五醇

Objective To compare the pharmacodynamics of five alcoholic extractives(Scorpion,SP、Centipede,CP、Stiff Silkorm,SS、Lumbricus,LB、Cicada Slough,CS)on anticonvulsion,and explore their mechanism of anticonvulsant action.

目的比较五种单味中药醇提物(全蝎SP、僵蚕SS、地龙LB、蝉衣CS、蜈蚣CP)的抗惊厥作用，并探讨其作用机制。

Methyl-5-ethyl-2-thiouracil,m.p.211°,was prepared according to the direc- tions of Johnson and Baily.4-Methyl-5-ethyl-uracil,m.p.236°,was formed in a 81% yield from 4-methyl-5-ethyl-2-thiouracil by boiling the latter with an aqueous solution of monochloroacetic acid.4-Methyl-5-ethyl-uracil reacted with phosphorous oxychloride and phosphorous pentachloride,giving 4-methyl-5-ethyl-2,6-dichloropy- rimidine in a 79% yield.

14-甲基5-乙基-2，6-二氯代嘧啶曾用磷醯氯和五氯化磷与其相应的2，6-二羟基嘧啶作用制取。(2)4-甲基-5-乙基-2，6-二氯代嘧啶与醇钠作用，极易转变成4-甲基-5-乙基-2，6-二烷氧基嘧啶。(3)4-甲基-5-乙基-2，6-二甲氧基嘧啶和2-氧代-3，4-二甲基-5-乙基-6-甲氧基嘧啶在高温时重排成其稳定构型的的异构体：1，3，4-三甲基-5-乙基-2，6-二氧代嘧啶。

We have investigated on the chemical constituents of Nepeta partite collected from Gansu Zhuanglang, and twenty eight compounds were isolated from the methanol extraction of this species by chromatography techniques. Twenty five compounds were identified by means of chemical and spectra methods IR, FABMS, EI-MS,〓, DEPT, and 2D NMR）, among which four compounds were new as isopimar-15-en-3β, 8β, 20-triol; phenylethanal-3-O-（2'-glycerin）-5-O-β-D-glucopyranoside; 3-O-linolenoylglyceryl-6'-O-(α-D-galactopyranosyl）-β-D-galactopyranoside; ethyl rosemarinate.

我们对采自甘肃庄浪的康藏荆芥进行了化学成分的研究，利用层析手段从该植物的甲醇浸膏中分离出二十八个化合物，经化学方法和波谱技术（红外，质谱，一维和二维核磁共振谱）鉴定了二十五个化合物的结构，其中四个为新的化合物，它们分别是：异海松-15-烯-3β，8β，20-三醇；苯乙醇-3-O-（2'-甘油基）-5-O-β-D-吡喃葡萄糖甙；3-O-亚麻酰基甘油-6'-0--β-D-吡喃半乳糖甙；迷迭香酸乙酯。

A pentacarbonyl complex (3) isolatedfrom the same reaction from which the complex (1) is obtained, whose accuratestructure is yet known, is preliminarily studied.

对从含吡啶基团的二硫醇三齿配体与Fe_3_(12)的反应中得到的另一个准确结构有待确定的五羰基化合物(3)进行了初步的性质研究及表征。

Said invented technical scheme is characterized by that it uses one kind of several kinds of five-and/or four-carbon alcohol to break the wall of wet-dried cell thallus in which the polyhydroxy fatty acid ester is self formed and extract the polyhydroxy fatty acid ester.

本发明的技术方案是用五和/或四碳醇中的一种或几种自形成聚羟基脂肪酸酯的湿/干细胞菌体破壁提取聚羟基脂肪酸酯。

Chemical Products, Chemicals: inorganic acid, sodium compounds, potassium compounds, calcium compounds, barium compounds, manganese compounds, chromium compounds, nickel compounds, zinc compounds, magnesium compounds, aluminum compounds, single-element chemical products, even items of the five machines Chemical products, paraffin, waxes other chemicals, coke, oil and chemicals, alcohol, aldehyde chemicals, acetate chemicals, ketones, ethers, phenols chemicals, alkanes, alkenes, acetylene chemicals, amine chemicals, aromatic chemicals, Miscellaneous organic chemicals, acid chemicals, other chemicals, dyes and intermediates, pigment materials, plastic materials, agricultural chemicals: fertilizers, pesticides, growth agents, plastic sheeting, etc., equipment, pyrophoric alloys, articles of combustible materials , chemical reagents, rubber, imports, machinery and equipment, machinery and equipment, apparatus; photographic equipment; printing equipment; general machinery; textile equipment; Machine Components; a variety of equipment, Shanghai, Zhejiang, Guangdong, Jiangsu high-quality, low-carbon The new satellites technology goods manufacturers, exporters, wholesalers, traders, USA, United States importers, wholesalers, retailers, investors, designers, planners, please contact our office, George Chen, Mobile :+

化工产品类，化工原料：无机酸，钠化合物，钾化合物，钙化合物，钡化合物，锰化合物，铬化合物，镍化合物，锌化合物，镁化合物，铝化合物，单元素化工品，什项五机化工品，石蜡、蜡类其他化工品，焦、油化工品，醇、醛化工品，酯化工品，酮、醚、酚化工品，烷、烯、炔化工品，胺化工品，芳烃化工品，什项有机化工品，羧酸化工品，其它化工原料，染料及中间体，颜料原料，塑料原料，农用化工品：化肥，农药，生长剂，农膜等，器材，引火合金，易燃材料制品，化学试剂，橡胶，进口，机械设备，机械及设备，仪器；摄影器材；印刷器材；通用机械；纺织器材；机械基础件；各种成套设备，中国上海，浙江，广东，江苏优质，低碳，新颗科技商品生产商，出口商，批发商，贸易商，美国，美利坚合众国进口商，批发商，零售商，投资商，设计师，规划师们，请与我处联系，George Chen，Mobile：+

Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established. Using 2,2,6,6-tetramethyl-4-piperinol as the starting material, the product was synthesized successfully through oxidation, free-radical reaction and transesterification in overall yield of 57.6%.

本文研究建立了三个受阻胺类光稳定剂的合成工艺，探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因，并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1，2，2，6，6-五甲基哌啶醇的酯交换反应的基础上，建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺，分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765，所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

Transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperidinol was studied with tetraisopropyl orthotitanate ,lithium amide and di-n-octyltin oxide used separately as catalysts.

对癸二酸二甲酯与1，2，2，6，6-五甲基哌啶醇的酯交换反应进行了研究；分别考察了四异丙基钛酸酯、氨基锂、氧化二辛基锡3种催化剂的性能；采用氢核磁共振确定了产物的结构；考察了以四异丙基钛酸酯为催化剂时反应温度、反应时间、原料配比和催化剂用量对反应的影响。

The synthetic technologies of three hindered amine light stabilizers were established, the reason for the insoluble side products formed in the production of polymerized hindered amine light stabilizers were studied, and a series of novel hindered amine light stabilizers with antibacterial properties were designed and synthesized in this present paper.1. Based on the investigation of the transesterification between dimethyl sebacate and 1,2,2,6,6-pentamethyl-4-piperinol, the synthetic technologies of Tinuvin292 and Tinuvin 765 were established. The two kinds of hindered amine light stabilizers were obtained in the yield of 93.3% and 92.4% respectively and qualified as the advanced level of the kindred overseas products.2. The synthetic technology of Tinuvin123 was studied and established.

本文研究建立了三个受阻胺类光稳定剂的合成工艺，探索了聚合型受阻胺类光稳定剂生产过程中不溶性副产物产生的原因，并设计、合成了一系列具有抑菌活性的新型受阻胺类光稳定剂。1、在研究癸二酸二甲酯与1，2，2，6，6-五甲基哌啶醇的酯交换反应的基础上，建立了受阻胺类光稳定剂Tinuvin292、Tinuvin765的合成工艺，分别以93.3%和92.4%的收率得到了光稳定剂Tinuvin292、Tinuvin765，所得产品质量达到了国外同类产品的水平。2、研究建立了受阻胺类光稳定剂Tinuvin123的合成工艺。

Among the five oily ingredients tested, C16~18 fatty alcohol can well facilitate the formation of liquid crystal; polar materials PPG-15 stearyl ether and stearic acid are not favorable for the formation of liquid crystal, while non-polar material white oil shows no effect on the formation of liquid crystal.

在所研究的五种油质原料中，十六~十八醇可以很好的促进液晶结构的形成；极性的 PPG-15硬脂醚与十八酸不利于液晶的形成；而非极性的白油则不影响体系液晶结构的形成。

The concept of equivalent rotationally rigidity is offered and the formula of rotationally rigidity is obtained.

主要做了如下几个方面的工作：对伸臂位于顶部的单层框架—筒体模型进行分析，提出了等效转动约束的概念和转动约束刚度的表达式。

Male cats normally do not need aftercare with the exception of the night after the anesthetic.

男猫通常不需要善后除了晚上的麻醉。