亚氨基的

Dimethylhexane-1,6-dimethyleurethane is the key material for preparation of 1,6-hexamethylene diisocyanate by non-phosgene route. Our work mainly focuses on the study of the catalytic performances of metal oxysalts and metal oxides for the ammonolysis of DMC to HDU-M. Experiment effect showed the ammonolysis was omposed by two steps, in which the first step was easier to occur than the second.

中文摘要六亚甲基-1，6-二氨基甲酸甲酯是非光气合成六亚甲基二异氰酸酯的关键原料，本文主要对金属含氧酸盐和金属氧化物这两类用于碳酸二甲酯胺解合成HDU-M 的催化剂进行了初步研究并优化了工艺条件。

Methods Activate GAMP with cyanogens bromide and prepare GAMP-protein conjugates using ADH as a linker and EDAC as a coupling agent.

方法采用溴化氰活化多糖，以无水己二酸二肼为连接剂，1-乙基-1-3-(3-二甲基氨基-丙基)-碳化二亚胺为偶联剂，制备结合物并免疫小鼠，检测小鼠血清中抗GAMP与抗载体蛋白抗体及抗GAMP抗体的杀菌活性。

Methods Activate GAMP with cyanogens bromide and prepare GAMP-protein conjugates using ADH as a linker and EDAC as a coupling agent. Immunize mice with the conjugates and determine the antibodies against GAMP and carrier proteins in their sera as well as the bactericidal activity of antibody against GAMP.

采用溴化氰活化多糖，以无水己二酸二肼为连接剂，1-乙基－1-3-（3-二甲基氨基－丙基）－碳化二亚胺为偶联剂，制备结合物并免疫小鼠，检测小鼠血清中抗GAMP与抗载体蛋白抗体及抗GAMP抗体的杀菌活性。

The clean synthesis of 1,6-dicarbamate hexane from dimethyl carbonate and 1,6-diamine hexane is studied.

对由1，6-己二胺和碳酸二甲酸合成1，6-六亚甲基二氨基甲酸甲酯的洁净化工艺过程进行了初步研究。

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Further aza-Wittig reactions of iminophosphorane 3 with aromatic isocyanates gave the carbodiimide s 4, which were reacted with secondary amines to give 2-dialkylamino-thieno[2,3-d]pyrimidin-4(3H)-ones 6 in the presence of catalytic amounts of EtO-Na+ in 58%～82%.

应用膦亚胺3与芳基异氰酸酯的氮杂Wittig反应，生成的碳二亚胺4，再与仲胺作用得到中间体5，而后在醇钠的催化下关环制得2-二烷氨基噻吩并[2，3-d]嘧啶-4(3H)-酮衍生物6，产率为58%～82

The hydrophobic core serves as a reservoir for water-insoluble drugs.Hence,these nanoparticles can be used as carriers for hydrophobic drugs.For the synthesis of cholesterol-modified glycol chitosan conjugates,a carboxyl group was initially introduced to cholesterol molecule using succinic anhydride,and then covalently coupled with the primary amino group of glycol chitosan in the presence of 1-ethyl-3-(3-dimethylaminopropyl)-carbodiimide hydrochloride and N-hydroxyl succinimide.

本文采用二步反应将胆固醇接枝到乙二醇壳聚糖，首先将胆固醇进行羧基化，将胆固醇与琥珀酸酐反应生成胆固醇半琥珀酸酯，然后用1-乙基-3-(3-二甲基氨丙基)碳二亚胺盐酸盐与N-羟基琥珀酰亚胺作为偶联剂，将胆固醇半琥珀酸酯的羧基与乙二醇壳聚糖主链的氨基进行反应，得到胆固醇疏水改性乙二醇壳聚糖共聚物。

Methylene blue is reduced and faded by ascorbic acid in the medium of dilute hydrochloric acid（ pH=2） with sulfanilic acid as a catalyst.The optimal conditions of the fading reaction were investigated in detail.Based on this fading reaction a new spectrophotometric method for the determination of ascorbic acid was established.

确定了亚甲蓝与抗坏血酸褪色反应的最佳条件，在 pH=2的缓冲溶液和对氨基苯磺酸存在的条件下，抗坏血酸能够很快还原亚甲蓝并使之褪色，褪色反应的体系具有很好的稳定性。

Twelve new Schiff bases of 5-amino-1H-1,2,3,4-tetrazolyl were synthesized. These Schiff bases were further converted into α-(5- tetrazolyl)-aminoalkyl phosphonates.

合成了12个新的5—氨基—1H—1，2，3，4—四唑的Schiff碱，而后与亚磷酸二乙酯反应，合成出了12个新的含四唑基的α-氨基烃基膦酸酯，通过IR，^1H NMR，^31P NMR和元素分析证实了它们的结构。

Then, it was condensed with-valine methyl ester to form a chiral imine, which was reacted with allyl zinc bromide in the presence of CeCl3·7H2O to afford the corresponding chiral homoallylic amine with high optical activity.

-N-Boc-3-苯基-2-氨基丙醛与-缬氨基酸甲酯缩合生成手性亚胺，在七水合三氯化铈（CeC13·7H2O）催化以及底物的手性诱导作用下，该手性亚胺与烯丙基溴化锌经不对称加成反应合成了高光活性的单烯丙基化手性胺。

The split between the two groups can hardly be papered over.

这两个团体间的分歧难以掩饰。

This approach not only encourages a greater number of responses, but minimizes the likelihood of stale groupthink.

这种做法不仅鼓励了更多的反应，而且减少跟风的可能性。