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Immunofluorescence confirmed that sweat glands in normal mice did not present gamma-aminobutyric acid receptor subtype GABAA andα-amino-3-hydroxy-5-methylisoxazole-4-propionic acid/kainic acid subtype of glutamate receptor. Mature mice with reactive sweat glands that declined more than 25% compared to baseline were defined as anhidrotic mice.

免疫组织荧光染色未发现在正常小鼠皮肤组织及汗腺的分泌细胞存在γ-氨基丁酸A型(gamma-aminobutyric acid,GABAA)受体α1亚单位、谷氨酸受体亚型α-氨基羟甲基恶唑丙酸(α-amino-3-hydroxy-5-methylisoxazole-4-propionic acid , AMPA )GluR1/2/3/4亚单位和海人酸(kainic acid,KA)受体GluR5/6/7亚单位的表达。

Immunofluorescence confirmed that sweat glands in normal mice did not present gamma-aminobutyric acid receptor subtype GABAA andα-amino-3-hydroxy-5-methylisoxazole-4-propionic acid/kainic acid subtype of glutamate receptor.Mature mice with reactive sweat glands that declined more than 25% compared to baseline were defined as anhidrotic mice.

免疫组织荧光染色未发现在正常小鼠皮肤组织及汗腺的分泌细胞存在γ-氨基丁酸A型(gamma-aminobutyric acid,GABAA)受体α1亚单位、谷氨酸受体亚型α-氨基羟甲基恶唑丙酸α-amino(来源:Ad1d1BC论文网www.abclunwen.com-3-hydroxy-5-methylisoxazole-4-propionic acid , AMPA GluR1/2/3/4亚单位和海人酸(kainic acid,KA)受体GluR5/6/7亚单位的表达。

A series of diazonium salts of 4-(N-methyl-N-phenylamino)-3-amino-1,8-naphthalic anhydride 5a, its naphthalimide derivative 5b, and 5e were designed and synthesized,and it was the first time to discover that aromatic radical-induced intramolecular aromatic 1, 5-hydrogen transfer was also involved in the nitrogen-contianed system during Pschorr cyclization.

实验设计合成了4--3-氨基-1,8-萘酐的重氮盐5a、其衍生物N-丁基-4--3-氨基-1,8-萘酰亚胺的重氮盐5b和N--4--3-氨基-1,8-萘酰亚胺的重氮盐5c,并首次发现了通过普朔尔环化反应以氮甲基化的氮为桥原子的体系存在着芳香自由基诱导的芳香1,5-氢转移。

We examined the association between intakes of the heterocyclic amines 2-amino-3,8-dimethylimidazo[4,5,-f]quinoxaline, 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine,2-amino-3,4,8-trimethylimidazo[4,5,-f] quinoxaline, and meat-deried mutagenicity and risk of distal colon adenoma using a cooking method questionnaire administered in 1996 in the Health Professionals Follow-up Study cohort.

我们卫生保健跟踪调查组采取烹调方法调查表的形式在1996年调查了摄入杂环胺2-氨基-3,8丙烷[4,5,-f] 喹噁啉,2-氨基-1甲基1-6-苯基亚氨基[4,5-b] 吡啶,2-氨基3,4,8-trimethylimidazo[4,5,-f] 喹噁啉和肉类衍生致突变物与患末端结肠腺瘤危险性的关系。

We examined the association between intakes of the heterocyclic amines 2-amino-3,8-dimethylimidazo[4,5,-f]quinoxaline, 2-amino-1-methyl-6-phenylimidazo[4,5-b]pyridine,2-amino-3,4,8-trimethylimidazo[4,5,-f] quinoxaline, and meat-derived mutagenicity and risk of distal colon adenoma using a cooking method questionnaire administered in 1996 in the Health Professionals Follow-up Study cohort.

我们卫生保健跟踪调查组采取烹调方法调查表的形式在1996年调查了摄入杂环胺2-氨基-3,8丙烷[4,5,-f] 喹噁啉,2-氨基-1甲基1-6-苯基亚氨基[4,5-b] 吡啶,2-氨基3,4,8-trimethylimidazo[4,5,-f] 喹噁啉和肉类衍生致突变物与患末端结肠腺瘤危险性的关系。

Results show that, by using thionyl chloride and N,N-dimethyl formamide as chlorinating reagent and dichloromethane as solvent and taking -15℃ as reaction temperature, Z-iomer crystals with pale white color and stable to temperature can be obtained with an overall yield of 70%.

以2-(2-氨基噻唑-4-基)-2-甲氧亚氨基乙酸为原料,经盐酸化、氯代等反应合成了Z-2-(2-氨基噻唑-4-基)-2-甲氧亚氨基乙酰氯盐酸盐;氯代时以用亚硫酰氯和N,N-二甲基甲酰胺的混合物代替五氯化磷作氯化剂,并考察了温度和溶剂对氯代产物中Z-异构体和E-异构体收率的影响。

IR spectra and UV spectra of the complexes are described. The results show that two phenolic oxygen and two imino nitrogen atoms in H2L coordinate to M ions.

通过对配合物的红外光谱和紫外光谱测定与归属,推测在三个过渡金属Schiff碱配合物中配体是通过酚羟基的氧原子和亚氨基的氮原子进行配位的。

Furthermore, single-point energy calculations were refined at the QCISD level of theory with the same basis set (6-311++G**). As a result, the singlet reaction of silylene with isothiocyanic acid contain S-atom abstraction channel, N—H inserted channel, and NH abstraction channel, respectively.

又用QCISD/6-311++G**//B3LYP/6-311++G**方法计算了各个驻点的单点能,计算结果表明单重态的硅烯与异硫氰酸的反应有抽提硫、插入、抽提亚氨基的路径。

The complexes were characterized by elemental analysis,UV,IR,TG,NMR and molar conductance measurements.Their formulas were in accordance with C34H32O8N2LnCl·nH2O or 〔(L4)2LnCl·nH2O,Ln=Nd,n=4;Ln=Pr,Yb,n=2;Ln=Sm,Eu,Dy,n=1〕.All the water molecules were uncoordinated.Dinuclear complexes were observed in the coordination environment.The coordination number of central ions was nine.

经元素分析、红外光谱、紫外光谱、核磁共振谱、质谱、摩尔电导、差热热重分析确证结构,其化学式为C34H32O8N2LnCl·nH2O,简写为:(L42LnCl·nH2O,Ln=Nd,n=4;Ln=Pr,Yb,n=2;Ln=Sm,Eu,Dy,n=1;该类配体是以酚氧原子、亚氨基的氮原子、桥联的羧基氧原子以及氯原子同稀土离子配位,形成了九配位的双核配合物。

Near-critical water is a promising reaction medium for conducting the hydrolysis of nitriles without the addition of any additives.

亚氨基二乙腈在没有外加催化剂的近邻界水中可以顺利发生水解。实验测定了亚氨基二乙腈在近临界水中(压力10MPa,温度200~260℃,反应时间10~60min)的水解反应动力学数据并考察了时间、温度、压力和初始反应物/水比对反应物转化率和产物产率的影响。

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