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Based on groups of single factor experiments, the yield could reached to 88.8% with the conditions: sodamide: cedrol :dimethyl sulfate = 1.6:1:0.9, refluxed 2h in first step reaction, and reacted at room temperature 1h after instillation of dimethyl sulfate, followed refluxed 1h in the second steps.

通过多组单因素实验发现氨基钠:柏木脑:硫酸二甲酯的摩尔比为1.6:1:0.9,第一步反应条件控制在回流2h,第二步反应先室温(25℃)滴加硫酸二甲酯后反应1h,再回流反应1h,得率可达88.8%。

Then,in the bovine serum albumin buffer solution containing disodium hydrogen phosphate and citric acid,ferrite/polyacrylamide was added with crosslinker glutaraldehyde and then be enwrapped by BSA.

首先在反相微乳液体系中制备出Fe3O4/PAM磁性微球;然后在牛白蛋白的磷酸氢二钠-柠檬酸缓冲溶液中,以戊二醛为交联剂,加入Fe3O4/PAM微球,使蛋白质特异性吸附在微球上。

When proceeding the research of drug identification by ultraviolet spectrophotometry, this paper adopts the approaches below: to identify Metronidazole Buccal Tablets and Potassium Sodium Dehydroandroan Drographolide Succinate by ulviolet maximum absorbent wavelength; to identify Metronidazole Disodium Phosphate for Injection by ulviolet maximum absorbent wavelength and minimum absorbent wavelength; to identify Ceftriaxone Sodium for Injection and Clarithromycin Tablets by retention time of high performance liquid chromatography- ultraviolet spectrophotometry.

通过测定紫外最大吸收波长λ_(max鉴别甲硝唑口颊片和炎琥宁、测定紫外最大吸收波长λ_(max和最小吸收波长λ_(min鉴别注射用甲硝唑磷酸二钠,结合高效液相色谱(high performance liquid chromatography-ultraviolet detector,HPLC-UV)中保留时间的测定鉴别注射用头孢曲松钠和克拉霉素片,本文建立了药物鉴别的紫外分光光度法。

The process of diethyl carbonate synthesis by transesterification reaction of ethanol with ethylene carbonate,coproducing useful ethylene glycol was investigated using catalyst of sodium ethylate .

研究了以乙醇钠为均相催化剂,碳酸乙烯酯和乙醇酯交换合成碳酸二乙酯同时联产乙二醇的过程。

As a precursive work of polymerization directly from vesicles, a polymerizable surfactant, allyl dodecyl dimethylammonium bromide was synthesized, and spontaneous stable vesicles were formed from aqueous solutions of ADDB and sodium dodecyl sulfonate in equimolar composition.

作为可聚合囊泡制备的前期基础工作,研究了一种可聚合的囊泡体系:1-丙烯基-2,2,二甲基-十二烷基溴化胺和ADDB与十二烷基磺酸钠的等摩尔比混合体系。

The factors which affect the average molecular weight of the polymer of AM and DMDAAC were investigated. The optimal reaction conditions are as follows: the concentration of monomer AM was 30%, while DMDAAC was 5%; the reaction temperature was 30℃, the amount of initiators at the low temperature stage was 0.05‰(compared to the weight of the monomers joining the polymerization), while V-50 was 0.025‰, the weight ratio of potassium persulphate to sodium bisulphite is 1:1, the amount of carbamide was 40‰, and complexing agent was 0.05‰, besides, aerate nitrogen gas for 8min, then the high molecular weight polymer (M=1.217×10^7) could be got after 16h reaction.

研究了影响AM与DMDAAC共聚物的平均分子量的因素,得到了优化条件为:单体浓度为30%,DMDAAC与AM摩尔比为5:95,聚合温度为30℃,低温段引发剂用量为0.05‰,K2S2O8与NaHSO3质量比为1:1,偶氮二异丁基脒盐酸盐(V-50)用量为0.025‰,尿素用量为40‰,乙二胺四乙酸二钠(EDTA-2Na)用量为0.05‰,在此优化条件下聚合反应16h后得到分子量为1.217×10^7的阳离子型聚丙烯酰胺。

An ODS column was selected as the separation column at 25 ℃, and pH 4.50, 0.02 mol/L of trisodium citrate-0.05 mol/L sodium phosphate dibasic to methanol (95:5, volume ratio) without ion-pair at a flow rate of 1.0 mL/min.

该实验采用ODS柱,流动相为V(0.02 mol/L柠檬酸三钠-0.05 mol/L磷酸氢二钠):V=95:5的溶液,用电化学检测器检测。

The reaction of sodium alkylcycloperitadienide with metal chlorides gave derivatives of bisdichlorides of titanium, zirconium and hafnium where alkyls were n-propyl and n-butyl.

本文报导烷基环戊二烯基钠与金属氯化物反应合成钛、锆和铪的双金属二氯化物以及通过卤素交换制备双钛的二氟化物的方法。

As the characteristic of mulberry, it was used the soda-sodium pyrophosphate-sodium dodecyl sulphate process with low temperature cooking schedule, the major purpose was to decoating than deliganification.

针对这一特点,我们采用了烧碱-焦磷酸钠-十二烷基磺酸钠的方法,进行低温缓慢蒸煮。

In which 18.02 and 230.08 are the molecular weights of water and sodium tartrate dihydrate, respectively; W is the weight, in mg, of sodium tartrate dihydrate; and V is the volume, in mL, of the Reagent consumed in the second titration.

其中18.02和230.08是水和酒石酸钠的各自分子量,W是二水酒石酸钠的重量,以mg计,V是第二次滴定消耗的卡尔试剂的体积,以毫升计。不好意思,废话不多说,请大家多指教

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What would he tell Judith and the children?

他将怎样告诉朱迪丝和孩子们呢?

I this is at that time, the opinion with peacockish true girl is full of in a heart.

这就是当时的我,一个心中布满虚荣的女孩子真实的想法。

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