recognized as a separate tribe.

分子证据支持把在Empetrum 和它的亲缘类群放在杜鹃花科Ericaceae内,尤其是Ericoideae亚科内,这与植物化学和孢粉学证据相一致,它们最好作为一个独立的族。

Lastly, based on analysis on phylogentic relationships among 39 ciliates combined with their main morphologic characters, some conclusion were drawn: 1 the monophyly of the peritrichs was strongly supported, and its subclass rank in the class Oligohymenophorea is reasonable; 2 the genus Epistylis might not be monophyletic, and the peristomial area, especially the peristomial lip, might be an important phylogenetic character within the genus Epistylis; 3 the taxonomic rank of the genus Carchesium and the genus Campanella were suggested to be adjusted; 4 Opisthonecta probably diverged from peritrichs with stalks; 5 the phylogenetic tree of peritrichs was reconstructed based on the molecular information inferred from SSrRNA gene sequences and the morphology.

测定了6科8属13种缘毛类纤毛虫的SSrDNA序列,将构建的最大简约树和邻接树与形态学相结合,分析得出:1)缘毛类纤毛虫是单系的,其分类地位是隶属于纤毛门寡膜纲缘毛亚纲:2)指出累枝虫属可能不是单系的,口围区是累枝虫属中重要的系统发育特征;3)建议调整独缩虫和聚钟虫属的分类地位;4)得出后游虫可能是由有柄缘毛类进化而来的类群;5)基于缘毛类反口区结构和SSrRNA基因序列提供的信息重建了缘毛类纤毛虫的系统发育树。

The former shifts equatorward when AE increases, just as the auroral oval does; the latter is divided into two sections: the midnight section shifts poleward when AE increases, while the morning section shifts equatorward.

在亚暴膨胀相,随着AE指数增大,整个极光卵向赤道扩展,而极光电集流带却表现出分段差异的特点:下午—黄昏东向电集流带向低纬移动,晨侧西向电集流带也向赤道移动,而子夜—凌晨西向电集流带则向极移动。

If this theory of value is combined with other elements of classic utilitarianism, the resulting theory can be called perfectionist consequentialism or, in deference to its Aristotelian roots, eudaemonistic consequentialism .

如果这种价值理论与经典功利主义的其他元素相结合,所产生的理论可以被称为完美结果论,或者是考虑到亚里士多德的根源,eudaemonistic结果主义。

Using the phases of ferrum and the parameters above to divide the subzones of interstratified-oxidation zone has both theoretical and practical significance in prospecting for u-ranium deposits of this type.

应用铁物相特征及其以上比值,可以简捷地对层间氧化带进行亚带的划分,这对指导铀矿勘查具有重要理论和实践意义。

The chemical constituents of extracts of Tamarindus indica L were determined by GC-MS. The relative contents of constitutes were determined by area normalizing method. 48 compounds were identified, amounting to total mass fraction 98.5%. The main compounds were 5-methyl-2(3H)-furanone, diethyl succinate, furfural, hexadecanoic acid, linolenic acid, 5-methylfurfural, oleic acid, linoleic acid, etc.

并利用气相色谱仪-质谱仪对罗望子萃取物的化学组成进行了分析鉴定,并用面积归一化法测定了各种成分的质量分数,共鉴定了48种成分,占总质量分数为98.35%,其中主要成分为:5-甲基-2(3H)-呋喃酮、丁二酸二乙酯、糠醛、十六酸、亚麻酸、5-甲基糠醛、油酸、亚油酸等。

Hexadecanoic acid,stearic acid,oleic acid,linoleic acid and linolenic acid from soybean salad oil have been quantitatively analyzed by using gas chromatograph combined with,Heated-filament pyrolyzer and Curie-Point pyrolyzer.

方法采用气相色谱仪,FID检测器,FFAP毛细柱,热丝型裂解器及居里点裂解器,对大豆色拉油的五种主要组分:软脂酸,硬脂酸,油酸,亚油酸,亚麻酸进行了定量分析。

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歌手leona刘易斯和前率领的飞艇的吉他手吉米页出现巴士转化为基层所涵盖的嘉年华花车,和一双合并为一移交&整个lotta爱&。

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